stone at the left corner and stretched             The timber and iron shingles, smaller
stone alternating ·with herringbone rubble      in cross section, contribute to divide the
- all of them beneath the parget. The           loads and to release them on to the main
base of the wall is cooler because of rising    supporting structures. Another typology,
damp. Delamination of plaster appears in        widespread in structures of the last
infrared thennograms as warmer areas. In        decades of the nineteenth century and the
the same building but in the ·western wall      beginning of the twentieth century, is
of the main hall, thermograms show              that of small vaults made of hollow
thermal anomalies, typical of filled holes      terracotta wares and supported by iron
used during the castle construction, as         beams with average spacing of 0.8 to 1.2
warmer areas.                                   m (2.6 to 3.9 ft).
    In Oratorio Suardi, 'I'rescore, Italy, the     Timber laths cover the supporting
masonry is composed of rubble and lin'le        structures. Embedded in mortar or sand,
mortar. The parget is completely frescoed.      the paving finishes the floors. Paving is
A homogeneous heating was performed to          usually made of timber, stone, bricks or
allow the infrared detection of the bond        tile, disposed with bonding that is
of the wall (8 October 1999). A convective      stretched, herringbone or other. The
heating for 2 h (3500 \tV, distributed on       development of floor tiling produced
1500 m3) was applied and the rubble             different kinds of patterned tiles with
beneath the parget appeared. The                different thermal properties.
preciousness of the surfaCe avoids a
thermal gradient higher than 1.5 Klrl           Vaults
(1.5 °C.!rl; 2.7 °F·h-1).
                                                Structural masonry (mortar and bricks or
   The structural masonry of the San            stone quoins) usually are used as
Michele monastery, Lunate Pozzolo, Italy,       supporting structure of vaults1 dome
was also investigated by infr<Hed               vaults and domes (cupolas).
thermography. A thermogram ·was
recorded after 1 h of lighting by two              Shuttering bricks/stones are used to
                                                flank the basis of the vaults (for about one
lamps of sao ,~, each, disposed 1 Ill           third of the height). In fact increasing the
                                                weight of the vault lets it withstand the
(40 in.) from the surface. The average          drift better. Because of the different
temperature increase at permanent regime        thickness of the structure thermograms
was about +3 K (3 °C ~ 5.4 °F). The bond        show a varying temperature from the
of the masonry is detectable in a               basis to the apex, at least in almost steady
thermogram as rubble stones despite the         state conditions. Transversal metallic
heterogeneous heating of the parget,            chains, spanned at the bases of the vaults,
thicker than 30 mm (24 May 1999).               help absorb the horizontal thrust.
                                                Another technique to reduce the drift is to
   In cases of mixed texture infrared           lighten the vaults ·with interlocking pipes
thermography is successfully applied to         to form rings of lightweight permanent
localize placement of bricks and stone. At      shuttering.
Sant' Abbondio cloister, Como, Italy
(12 May 1999) infrared thermography                 After the seventeenth century lighter
makes it possible to detect the bricks          vaults were built by using panels of reeds
around the arches and beneath the parget        nailed on wooden centering. Often
as wanner areas after 20 min of solar           frescoes decorated the pmgcts that cover
irradiation. The colder areas correspond to     the panels. Thermography makes it
rubble.                                         possible to see the timbering and the
                                                metallic fixtures, at ease during transient
Analysis of Horizontal                          conditions.
Structures
                                                   The largest domes are often made 'With
In the construction pattern the horizontal      external iron beam struu ures supporting
structures distribute the loads to the          the metallic or timber shell of the bottom
vertical elements. Briefly, they can be         face.
classed as follows.
                                                Roofs
Floors (Girders, Shingles, Laths
and Paving)                                     Generally a suitable roof covers the
                                                structure. Timber beams and rafters are
The main supporting structures, with            the simplest supporting structure of
larger cross section, <ne the beams or          double pitch and hipped roofs. Trusses
girders. Usually the materials are timber,      and a third byer of shingles are used in
iron and cast iron. They can be hidden in       larger roofs. Additionally, the coating lies
the thickness of the floor or can be            on a lath layer. The roof tiles are tht' mmt
external, sometimes with parget or plaster      external layers, used to ·withstand the
facing or just a painted surface.               weather. Other covering are made of
                                                wooden shingles, disposed with a
                                                multilayer arrangement or slabs of stones
636 Infrared and Thermal Testing
(slate, gneiss or other). lvfetallic plates or  Moisture Diffusion and
occasionally vegetable materials such as        Water Content
straw can be also found as roofing in
historic buildings. Usually, during             The need to repair moisture damage is
refurbishment, one or more insulating           secondary only to structural damage
layers or impermeable membrane are              when preserving ancient buildings. The
added between the covering and the              presence of water in a structure and its
supporting structure to prevent                 changes of state (solid, liquid, vapor) arc
infiltration and to reduce heat losses.         responsible for damage to the building, it~
                                                content~ and its inhabitants. The same
Examples of Structures in Vaults                materials can be damaged differently
                                                depending on environmental conditions
and Roofs                                       and especially on the amount of water in
                                                the wall. Concurrent causes are biological
Another example is the vault of San             and chemical or are linked to pollution.
rvlichele in Cambianica, Bergamo, Italy.
The thermogram, shown in Fig. 35 was                The knowledge of the water content
recorded after 1 h of convective heating        within walls is fundamental to the decay
(4000 W over 2500 m'). The ashlars of the       analysis. In cold climactic conditions it is
masonry are well defined. Moreover,             usually a key factor when temperatures
cracking at the base of the vault is            stay below zero for several months.M• In
detectable; three areas; in the white           t110se cases, the water volume grows in
squares are cooler because of moisture          tile form of frost and generates strength
caused by rain infiltration from the roof       ·within the porous wall materials,
(24 October 1997; temperature before the        therefore generating cracks in the
                                                structure especially during long and cold
heating 284 K= 11 oc = 52 °Fi relative          winters. In temperate climates during
                                                winter, the thermal inertia due to the
humidity 44 percent; average temperature        thickness of the ancient walls (more than
                                                0.50 m), prevents frost inside the wall.
286 K = 13 "C =55 "F; background                Damage is limited to the surface, 0.03 or
temperature 281 K =8 "C =46 "F).                0.04 m 0 or 2 in.} deep, because of
                                                continual cycles of freezing and thawing.
    The irregular texture due to the reeds
beneath the frescoed parget of the vaults           An additional issue related to moisture
is recognizable in the infrared                 damages of the surfaces is the water
thermogram of Fig. 36, taken at Villa           transition between the wall and the
Arconati. The darker areas indicate some        ~urrounding environment because of
infiltration of water. Very favorable           evaporation and dew. The objective of
environmental conditions let these images
be recorded without applying any                 FIGURE 36. Thermography of vaults of Villa
artificial heating (23 June 1997, air           Arconati Castellazzo di Bollate, Italy. Beneath
                                                 frescoed parget of vaults there are reeds
temperature 290.8 K =17.6 "C = 63.7 "F,          nailed on timber centering, 13 june 1997.
                                                 Air temperature 290.8 K (17.6 oc = 63.7 oF),
relative humidity 36 percent).                   relative humidity 36 percent.
    In a passive test on 22 November 1995,
the timber centering of the vault of
Palazzo Peloso-Cepolla, Albenga, Italy, was
detectable in a thermogram as warmer
areas.
    In Oratorio Suardi, the infrared images
of the roof revealed different material
covering the ceiling after 2 h of heating
 by convection at 3500 W over 1500 m3
 (8 October 1999).
FIGURE 35. Ashlars of masonry shown by
thermography of dome vault of San Michele
in Cambianica, Bergamo, Italy, 24 October
1997 after 1 h of convection heating. Air
temperature 284 K(11 "C = 52 "F), relative
humidity 44 percent.
Infrastructure and Conservation Applications of Infrared and Thermal Testing 637
moisture analysis is to find out the         Leakage and Infiltration
sources of water and to plan the correct
intervention to dry the walls and save       Infiltration of rain or snow may occur
their surfaces. The main paths of ·water     where the roof is not well maintained.
coming into building materials are           Typical stains may be found on the
(1) from the ground (capillary rising),      ceilings (or vaults) on the upper floor. In
(2) by condensation from the air and         case of wide infiltration even the walls
(3) from infiltration because of broken      nearby may absorb much more water
piping or guttering or leakage from the      than the floor itself (depending on the
roof.                                        thickness and the absorption
                                             characteristics of the walls).
Capillary Rising
                                                It is interesting to observe the
Most ancient buildings are affected by the   correlation of water staining on the
presence of moisture due to the              surface and the actual water content of
absorption of water from the ground. The     each point. Such a visual indication is
presence of water in the ground depends      important but sometimes misle<Jding. In
on the following: shallow groundwater;       fact, it appears suddenly when moisture
impermeable ground layers (such as clay)     concentrates but remains after the surface
that prevent rain drainage; proximity of     dries out.
rivers, sea, lakes and channels; proximity
of sewage and drainage system failures;         Broken pipes cause localized high water
slope of the ground; inadequate (highly      concentration: the wall materials soon get
porous, lacking waterproof layers or         saturated. Although in many cases the
broken) pavement near the building.          extent of the infiltration will not appear
                                             visually and also not close to the failure,
   The bases of the walls are the typical    infrared images show the extent of its
areas affected by rising damp. It does not   spread. Careful analysis is needed.
depend very much on seasonal thermal
changes. Nevertheless, the water content     Detection of Moisture in
and its distribution inside the wall may     Buildings by
vary depending on the particular source      Thermography
supplying the underground moisten
volume.                                      Thermography for the moisture
                                             monitoring of buildings is well
   The main characteristic is an almost      documented in the Jiterature.67-n9
horizontal frontier, bending higher from
the ground at the corners or where the       Different approaches have been proposed,
masonry is thicker. The height of the        imposing a transient thermal state or
damp areas may vary during the year. Salt    considering almost stationary the
efflorescence is frequently generated at     boundary conditions. Active or passive
the border of the damp areas.                techniques have been based on the
                                             changing of thermal parameters70 or using
Water Condensation                           dependency of optical surface properties
                                             from moistureJl
\'\1here relative humidity is high and
temperature drops, vapor condenses on           Generally speaking, the choice of the
the colder surfaces. The condensation risk   right time to perform the test is very
depends on a high rate of environmental      critical, because various phenomena are
relative humidity and cold surfaces; on      activated by the moisture accumulation.
evaporating surfaces, for instance due to a  In fact, buildings are subjected to slow
crowd in the rooms; and on inadequate        varying but no;sy boundary conditions
ventilation, for instance lack of window     and different heat fluxes may interact
frm'nes.                                     with each other in destructive or additive
                                             effects. The building envelope exchanges
   Any part of the wall may be affected by   energy with the surrounding environment
dew, depending on the temperature of the     by convection and radiation. In addition,
wall. Thermal bridges are preferred areas.   a significant amount of energy could be
But corners are often subjected to           associated with changes of phases of water
condensation because of limited air speed.   on the building surface, Hence, a heat and
Condensation may disappear within a          mass transfer is activated through the
short space of time and occurs               wholE' building envelope, driven by
periodically (in the same season).           transient and quasiperiodic boundary
                                             conditions.
   The condensation areas often
correspond to stains or mold. The dew           The mathematical modeling of the
point may be monitored to measure the        thermal problem is very complicat<:'d
wall temperature and relative humidity of    because elementary fluxes are combined
the air.                                     with each other. Furthermore, the liquid
                                             and vapor phases are in equilibrium
                                             inside porous material and the phase
638 Infrared and Thermal Testing
changes continuously inside the wall and      Of course, using a passive procedure only
on its surfaces. As a consequence, a          the environment acts on the surface.
moisture increasing generates warmer or
colder areas than normal one, depending           Finally, the following problems may hl'
on the boundary conditions or
gl2'ometrical aspects. A simplified solution  anticipated:
is then to be searched, trying to perform
the measurement when transient thermal          I. A preliminary scanning of all the
state is more understandable.                      surface of the wall makes it possible to
                                                  set camera parameters and to identi~·y
   The final target is to recover from the        the most evident anomalies; a set ot
thermogram information about the water             further measurements closer to the
content of the surface. The objective of           surface yields the actual analysis.
the test could be the evaluation oft he
moisture in each point of the field of         2. Spot heating due to active elements
view. A simpler aim is the segmentation            like hot pipelines or electric cables
of the ·whole surface in a few zones of            may disturb the test.
more or less homogeneous ".;ater content.
The latter objective is realistic and          3. Dming an active procedure, the
informative. In fact, knowing the water           presence of plaster delaminations and
distribution in space, a very few                 stains or colored parts may affect
measurements made with other methods               results.
could be enough. In addition, the wet
areas' location and shapes and their           4. The winter heating aCtive inside the
changes in time are very indicative of the         building could prevent a correct
source of the water. As an example, an             moisture detection of the wall.
almost horizontal line delimits the wet
zones due to capillary rising. Another key      5. The heating tends to dry the wall
point is the correlation in time between           surface, masking the moisture map in
moistened areas extension and the driving          case of low to medium water content.
phenomenon. This approach spoils ~he_
imaging features of thermography, hnkmg         6. Thermal bridges and thinner walls, the
thermograms to quantitative measures of            imperfect connection between walls,
thennohygrometric conditions. In such a            the presence of windows and doors
way, the continuous monitoring in space            close to the investigated area -all
given by thermography may be correlated            these may cause false alarms.
with the almost continuous data logging
in time of conventional sensors.              Surface Evaporation Flux
    Infrared thermography can be used for     Thermography allows estimation of t11e
moisture evaluation as an indirect            evaporation rate of a wall. This technique
technique72 starting from the temperature     is based on the high value of the latent
map.                                          heat of water. Each gram of water
    An approach in applying                   evaporating absorbs 2500 J and cools the
thermography is to follow qualitatively
the n:10isture distribution due to the        surface ver}' effectively. Therefore, moist
cooling effect of water evaporation.73        areas are colder than dry ones, assuming
Another approach is based on water's high     the same boundary conditions. The
thermal capacity revealed during transient    appearance of the phenomenon depends
thermal tests?4•7s                            on air temperature and relative humidity
                                              levels. The flux cp of the evaporating watt'r
    A second level is the quantitative        is given by Fick's law (Eq. 2) and is
estimation of water content using the         proportional to the water concentration
surface temperature distribution in space     gradient between the porous surface and
and time or additional measurements           the air outside the boundary layer (free
with alternative techniques on selected       air):
points. Notice that measuring the water
content of a \Vall by thermography alone      (2) <I>       t.C
appears practically impossible and an
estimation of the moisture in a shallow                -/)-
layer is the maximum achievable result.
                                                            t.z
    Even if an absolute evaluation of
moisture is possible76•77 a relative             At equilibrium, the moist material
approach is much more used. In this case,     supplies the water flux, hence <I> is related
the investigation of damp areas is based      mainly to the porosity of the material and
on the comparison of the thermal              its soluble salts content. The diffusion
behavior of dry areas with damp ones.         coefficient D depends on properties of the
Therefore, in the same thermogram there       vapor and is a function oft he constant R,
can be both circumstances, assuming the       temperature T and the average molecular
same heating and boundary conditions.         mobility u of vapor. The measure of <1)
                                              could be obtained, at a specific point,
                                              measuring the relative humidity (lUI) of
                                              the free air and very close the wall
                                              surface. The thickness of the boundary
                                              layer d, where molecular migration takes
                                              plac<:, approximates l1z. i\·lolar
                                              concentration (.'of water can be expressed
                                              as a function of the relative humidity of
Infrastructure and Conservation Applications of Infrared and Thermal Testing 639
the air. Therefore, the flux Q> can be          2. Environmental conditions should
expressed directly in terms of the relative        have a medium to high transpiration
humidity gradient (RJ-!1 to RHa) as follows:       (relative humidity lower then. XO
                                                   percent and air tt>mperature not below
(3)
                                                  279 K !6 <>c = 43 oF] in the air surface
where: C~Jt is the molar concentration of
water at saturation.                               boundary layer). Note that adverse
                                                   microclimatic conditions may prevent
   Of course, values of ct> are affected hy        a reliable testing. Most E'IWironmental
the convective exchange with the                   circumstances require increasing the
ambient described by the term uRT d- 1•            level of transpiration. During outdoor
This is usually difficult to be determined         surveys, the weather can change
in real tests. In the laboratory, cf> was          quickly, so the operator has to
directly obtained by weighing the tested           measure temperature and relative
sample. In such a way, an evaluation of            humidity periodically. The indoor
parameters affecting the evaporation               microclimate may vary too hut in a
phenomenon in natural convection has               longer time scale than that needed for
been ohtained?f~                                   the scanning. Hence relative humidity
                                                   and air temperature can be measured
Testing Procedure                                  only at the beginning of the test, after
                                                   it and at any significant change of the
A preliminary scanning from a point as             setting.
far from the masonry as possible makes it
possible to set the camera parameters and       3. Normally, the infrared camera is set at
to detect the anomalies in a few images,           the maximum sensitivity. In fact, the
covering the whole surface. Further                cooling effect of evaporation gives
measurements closer to the surface permit          stnall differences of temperature. The
more precise analysis for small                    manual setting of the readout range is
discontinuities.                                   preferable, even if some detail of the
                                                   infrared image can he out of scale.
   The classification of the surface in            Furthermore, the average function h
more or less homogeneous areas is                  usefully applied in case of noisy
achieved in almost steady thermal state            images because of smooth temperature
because of natural boundary conditions,            variations.
according to the following steps.
                                                4. The choosing of the fidd of view
  1. Collect the available description and         depends on the lens and on the
     plans of the building; the particular         distance. Normally, a double scale
     building technology; information              taking is suggested.
    about the masonry, finishing and all
     material used; and the survey of the       5. The identification of the damp areas is
     present state of damage due to                achieved by comparing the
     moisture.                                     temperatures of the dry surfaces to
                                                   those of the moist surfaces. In the case
  2. A suitable geometrical drawing of the         of wide surface the investigation may
     interior and exterior of the building at      require the shooting of numerous
     adequate scale represents the template        thermograms, which will be composed
     on ·which the visual state,                   into a composite image.
     thermograms and others ancillary data
     will be superimposed.                     Thermograms may be assembled into
                                               composite images through the following
  3. The actual boundary conditions and        process.
     particularly the temperature, relative
     humidity and solar irradiation have        1. Some removable marks are placed on
     been recorded for at least 24 h before         the surface to identify the position of
     the thermogram is recorded.                    the thermogram borders.
Boundary conditions arc controlled as           2.The operator has to record also the
follows.                                            pattern of the shots during the
                                                    inspection.
  1. The inspected surface has to be kept
     out of direct heating for about 12 h       3. The position of the camera has to be
     before the scanning, because different         as perpendicular as possible to the
     absorption coefficients of the surface         surface.
     cause effects contrasting the cooling
     due to the evaporation.                     4. For optimum matching, correction of
                                                    the perspectivt' distortion is needed.
                                                 S. lf a selected palette is permanently
                                                    associated to the thermogram by the
                                                    digital image format, it has to be
                                                    recorded also in grayscale. Additional
                                                    palettes can be used in the final
                                                    editing of the images.
640 Infrared and Thermal Testing
Effects of Moisture on Thermal                 (8) T  2 (l {L
Parameters
                                                       <' \ rr
Thermal properties mainly influenced by
                                               where Q is absorbed energy (watt) and I is
moisture are heat capacity c and thermal       time (second).
conductivity k. \Vater fills pores inside         Assuming that effusivity of a moist
material making it heavier and more            material is £'(H') = l1+w(c1Jc)]-0·\ the finJ:I
thermally inertial due to its high specific    equation for determining moisture
heat (cw = 4181.1 }kg--l.K-1), compared
\Vith that of dry building materials           content w was proposed in the following
(c.,= 800 + 900 ]-kg-l·K-1) and its
considerable density (p = 1000 kg·nr~).        form:
lvfoisture w is specified on dry specimen      (9)
base:                                             The accuracy in moisture measurement
                                               by Eq. 9 depends mostly on the ilccmacy
(4) w                                          in determining absorbed energy. To loosen
                                               this problem, a reference technique has
where Mw is masses of water and Md is dry      been introduced.76 Adopting this
specimen. For physically dear rea~ons:         approach, Eq. 10 gives the water content
                                               value for the moistened material:
(5) M(w)
(6) c(w) M(w)
(7) C(W) =                                     where '/~is the temperature from the
                                               surface of the reference area.
    The variation of thermal conductivity
with moisture is a much more complex              Equation 10 assumes that conductivity
matter, not yet fully understood, and          does not vary significantly with water
most of the proposed models are                content. Finally, here the ratio of
semiempirical79 Considering that the           absorptivity coefficients of the surface in
thermal conductivity of water,                 the appropriate spectral range (al\"2 u,fz) is
kw = 0.58 f\'\'·m-1·K-1], is much higher       introduced.
than the conductivity of moist air in the
pores, ka = 0.026 IW·m-l.K-1], an increase        If the impinging one-dimensional heat
of conductivity ·with water content is to      flux is described by a harmonic function,
be expected. As a consequence, the effect      as periodic natural sources, then the
of moisture on conductivity is an              moisture influences the amplitude and
informative parameter. Because heat can        shape of surface temperature response.
be transported both by conduction and          Then, the temperature patterns can he
water flow, however, the exploitation of       inverted <IS well applying an iterative,
the thermal conductivity to detect moist       nonlinear least squares technique59
zones is quite ambiguous.
                                               Testing Procedure (Active and
   The dependence of thermal inertia or        Relative)
effusivity (e = \1(kc) versus moisture is
straightforward and makes this parameter       An active approach is used in this case but
attractive for the moisture monitoring.        in some cases solar radiation is sufficient.
Building parts of larger thickness could be    Artificial heat sources are normally limited
considered as semiinfinite bodies and heat     to a selected area.
flux one-dimensional. As a result, the
corresponding mathematical solutions              The succeeding steps are to be
                                               substituted to the previous procedure for
become simpler than those for a slab.          the surface classification:
Such a solution a1Iows solving the inverse      1. Apply a suitable heating, about
problem in an explicit form. On the other           I kW·nr2 (-320 BTUrch-1·ft-2 )
hand, this approach requires an active             starting just after the first thermogram
stimulation of the surface, reducing the           has been taken,
tested areas if an artificial source is used.
In the adiabatic case, the surface              2. Record a sequence of thermograms for
temperature is given in a very simple              at least 15 min using if possible a
form, after a step heating:                        logarithmic time scale (if not possible
                                                   use a constant grabbing frequency
                                                   according to the capJ:bilities of tlw
                                                   system).
                                                :1. Process the data using Eq. 10.
               Infrastructure and Conservation Applications of Infrared and Thermal Testing 641
Examples of Detection of Damp                                    the eastern side (air temperature
              Areas by Evaporative Flux                                        296 K = 23 oc = 73 oF, relative humidity
                                                                               67 percent). Gtavimetric tests confirmed
              The thermal hygrometrical status of the                          the presence of water. The water content
              masonry of the Oratorio della Guardia di                         resulted 11.6 percent on bricks at 0.50 m
              Satta, Corsica, Italy, was measured from                         20 in.) from the ground; 7.2 percent on
              1995 to 1997 (see Fig. 37a).                                     brick at 0.98 m (39 in.) in area 1 and
              Thermographic monitoring '''as                                   3. 6 percent in area 2.
              performed to study the dependence on
              climactic changes. Periodically,                                    The infrared images of Fig. 39 have
              gravimetric tests verified the water                             been taken at Sant' Massimo Church,
              content and thermographic results.                               Sedriano, Italy. It shows the distribution
              Gravimetry measures quantitative water                           of rising damp at the base of the facade
              content as a percentage of weight. The                           wall. Here, the damp areas appear warmer
              building has structural masonry and lime                         during the night, after 12 h of solar
              mortar. In Fig. 37b is shown an infrared                         irradiation (15 May 2000, air temperature
              image (21 November 1995, air
              temperature 280 K = 7 oc = 45 °F, relative                       290 K = 17 oc = 63 oF, 85 percent relative
              humidity 57 percent, clear sky). Smooth
              gradients found on thermal images                                humidity).
              indicate a rather homogeneous moisture                              Thermograms recorded on 21 March
              distribution although gravimetric results
              verified a high water content. The high                          1995 show the visual state of the western
              humidity percent and low air temperature                         side of Santa lv1argherita church without
              mitigate against a sharp separation of wet                       active heating of the surface. The base of
              from dry areas. In fact, under these                             the masonry appears colder and wet.
              conditions evaporation is at the                                 Gravimetric tests confirmed the higher
              minimum. On the contrary, passive                                'i\'ater content in that zone of the wall.
              thermography detected rising damp on
              16June 1997.                                                        The picture of Hg. 40a shows Sant'
                                                                               Abbondio Cloister and the thermograms
                 Figure 37c shows the thermograms of                           of Hgs. 40h and 40c indicate the rising
              the facade. A colder area is evident in the                      damp affecting the base of the wall. The
              lower part of the facade. Notice that the                        damp area expands near the corner with
              growing vegetation partially covers the                          the north side {right side) following the
              left side of the door (area 2). 1n addition,                     shape of the decay of the p(trget.
              Fig. 38 shows the infrared image shot on                         Thermograms ·were acquired by using the
                                                                               passive technique. In this case, the high
                                                                               correlation between the visual and
                                                                               temperature pattern corresponds to an
FIGURE 37.  Facade of Oratory of Gu.ard!a di           Sotto, Corsica, Italy:  (a) visible light   photog~aph;    0(b) therm~gram o~ f.ar;ade  does
            any moisture accumulation (21              November 1995, a1r      ~emperature 28
not reveal                                                                                        0 K := 7 C =:,  45 F, r;lat1ve ~urn1d1tX .
57 percent, clear sky); (c) passive thermogram (16 june 1997, a1r temperature 296 K ~ 23 C ~ 73 F, relattve humtdtty
67 percent).
(a) (b) (c)
legend
  1. Colder, moister areas in lower part of fa~ade.
  2. Vegetation partially covering left side of door.
actual moisture distribution as confirmed                     FIGURE 40. Sant'Abbondio cloister, Cremona,
by gravimetric measurements (20 june                          Italy, 20 June 1995: (a) visible light
1999, air temperature 298 K ~ 25 'C ~ 77                      photograph; (b and c) passive thermograms
0 1~ relative humidity 40 percent).                           showing rising damp in" masonry. Air
                                                              temperature 298 K (25 'C ~ 77 'F), relative
    In the case of Corte Castiglioni Manor,                   humidity 65 percent.
Mantova, Italy, the building is made of
structural masonry, bricks and lime                           (a)
mortar.!:!° Chemical physical analyses
varied greatly because of the different
kinds of mortars and bricks used.
Furthermore, their absorption coefficients
vary in a few centimeter square (a kw
square inches) of the surface.
Nevertheless, Fig. 41 acquired according
FIGURE 38. Passive thermography indicates
rising damp on lower part of masonry in
oratory of Guardia di Sotto, Corsica, Italy,
16 June 1997. Airtemperature 296 K
(23 'C ~ 73 'f), relative humidity
67 percent.
                                                              (b)
legend
  1. Colder, moister areas in lower part of fa~ade.
  2. Warmer and drier masonry.
FIGURE 39. Image composed of infrared thermograms shows       (c)
distribution of rising damp at base of facade of San Massimo
Church, Sedriano, Italy, 15 May 2000. Damp areas appear
warmer at night, after 12 h of solar irradiation. Air
temperature 290 K (17 'C ~ 63 'f), 85 percent relative
humidity.
Infrastructure and Conservation Applications of Infrared and Thermal Testing 643
to a passive procedure clearly indicates                       thermography in Fig. 43b allow~ locating
rising damp as colder areas 1 and 2 at the                     the distribution of damp an•as. Causes
base of the wall (17 june 1998, air                            have been identified both in rising damp
temperature 298 K = 25 "C::::: 77 "F, relative                 from the pavement and the local leakage
humidity 74 percent). The three strips                         of a pipe (17 June 1999, air temperature
detectable by thermography correspond to                       299 K::: 2() "C::: 79 "g relative ·humidity
the average water content decreasing with                      54.3 percent).
height.                                                        limitations of Infrared
    In Santa Maria in Cantuello (21 :1\•farch                  Thermography
1997), thermography was used to locate                         Constraints on Field Applications
damp areas. The thermogram was
recorded using the passive technique on                        After a period of laboratory
one side of the building. ~vfoisture ·was due                  experimentation and theoretical
to the leakage of an external basin.                           modeling, the application of infrared
                                                               thermography has been optimized in the
   The visual state of the sacristy of Santa                   field. The effectiveness of tile analyzed
Maria del Lavello is shown in Fig. 42a,                        techniques and influences of some
where the state of decay of the plaster is                     conditions in real tests are discussed
evident. The actual extension of the damp                      below.
area is shown in the thermogram of
Fig. 42b. Notice that the moist surface (at                    FIGURE 42. Santa Maria del Lavello1 Bergamo,
the right side of the basin) is more                           Italy, 19 March 1998: (a) visible light
extended than the ruined one (19 March                         photograph of sacristy; (b) demarcated
1998, air temperature 287 K = 14 "C =57                        damp area larger than damaged parget
"l~ relative humidity 38.8 percen.t).                          zone in sacristy. Air temperature 287 K (14
                                                               oc = 57 oF), relative humidity 38.8 percent.
   In Addolorata Church, Gessate, Italy
(20 March 1996), the visual state of the                        (a)
interior plaster did not show any mark of
decay but infrared thermography revealed
the extent of recent leakage from the roof
on one side of the vault.
    During the renovation of the plaster at
lstituto Musicale Donizetti1 Bergamo,
Italy, two sets of tests were performed to
localize the cause of infiltration. In
Fig. 43a it is shown the state of decay of
the plaster in a key zone near the down
pipe. The diffused damage prevents
identification of any indication of direct
infiltration. Nevertheless, infrared
FIGURE 41. Thermography of facade of Corte
Castiglioni, Mantova, Italy, 17 June 1998.
Three bands correspond to water content
decreasing with height. Air temperature
298 K (25 oc = 77 oF), relative humidity
74 percent.
                                                               (b)
                              legend
                                 A. Relatively dry.
                                 B. Moderately cool and damp.
                                C. Cold and damp.
644 Infrared and Thermal Testing
In situ applications require the            temperature change. On the contrary, the
procedure to be as fast as possible, to keep   passive approach works at steady state.
constant the condition of the scanning
and to reduce the costs. Passive               SURFACE CoNDITION. Oftt>n hhtorical
techniques have the advantage of being         buildings lt~ck homogeneous surfaces,
much more productive and easily applied        either in color or material. Difference~ of
to surfaces larger than 10m2 (108 ft2). On     heating absorption affect the thermal
the contrary, using artificiJl sources only a  ;malysis, causing false alarms and altering
small area can be homogeneously heated.        the thermal response of the structure.
Moreover, effective radiating requires a       Ptlfticult~rl)' in the case of frescoes and
powerful power supply (more than :1 k\IV).     paintings the artificial heating (for
The sources must be supported close to         instance by lighting) increases such a
the surface with expensive scaffolds. As a     difference. Furthermore, salt deposits
consequence, it is necessary to scan the       modify reflectance and emissivity. Soluble
whole surface in smaller areas of 1 to 2 m 2   salts arc ever present in a surface d(lmag(•d
(1 0 to 22 ft2). Additional time is needed     by damp. (Jenerally, deposit of salts
for the transient analysis. In fact, a         decreases the emissivity, causing an
sequence of thermograms is recorded and        apparent temperature lower than true.
each pixel processed in its turn. The only
advantage of the active procedure is the       THERMOGRAPHY SETIING. Usually
reduced dependence on environmental            thermography is applied in the
conditions. Hence, the active approach         preliminary phase, to obtain the
can be applied also in case of presence of     information necessary to plan the
other (not removable) sources of heating,      intervention. In this phase the yard of
because the estimation is based on             conservation is not settled yet, so the cost
                                               of the scaffolding could inflate the cost of
FIGURE 43. lstituto Musicale Donizetti         the project. Also in the maintenance
Bergamo, Italy, 17 june 1999: (a) visible      program, where thermography is applied
light photograph of plaster of northern side;  as ·well, the cost of the scaffolding or
(b) thermogram of plaster indicating cooler,   pickup elevator could make active
damp area (darker zone) due to pipe            thermography inconvenient. Qualitative
leakage. Air temperature 299 K (26 'C =        analysis may help in such a situation.
79 'F), relative humidity 54.3 percent.
(a)                                            HEATING. Artificial heating must be applied
                                               as perpendicularly to the smface and as
(b)                                            diffusely as possible. In cases of heating
                                               from long distances or from the bottom of
                                               elevations, artificial heating could be very
                                               uneven. An autonomous power supply
                                               could be ne<.:essary. In many cases the
                                               temperature increase must be limited to
                                               only a few degrees, because of the
                                               preciousness of the surfaces.
                                                   The healing of aU the layers of thl'
                                               structure is hardly achievable: the low
                                               thermal diffusivity and the wideness of a
                                               building requires long and powerful
                                               heating. The direction of the heat flux
                                               should be one-directional but the
                                               discontinuities of the surface modify the
                                               propagation of the heat inside the
                                               structures.
                                               VISUAL ANALYSIS. The Visible damage of the
                                               materials docs not correspond to the
                                               actual state of the masonry. For example
                                               cracks in the co(lting, in the plasters and
                                               in the external layers sometimes can be
                                               smaller than inside damage and traces of
                                               damp. Stains, salt deposits, increases of
                                               porosity, delaminating of plasters, voi{h
                                               and other kinds of damage may occur
                                               even if water has dried. Furthermore, the
                                               damage of the surface often modifies
                                               locally the imposed heat flux,
                                               complicating the diagnmh. Neverthek~~,
                                               the availability of the picture of the
                                               surf<Ke is extremely useful.
Infrastructure and Conservation Applications of Infrared and Thermal Testing 645
Integration with Other Testing
                 Techniques
                     Thermography allows moisture
                     distribution in the surface to be mapped.
                     The results are qualitative only and are
                     restricted to the surface. There is no easy
                     correlation between the temperature
                    measured and the '"later content.
                         The integration with other quantitative
                     techniques (for example, gravimetric
                     testing) is suggested. A moisture map
                     obtained nondestructively by
                     thermography makes it possible to
                     decrease the number of samples to collect
                     without affecting the reliability of the
                        tests.Hl
                        A variant of the active heating involves
                     microwave radiation.82 In this case, the
                     water selectively absorbs the energy. The
                    drawback of this technique is· the more
                    complex managing of the heat source.
                        The measures could be repeated on the
                     same wall in different periods of the year.
                     Further validation by gravimetry also
                     permits the paths of the water coming
                    into the wall from the sources to be surely
                    determined.
                        The tradeoff beh\'een a complete
                    refurbishment and a detailed but
                    circumscribed diagnosis push toward the
                    latter- particularly for historical
                    buildings where the cultural heritage must
                    be preserved.
646 Infrared and Thermal Testing
PART 6. Infrared and Thermal Testing for
Conservation of Fine Art83
The scientific examination of art can he        1. For inspection of the surface,
divided into two basic categories:                 conservators use ultraviolet fluorescent
destructive and nondestructive. Among              photography. Ultraviolet light will
the destructive methods are those that             cause old varnish to fluoresce.
involve sampling, taking a small slice or          Therefore, if portions of the protective
scraping for closer scrutiny, perhaps by           varnish do not fluoresce under
microscopy or thermoluminescence. A                ultraviolet light or if they appear
conservator's goal, however, is to carefully       darker than the surrounding area, it
maintain valuable works of art and to              can be assumed that relatively recent
slow the inevitable deterioration.                 changes have been ma.de to the
Nondestructive testing is an invaluable            surface. Unfortunately, as the newer
tool to this end. The art historian also           varnish begins to age, it too will begin
finds nondestructive testing an important          to fluoresce and then the conservator
asset in the pursuit of information of             has to use another method to look
historical value - for example, about              under the surface.
creative techniques of a particular artist or
a certain period of art.                        2. x.radiography records the distribution
                                                   of pigments that have a high
Three-Dimensional Art                              absorption coefficient for X-rays. The
                                                   X-rays used in X·radiography will
Three-dimensional art includes                     completely penetrate a canvas.
architecture and sculpture and infrared            However, if pigments such as white
thermography finds applications in these           lead or vermillion with high
fields. Nondestructive testing methods             absorption coefficients are present,tiH
applied in building maintenance and                their distribution will be indicated on
restoration is in many cases the same as           a photographic plate placed behind
that used for art conservation. Such               the canvas.
applications of thermography are
represented in the literature.s6,H4·87          3. A third part of the electromagnetic
Conservation of frescoes, paint on plaster,        spectrum used in the nondestructive
is a special case of interest to both              testing of art is infrared.
building and art conservationists.H77
Nondestructive testing technologies also       Infrared Techniques
find applications in archaeology and
anthropology. The balance of the present       Infrared waves will penetrate different
discussion focuses on painting on canvas.      pigments with varying effectiveness. The
                                               degree of transparency depends chiefly on
Two-Dimensional Art                            wavelength (the longer the wave, the
                                               greater the degree of transparency),
As part of the creative evolution of a         thickness of the paint film and reflection
painting, an artist will often change his or   or absorption properties of the pigment.~'W
her mind during composition and paint          Carbon black is the most absorptive;
over the original idea. The artist may even    white is the most reflective. Infrared film,
paint over one of his earlier works if the     used in infrared photography, is receptive
artist considers the painting less             only to the portion of the spectrum with
important than the need for another            wavelengths up to about 900 nm. At
canvas. A change can also be made by           those wavelengths, not all colors will
someone other than the original artist.        allow infrared penetration with the same
From the art historian's point of view,        facility. Green and blue, for instance, have
these underpaintings can afford insight        absorptive qualities very similar to those
into artistic development or the               of black and may !Je opaque whereas
techniques used to achieve a particular        brown and red generally reflect about the
effect. They can also help determine the       same as white.YO
artist or the authenticity of a painting.
                                                  The typical arrangement for infrared
    Three of the methods often used in the     examination has a source of visible and
inspection of two·dimensional art use          infrared radiation, an object to he
electromagnetic energy. Each of the three      examined and an infran.·d recording
wave types is used to survey a different       device or camera with an infrared filler to
layer of a painting.                           exclude all but the infrared waves.
Infrastructure and Conservation Applications of Infrared and Thermal Testing 647
Photographic studio lights are used in a       painting. This has been and still is the
 darkened room. The lights are controlled        most widely used procedure for
 by a rheostat that dims them to the             maintaining a permanent record.
 infrared range.91 The radiation produced
  at this point is very largely infrared with    Renaissance Netherlandish
  little of the visible portion of the light     Art
 spectrum. This source is aimed at the
 painting. \'\1!1en infrared waves reach the     Flemish artists of the fifteenth and
 painting, they will penetrate the surface       sixteenth centuries were very consistent
 and the recording device takes the              in their mettwd of producing paintings.
 ensuing picture. Years of grime or cloudy,      First, the artist covered an oak panel with
 darkened varnish are not obstacles: they        a ·white preparatory surface, or ground,
 are easily penetrated by infrared radiation.    that was a mixture of chalk and animal
 Contrasting reflected waves are collected       glue. The next step was the preliminary
 by the infrared camera to produce a             sketch made with carbon black or charred
 record of the paint layers beneath the          bone mixed with water. These two
 surface.                                        elements make this period of art
                                                 amenable to inspection with the infrared
    Infrared pJ1otography using a 35 mm          reflectographic technique. The white
                                                 ground ensures that the infrared rays not
 camera and infrared film has been used          absorbed by the black portions of the
 since the late 1950s at conservation            sketch are reflected back to the camera.
 laboratories. One such laboratory is the        The carbon black sketch produces a very
 Intcrmuseum Conservation Association,           visible contrast against the white ground.
 Oberlin, Ohio. This facility was
                                                    Although best results are obtained with
 established in 1952 as a cooperative            Netherlandish panel paintings, French,
 conservation lab. Some of the typical           German and Italian art from the same
 examination procedures used in the             period will sometimes give good re!iults
 Oberlin lab are illustrated by the infrared    although certainly not with the same
 photographs of Charles Baum's Bo}' with        frequency as the Flemish art.
 Still Life, owned by the llutler Institute of
 American Art and once attributed to                The Paintings Conservation
 another artist, Severin Roesen. Figure 44a      Department. of the Metropolitan J\Juseum
shows a photograph of the portrait using        of Art, New York, in a project conducted
normal, visible light. No images other          by 1vfaryan Ainsworth, examined the
 than that of the title are apparent. An        1:aintings of joos van Cleve, an early
 infrared photograph of the same painting       SIXteenth century Delgian artist. None of
shows a sketch, or underdrawing, of the         his drawings on paper were thought to be
face of the young boy and the faint image       still in existence. Because the
of a young woman slightly above and to          underdrawings of his paintings were so
the right (Fig. 44b). X-radiography (Fig.       much easier to discern using
44c) reveals a third image and appears to       reflectography, van Cleve's graphic
be that of an older man. In addition            vocabulary became apparent. \•Vith this
                                                new acquisition, Ainsworth was able to
darker areas slightly below center and          attribute to van Cleve previously
                                                unidentified drawings on paper.
lower left indicate some restoration.
    The newest addition to infrared                 An interesting note in infrared
                                                investigation of this period is that it
examination is infrared reflectography,         afforded insight into ·workshop
developed by ].H.]. ~'an Asperen de Boer        techniques of reproduction. If a painting
specifically for fifteenth and sixteenth        exhibits underdrawings or changes in
century Netherlandish panel paintings.          composition, it is probably a prototype
This system uses a vidicon camera to            and attributable to a single artist.
capture the infrared image and transmit it      However1 artists often copied their most
to a black-and-'white monitor. The vidicon      popula~ paintings. The work of copying
tube is receptive to the entire infrared        these pieces was delegated to other artists.
spectrum and the blues and greens               One copying technique, called pouncius,
become transparent to the-longer                uses a line drawing on paper pierced
wavelengths. An excluding filter, opaque        along the outlines. This paper pattern was
to wavelengths belmv about 0.9 pm,              placed over a canvas and black carbon
admits infrared \Vaves up to 2 pm.              powder was rubbed through the holes to
                                                produce a matching image on the canvas
    Reflectograms are the photographic          beneath. This image was then painted in
record of infrared refJectography.              to match the original. Visible in
Typically, to obtain a detailed overall         reflectography, these tiny dots of carlJOil
image of a painting, the vidicon camera is      indicate a copy and therefore worksllOp
aimed at part of the canvas and the irnage      production.
displayed on the monitor is
photographed. This process is repeated
until the entire canvas has been captured
on film. These discrete photographs are
then carefully arranged in their correct
sequence to produce a whole image of the
648 Infrared and Thermal Testing
Vermeer                                      defined images of undersketches. Though
                                             his paintings do not contain the defined
Arthur K. Wheelock, Jr., in research as a
National Endowment for the Arts Fellow,      underdrawing used in earlier centuries,
used reflectography as a n1ethod             reflectography has revealed roughly
complementary to X-radiography in            blocked-in forms. View of IJelft, known for
relating the painting techniques of          the realistic impression it gives, was
seventeenth century Flemish artist jan       examined by \o\'heelock. The painting is a
Vermeer to his distinctive style.92 Because  cityscape of the seventeenth century
Vermeer used carbon black to do his          mirrored in the still waters of a harbor.
sketching, reflectography can provide well   Using infrared and X-radiography,
                                             \-\'heelock was able to determine the
FIGURE 44. Charles Baum's Boy with Stiff Life, previously attributed to Severin Roesen: (a) visible
light photograph; (b) infrared photograph shows underdrawing sketch of boy's face and
image of young woman; (c) X·radiograph of entire canvas shows image apparently of older
man.
(a) (b)
(c)
Infrastructure and Conservation Applications of Infrared and Thermal Testing 649
changes made in the length and                 especially when they appear to be done
positioning of the reflections in the water    by someone other than the original
cmd in the outlining of the city's profile:    mtist?2
changes that Vermeer made to achieve his
realistic effect.                              Randall's Mill
   ln addition to learning more about          The painting RnndnW< Mill ( 1922-23) by
Vermeer's working techniques, \·Vheelock       American artist Victor Higgens was
attempted to determine compositional           examined by the Intermuseum
changes and also to learn more of actual       Conservation Association laboratory
physical condition - that is, abrasion,        (Hg. 4Sa).9.1 The painting was presented to
restorations or any sort of alteration of      the Snite Museum in 1982 by William
size. Some changes to a painting can
result in questions of authenticity,
FIGURE 45. Victor Higgens' Randall's Mill: (a) visible light photograph; (b) infrared reflectogram shows complex of mill buildings
and figures in foreground, including human and donkey; (c) X-radiograph shows mill of title.
(a) (b)
                                          (c)
               .....,., ;.;: .-).
650 Infrared and Thermal Testing
Harmsen and wife of Denver, Colorado,         penetration depth of the exciting
stiH on the original canvas stretcher and     radiation and (3) the sensitivity of sensors
in a frame with a brass label that reads:     used in the design of the available system.
"VICTOR HIGGENS NA [sic] I 1884-1949 I        A technique called raman spectroscopy has
RANDALL'S MILL."                              shown promise for in situ examination of
                                              fine art and archaeological artifacts_94,95
    Porter noticed that, in light from an
adjacent window, the raised surface of           An image spectroscopy system has
another painting appeared on the canvas.      been proposed and shown to be capable
After examining Randall's Mill under a        of collecting sequences of images at
raking light, the Oberlin laboratory          several wavelengths. Suitable procedures
assayed the oil*on*canvas painting with       were developed for calibrating and
various methods including X~radiography       spatia11y registering the acquired data. An
and infrared reflectography. The painting     experiment on a test panel painted with
appears as a depopulated landscape, but,      known pigments showed that image
when the painting is viewed by infrared       processing is a powerful tool for pigment
reflectography, the structure of a mill       identification when used with spot
appears along with carriages filled wHh       spectral analysis. Measurements in one
figures, horsedrawn wagons and the figure     case reveal that the methodology is valid
of a saddled donkey being led by a man        and can give additional information that
(Fig. 4Sb). Photographic images of the        is otherwise not easily extracted.96
infrared reflectography examination were
made from the black and white monitor            A sixteenth century drawing attributed
as the camera scanned various portions of     to the school of Pieter Bruegel the Elder
the canvas. With X-radiography, the           had been damaged by cleaning. Near
structure of the mill is the dominant         infrared spectroscopic imaging was used
element (Fig. 4Sc).                           to analyze the remnants. Using a
                                              combination of a charge coupled device
    A }Jainting of this description by        camera and a liquid crystal tunable filter,
Higgens was detailed in the Indianapolis      near infrared spectroscopic images (650 to
Star in 1924 but the painting                 1050 nm) ·were collected from the
subsequently disappeared. In an interview     drawing and from a test sample composed
in 1975, Helen Spiess Ferris, daughter of     of four substances with various near time
Benjaman G. Randall, a civil engineer         resolved spectra deposited on a white
who had settled in Taos, New Mexico,          board. Linear discriminant analysis and
related the tale explaining the painting      fuzzy C-means clustering were used to
beneath a painting. Randall had built t11e    analyze the data. Fuzzy C*means
mill of the title. In the vicinity of the     dustering with spectral normalization
mill, he owned a cabin that he made           routines proved an excellent data
available to the artist Higgens. Higgens      exploration technique for the test sample.
painted the picture of Randall's Mill from    Linear discriminant analysis gave
that cabin. Upon seeing the picture,          consistently clearer results than the fuzzy
Randall pronounced it 11the worst picture     C-means technique but required prior
Higgens ever painted." The statement          knowledge of the spectral properties of
must have bothered Higgens for some           the sample; fuzzy C-means analysis
time, for the overpainting is in a style      provides such spectral information. Linear
that Higgens used much later during the       discriminant analysis of the spectroscopic
1940s.                                        image located faint traces of ink residue
                                              on the drawing??
Spectroscopy
                                                 The most widely established
Spectroscopic techniques involve analysis     spectroscopic methods are not thermal.
of the spectrum of radiation emitted from     For analysis of metal objects, X-ray
a test object in order to identify the        fluorescence (XRF) spectrometry uses low
chemistry of the radiating material.          energy X-rays or gamma rays to excite
Spectroscopy can be destructive in cases      characteristic X~rays in the suhject
where the design of the inspection            material. Sensitive laboratory X-ray
hardware requires removing a sample of        fluorescence systems exist with advanced
material from the art object. However,        detectors and microelectronics, coupled
some nondestructive spectroscopic             with advanced computer technology.
designs permit the identification of          Portable units can yield precise readings
materials in situ and these are likely to be  in the laboratory and in the field?~>
more valuable for those who study or
conserve works of art. Spectroscopy is        Other Thermographic
performed at wavelengths in X-ray,            Applications
ultraviolet, visible and infrared
frequencies. The wavelength used for the      William A. Real, while a }vfellon Fellow at
test is a function of test patameters such    the Cleveland :ivfuseum of Art, Cleveland,
as (1) the material of interest, (2) the      Ohio, explorPd the broad potential of
Infrastructure and Conservation Applications of Infrared and Thermal Testing 651
ii-1frared reflectography as a research tool.
                   He inspected successfully not only
                   paintings but objects, manuscripts and
                   graphic works on paper. In addition to
                   fifteenth and sixteenth century Northern
                   European ait, Heal has examined works as
                   diverse in media and period as paintings
                   by I~rench artist j.A.D. Ingres of the late
                   eighteenth and early nineteenth century;
                   a portable carved, wooden japanese shrine
                     attributed to the Heian period (795-1185);
                   a surrealist collage by Max Ernst, jeanne
                   Hachette et Charles le Tememire (1929), on
                   paper; and an East Indian min'1ature
                     Pradywnna, Son of Krishna, mzd His Wife
                   Maya Fl}•ing through the Air (ca. 1750),
                   color on paper. Real has discovered
                   preparatory sketches under layers of
                   grime, stain and coatings on the japanese
                   shrine, indicating it is unfinished. He has
                   discovered compositional changes and
                   even hidden inscriptions in the East
                   Indian piece and improvisational changes
                   (painting over already dry paint) as well
                   as underdrawings in Ingres' Antioclws and
                       Stratonice.
                       The infrared method has continued to
                   be developed. The Jvlctropolitan Museum
                   of Art in conjunction with the
                   manufacturers of sofh\•are programming
                   have investigated a system to digitize the
                   reflectograms (images from a vidicon
                   camera) and join them in one complete1
                   permanent electronic record. The
                   portability of the system (examination
                   and recording) is such that it can be rolled
                   right into the galleries where the
                   paintings can be examined and a
                   permanent record of the results can be
                   obtained.
                       Information pertaining to technical
                   inspection of art has not always been
                   extensively published and therefore has
                   not been widely applied. Hmvever,
                   because of growing awareness by
                   museums and private collectors, the
                   advances in nondestructive test methods
                   and infrared inspection in particular have
                   found ·wide acceptance and application in
                   art conservation.
652 Infrared and Thermal Tesfmg
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658 Infrared and Thermal Testing
CHAPTER
Infrared Thermography of
     Electronic Components
                                   Bo Wallin, FUR Systems AB, Danderyd, Sweden
                                   (Parts 1 and 2)
                                   Boguslaw Wiecek, Technical University of L6dz,
                                   Institute of Electronics, L6dz, Poland (Parts 3 and 4)
PART 1. Temperature Measurement of
Electronic Components
\'\1ith the availability of a commercial        nonunifonnly in the object. Only if the
thermographic camera system in 1965,            emissivity and the reflected ambient
thermography became an important tool           temperature in each point of the object
for quality control of electronic               are known, can its true temperatures also
components. Since then thermographic            be measured.
techniques for electronics have been
developed. Noncontact measurement has              One way of making the emissivity
shown its applicability for measuring the       uniform over the object is to paint the
true temperatures on components like            object with some high emissivity paint,
printed circuit boards, hybrids and             thereby making the measurement easier.
microcircuits.l·2                               However, there are at least two good
                                                reasons for avoiding such techniques. The
   To measure true temperatures it is           first reason is that painting might destroy
necessary to understand not only the            the object; the second is that it changes
virtues but also the limitations of this        the radiation properties of the object.
measurement technique. The physical             Thus the object will be a better radiator. It
background must be understood to
develop relevant techniques. This               will dissipate more ener&1-' and stay at a
application demands a complete
measurement solution, including the             lower working temperature, which might
proper hardware tailored to this                lead to a thermal design that gives the
application and software necessary for          designer incorrect information.
processing the thermograms acquired
with this hardware.                             Temperature Measurement
                                                on Printed Circuit Boards
    Measurement techniques must be
adapted to test objects. Looking at a           Printed circuit board components are
printed circuit board is different from         normally made of materials ·with strongly
using a microscope to look at                   varying radiation properties. From a
microcircuits or objects measuring a few        thermographic point of view the printed
square centimeter, such as hybrids and          circuit board surface is built up by a large
surface mounted devices.                        number of points. Each of these points
                                                might have another emissivity value. The
    Delow, a technique is described that        calculation of the temperature must
makes it possible to measure true               therefore take the individual emissivity in
temperatures, even of objects hidden from       each point of the image into
direct measurement ·while sitting in a rack     consideration. For example, the emissivity
or box.                                         over one arbitrary printed circuit board
                                                varied from 0.13 to 0.93.
Temperature Measurement
                                                    Figure 1 shows a measurement setup.
In noncontact temperature measurement           Note that the distance between the object
it is possible to calculate the correct object
temperature provided the object                 FiGURE 1: Setup for temperature measurement on printed
emissivity, the ambient temperature and         circuit boards.
the atmospheric temperature are known.
Electronic components are generally made
of various materials such as metal,
graphite and plastics. It should always be
assumed that the emissivity varies from
point to point over the object.
    Furthermore, the setup for this J..;ind of
measurement with the thermal camera
close to the object usually makes it
necessary to perform calculations in the
pre.~ence of varying reflected ambient
temperature over the object, because the
camera itself is reflected in the object. A
working camera shows a nonuniform heat
pattern, so it will be reflected
660 Infrared and Thermal Testing
and the camera is about 1 m (40 in.). A                       !Jiack and hence cold looking componenb
     wider fidd of view would let the camera                       at 5P03 and SP04. The printed circuit
     come closer to the object. On the other                       hoard contact under SPOS is not powered
     hand a closer range would create more                         up but has obviously been heated to the
     geometrical distortion in the image.                          same tempcratme as the board itself.
     A 20 degree lens at about 1 m (40 in.)
     distance will usually give a good result for                     Figure 2b shows exactly the same
     printed circuit boards of European size. It                   object after emissivity correction. The cold
     will also diminish the camera's influence                     looking parts at the top ll0\\7 have a
     on the reflected ambient temperature.                         higher temperature, obviously from
                                                                   applying the correct emissivities.
              How to Measure True                                  Finding of Emissivities in
              Temperatures on Objects                              Each Point of Object
              with Different Emissivities
                                                                   The true temperatures on complex objects
                     The true temperatures can be calculated       can be found only in controlled
                     only if a technique is used that can          measurement u mditions. The individual
                     handle the variation of the emissivities      emissivity in each point of the object is
                     over the object. Such a process ran he        calculated by means of a n•(erencc imase.
                   t·alled eqttalization, meaning that the         One way to obtain such an image is to
                     thermal image of an object can be
                     recalculated to a situation where the         FIGURE 3. Equalization box: (a) cross section; (b) sliding lid
                     object can be considered to have only one     drawn off box.
                     emissivity value. This recalculation can be
                     done if the emissivity is known in each       (a)
                     point of the object. After recalculation,
                     this knowledge will help find the true                                                                                     Printed circuit board
                     temperatures of the object.
                                                                        ~                Airflow
                         So the problem is to measure the
                     emissivity in each point of the object,           J'=~=_}==~;: '_ ."':He~~t~_"9_'_''_ment_'____ ,_ _ __
                     that is, to create an emissivity map of the
                     object. The values of this emissivity map     L _________"_"_'_'"-"_.,,_ti~---·-----_j
                     are then used to calculate the correct, true
                     temperatures over the object.                 (b)
                         Figure 2a shows a thermogram of the
                     control board of a hard disk before
                     emissivity correction is applied. Note the
FIGURE 2. Printed circuit board, powered up: (a) before
emissivity correction: (b) after emissivity correction applied.
(a)
(b)                                                                        Mirror plate                          Slidable lid
                                                                        Infrared Thermography of Electronic Components 661
put the printed circuit board into an          Therefore neither the object nor the
                     insulated box, an equalization box, where      camera may be moved from the moment
                      it can be heated up uniformly (see Fig. 3).   when the reference image is captured
                                                                    until the last real image of the printed
                         The objective is to heat up the whole      circuit board to be tested has been
                      object as equally as possible to a            captured. The printed circuit board and
                                                                    the infrared camera must stay in the same
                   temperature of, say, 323 K (50 oc =              positions during all measurements.
                      122 °F). This temperature is not crucial      Equalization Boxes
                      but should be above ambient (293 K
                      120 'C = 68 'FJ) and preferably close to the  Equalization boxes have been designed
                      expected working temperature of the           and manufactmed. Such a box is shown
                     object.                                        in Fig. 5.
                         The reflections should come                FIGURE 5. Equalization box: (a) with lid dosed, measuring 473
                     exclusively from the surroundings              x 220 x 310 mm (18.9 x 8.9 x 12.4 in.); (b) from behind with
                      (ambient) to the hox. Therefore the           lid opened to show printed circuit board mounted in box.
                      slanted walls are made of polished            (a)
                      aluminum, which has a very low
                      emissivity. Its high reflectivity will then    (b)
                      reflect the ambient (low) temperature
                      from the room rather than the high
                      temperature from the sliding lid-or the
                      mirror plates themselves.
                         \·Vhen the wanted reference
                     temperature is reached the lid is quickly
                     drawn off the box and the reference
                     thermogram is captured.
                         From the reference thermogram it is
                     possible to calculate the emissivity in each
                     individual point. The image in Fig. 4
                     includes an emissivity chart, ·where the
                     emissivity values (multiplied 100x) are
                    shown in a few spots. As can be seen SP03
                     and SP04 have very low emissivity values.
                     This is also the reason for the low
                     apparent temperatures in Fig. 2a. The
                     emissivity value used for calculating the
                     temperatures was incorrect.
                         The software program uses the
                     emissivity map to calculate the
                     temperatures in the corrected image,
                     which displays the true temperatures of
                     the object. It is important that the
                     reference image and the images to be
                     corrected cover each other exactly.
FIGURE 4. Emissivity chart showing emissivity values in image.
IR-1 EMRefl
SP01 91.1
SP02  7,5
SP03 23.0
SP04 03,8
SP05 84.2
662 Infrared and Thermal Testing
Thermographic equalization was
already being implemented in the 1980s.
Today's powerful computers make it
possible to pron:·ss such an image in
about 1 s. As the inspection usually
generates quite long sequer'Kes of raw
images, equalization must be able to
process these sequences automatically.
   There seems to be no comparable,
noninvasive technique <lvailable for
temperature measurement on printed
circuit boards. l-Ienee equalization is an
i11evitable tool for correct temperature
measurement on electronic components.
Long experience of the technique has fine
tuned the man-to-machine interface so
that it is quick and easy to handle. Once
the reference images arc captured the rest
can be handed over to the system.
                                                                         Infrared Thermography of Electronic Components 663
PART 2. Temperature Measurement with
Infrared Microscope
               1vteasurement with a microscope needs a            to the object surface. This can usually be
               more developed equalization technique.:l           done hy putting a smi:lll dot of paint \Yith
               The emissivity certainly varies over the           a known emissivity on the object. The
               object ~as in the example with the                 temperature difference between the
               printed circuit board. Figure 6 shows a            heating stage and the surface of the object
               thermal microscope.                                can be one or a few degrees, so it is
                                                                  important to know the real temperature
                  The microscope itself is a dominant             of the object.
               part of the object's cmzbintce. The object is
               very small, in this case about 6 x 3 mm               Comprehensive software for this kind
               (0.24 x 0.12 in.). The distance between            of thermographic measurement includes a
               the front lens of the microscope and the           presentation of the image in real time as
                                                                  well as a presentation of the equalized
               object is about 25 mm (l.O in.). The               image in at least quasi real time. This
               microscope has its working temperature,            makes it possible for the operator to
               which might be a few degrees above                 control the geometrical setting (focusing)
               ambient. Jf the object is shiny, \Vhich is so      of the object during the actual
               often the case with chips, tlle very cold          measmement. Simultaneously it is
               detector can see itself- that is, there will       possible to follow the development of the
               be a very cold spot h1 the middle of the           thermal situation in a twe temperature
                                                                  image.
               imnge. This is called the narcissus effect.
                   In this case the emissivity as -..veil as the      If the test strives for the highest
                                                                  possible time resolution it should also be
               reflected ambient temperature both vary            possible to perform equalization
               from point to point, so it is necessary to         aftenvards as a postprocessing operation.
               c<tlculate with two unknowns. Hence two            A practical technique for microscopic
               reference thermograms at different                 measurement might then look like the
               temperatures need be captured. The object          follO\\'ing:
               has to be heated up to two different
               reference temperatures - for example,                1. Put the object on the heating stage.
               60 degrees and 80 degrees- because it is            2. Localize the object and bring it into
               necessary to create two different cases. To
               do that the object has to be fixed in a                 focus.
               ltcatiug stage, that is, some device that can       3. Activate the equalization function.
               give the object these two different                 4. Power up the heating stage to the first
               temperatures in a controlled way.
                                                                       temperature.
                  The heat transfer between the heating            S. \'\1hen the first reference temperature
               stage and the object usually takes place
               via comluction. 1t is therefore important               is reached capture the first reference
               that the operator check the real                        image and store it. Re careful \'l'ith the
               temperature of the object while the                     name of the image so that they can be
               temperature falls from the heating stage                identified afterwards, for example,
                                                                      ref60.
FIGURE 6. Diagram of thermal microscope.                            6. Set the heating stage to the second
                                                                       reference temperature and capture a
                                                Mirror                 corresponding reference image. Name
                                                                       it , for example, re(SO.
                   ·--                                              7. Let the heating stage cool down for
                                                                       the measurement session.
                                     @                             8. \'\'hen the wanted heating ~tage
                                                                       temperature is reached power up the
               Magnifying lenm ---------------                         object with the wanted voltage and
                                                                       current.
Signal output                                                       9. Capture one or more thernwgrams of
                                                                       the object under pu·wer.
                                                                      If a whole healing process is to be
                                                                  studied, then a whole sequence with the
                                                                  wanted speed should be captured.
                                                                  Activate the equalization function to get
                                                                  the quasi real time trw.' temperature
                                                                  image onto the screen. The software
                                                                  should allow the processing to he carried
664 Infrared and Thermal Testing
out automatically, ending up in a             total field of view is about 6 x 3 mm
                    sequence of stored, true temperature          (0.24 x 0.12 in.) and the active part of the
                    images.                                       object !s about 1.4 x 0.45 mm
                                                                  (0.06 x 0.02 in.).
                        When this sequence has been
                    performed, the result may look as in          Practical Measurement on
                    Fig. 7. This series of images shows that the  Printed Circuit Board
                    true temperatures of the chip at 5 V and      Sitting in Rack
                     I A load (Fig. 7c) are considerably higher
                    than they seem to be in Fig. 7d. From the     One requirement of noncontact
                    reference images it can be seen that the      temperature measurement by
                    emissivities vary a lot over the image. The   thermographic imaging is that the object
                                                                  must be seen by the infrared camera. This
FIGURE 7. Reference images for stages of microscopic              necessity, unfortunately, makes it difficult
measurement: (a) reference image at 352 K(79 oc = 174 °F);        to study the temperature distribution on a
(b) reference image at 334.1 K(60.9 oc = 141.6 oF);               printed circuit board in its normal
(c) circuit being powered up, image not yet equalized;            environment. However, there is a
(d) equalized, true temperature image.                            technique that works in many situations.
                                                                  Consider the exponential cooling curve in
(a)                                                               Fig. 8.
(b)                                                                  Figure 8 shows the normal cooling
                                                                  curve for an arbitrary component. The
                                                                  idea is to determine the time constant for
                                                                  each point in the image and then apply
                                                                  that to the images taken at times t1 and t2•
                                                                  It is then possible to extrapolate
                                                                  backwards to find the image at t0 , when
                                                                  the object was still hidden from the
                                                                  thermal camera.
                                                                     The sequence in Fig. 9 illustrates the
                                                                  principle that an object adapts itself to a
                                                                  new ambient temperature along an
                                                                  exponential curve. The first image at
                                                                  time t0 (Fig. 9a) has been calculated from
                                                                  the images taken at times t1 (Fig. 9b) and
                                                                  t2 (Fig. 9c). The technique is as follo\vs:
                                                                                   FIGURE 8. Cooling curve for component on printed circuit
                                                                                     board.
(c)
(d) ,, ,,
                                                                                                                          Time (arbitrary moments)
                                                                                                             legend
                                                                                                                   u = observation angle (at specified moment)
                                                                                                               T~,,b =ambient temperature
                                                                                                                To!>J = temperature of test object
                                                                                                                 t -=- time (arbitrary points)
                                                                                                                   10 "' time at moment 0
                                                                                                                   11 = time at moment 1
                                                                                                                   !2 = tin1e at moment 2
                                                                                       Infrared Thermography of Electronic Components 665
1. Let the printed circuit board heat up           backwards by means of its individual
         and reach its normal operating                  cooling time constant. Different
         temperature in the rack.                        components have different cooling off
                                                         time constants, so they must therefore be
      2. Switch Off the power, take out the              calculated individually.
         printed circuit board and put it into
         an equalization box. At power off                  After the extrapolation procedure is
         capture the first thermogram. It will           carried out the normal equalization has to
         show nothing of interest but will               take place and results in a true
         capture the time for power off.                 temperature thermogram of the hidden
                                                         object at pO\\'er+off time. That has been
        \Vhen the printed circuit board is fixed         done in the pictures shown in Fig. 9.
     to its place in the box, start capturing a
     sequence which lasts two to three times
     the time between power off and the
     capture of the second image.
        Ilaving stored the two images, nm the
     program for extrapolation backwards and
     find the restored first image. This image
     represents the thermal picture of the
     object when it was still in its rack. Every
     point in that image has been extrapolated
FIGURE 9. Printed circuit board cooling to ambient
temperature: (a) at power oft, timet= 0; (b) 19 s after
power off; (c) 50s after power off.
(a)
(b)
(c)
666 Infrared and Thermal Testing
PART 3. Emissivity Evaluation for Electronic
Circuits and Components
Introduction                                 detector in the camera: 2 to 5.6 pm for
                                             short wavelength detectors; 8 to 12 pm
A persistent challenge in thermographic      for long wavelength detectors.
measurement is correction of temperature
readout according to emissivity of the          To evaluate the incident flux, the
investigated object. In electronics where    infrared mirror in the form of a highly
there are many clements with different       polished copper plate with reflection
emissivities (epoxy substrates, metals and   factor about 0.98 is used. One assumes
ceramics) the correction of thermographic    independence of the emissivity and
images by assuming homogenous                reflectivity from the wavelength in the
emissivity may lead to misinterpretation     spectral ranges mentioned above.
of measurements. The problem of
emissivity measurement will exist as long    fiGURE 10. Measurement of flux: (a) incident flux;
as thermography does. There are some         (b) reflected flux. Infrared mirror has emissivity close to zero.
techniques that permit measurement of
emissivity values. The calorimetric          (a)                                                       Infrared c<Jmera
technique is well explored. It is based on
measuring radiation flux while the                        Heilt source
temperature of the material is known.
Below, an indirect approach of measuring
emissivity is mentioned, where reflectivity
is used to measure emissive energy.
Principle of Reflection                                                 Infrared mirror
Technique
                                             (b)                                                       Infrared camera
The behavior of electromagnetic waves on
the border of two bodies can be                         Heat source
described:'1
                                                                             Object under measurement
(1) A + 11 + T
                                             legend
where A = absorbed energy, R = reflected
energy and T = transmitted enert,')'.          f.,"",!> =- energy density emitted by environment
Figure 10 shows test setups for                 f"'' = incident energy density
measurement of incident and reflected
flux.                                           £m:, = emis5ivity of infrared mirror (do5e to zero)
                                                F,.t.1= emis5ivity of object
   Some opaque objects have
transparency equal to zero. For radiation
parameters independent from the
wavelength, emissivity cis expressed as:
(2) E ~ 1 - p
where p is reflectivity.
   For objects in ambient temperature it is
possible to evaluate emissivity on the
basis of ine<Jsurements of the incident and
reflected energy.
   One aim for developing the technique
for emissivity measurement is to use the
same infrared camera used to measure the
temperature. To evaluate total
hemispherical emissivity, the heat source
has to emit the radiation that totally
covers the spectral range of the infrared
                                             Infrared Thermography of Electronic Components 667
A set of metal bodies (aluminum and                         The reflected flux including power
iron) with different surface states was                     emitted by investigated body in ambient
prepared to verify the accuracy of the                      temperature can he expressed as:
tedulique described below. The emissivity
factor for each body was evaluated
calorimetrically.5,6 Obtained values of
emissivity vary from 0.25 to 0.45.
Emissivity Evaluation for                                   where c is <tn unknown emissivity and 1~n
Specular Surfaces                                           is a substitute temperature obtained from
                                                            the camera.
Measurements of the emissivity are based
on the assumption that reflection                              nnally, the value of emissivity can be
characteristics for specularly reflecting                   calculated as:
surfaces (such as well polished metals) is
very sharp- that is, a very small                           (6)
deviation from the mirror angle causes
very rapid decrease of the reflectivity. This               In many practical cases for diffusely
sharpness means that the main part of the                   reflecting surfaces, the values of emissivity
flux is reflected in the mirror angle. In                   obtained using Eq. 6 are incorrect because
consequence it is possible to evaluate the                  only that part of the enerb'Y reflected in
emissivity on the basis of specular                         the mirror angle has been measured.
reflectivity.                                               Emissivity strongly depends on surface
                                                            conditions. In many practical cases there
   For an infrared mirror in ambient                        is a difference between emissivities
temperature, the flux measured by camera                    measured according to Eq. 6 and results
takes the form:                                             presented in the literature.5·8
where Einc is incident flux, Tcu is copper
mirror substitute temperature, 7~ is
ambient temperature and Pcu is copper
mirror reflectivity:
FIGURE 11. Reflectivity characteristics of real body (representative metal) for different angles of
incident flux.
                                                            Ref!ectivily P1.~N
                           legend
                               jJ =angle of incident flux
                               q =angle of reflective flux
                               p = reflectivity
                                t = trammissivlty
668 Infrared and Thermal Testing
Emissivity Evaluation for                       reflection that exists in many practical
Diffuse Surfaces                                cases. To take this phenomenon into
                                                account the measurements have to be
As mentioned above, the assumptions on          made in different directions,
the mirror reflection is sometime not
valid, even in the case of metal bodies.        Evaluation of Emissivity
The state of the surface of the investigated    with Anisotropy of
body (mainly its roughness) is the main         Reflection
factor that can change the emissivity. The
diffused reflection has to be taken into        The analysis of errors in particular
account in many practical cases:P) The          measurements of emissivity using the
reflectivity characteristic for a               technique described here has led to the
representative metal object is shown in         conclusion that reflectivity characteristics
Fig. 11.                                        sometimes depend on angle of
                                                observation. Such anisotropy effects have
    For the object with given emissivity,       been observed for samples with distinct
the total reflected energy is equal to          texture on their surface. If one of the
(1 ~f.)Eino where Einc is incident cncq,')'.    directions on the surface of the sample is
The mirrored reflection is sharper and the      marked out (for example in the mat
more diffuse reflection is flatter. As shown    process), the reflectivity characteristic in
ii1 Fig. 11, the correlation between the        that direction will differ significantly from
valne of flux reflected in the mirror angle     the characteristic measured in the
and a certain a parameter describing the        perpendicular direction (Fig. 13).
characteristic width is expected. As such a
parameter, coefficient 0 is chosen as a             In Fig. 13 the variable ~<1> represents
                                                deviation from mirror angle and the value
ratio of reflected flux for angle p (different  of the reflected energy E is expressed in
                                                scaled units:
than mirror one) to the flux reflected for
                                                (10) E[/TJ
the mirror angle Pmir-
   To continue the evaluation of                    The total value of the reflected energy
                                                is proportional to the volume of the solid
emissivity, the heat fluxes must be             limited by the shapes of the reflectivity
measured as follows: (1) for an infrared
mirror and mirror angle, (2) for a given        FIGURE 12. Correlation curve of reflected flux in mirror angle
object and mirror angle and (3) for a
given object and the angle deviated from        and parameter 0 defining shape of reflectivity characteristics.
the mirror one,
                                                Real emissivity of aluminum and iron samples has been
   The relative value of the energy K           evaluated calorimetrically. Rectangles indicate range of
reflected in the mirror angle has been          results considering accuracy of measurements and
introduced as:                                  environmental noise.
(7) K  cr7~~ - Ea
       aT~11 - Ea
where Ea = a'l~4, Hnally:
(8)    ym4 - Ta"mb
       T C4u  -  T  4
                    amb
The parameter 0 of the shape of the
reflection characteristic is defined as:
(9) s                                                                                  12
                                                0.2 'o::J
                                                0.1
where Til is substitute temperature (K)                     0 0.1 0.2 0.3                            0.4
measured for angle p, 1~n is mirror             legend
                                                    I to 5. A!t,minum, emissivity t: "'0.31 to 0.35
angle temperature (K), 7~ is ambient                      6. Iron, emissivity£=- 0.44 to 0.51
temperature (K) and Tcu is substitute
temperature (K) for infrared mirror               7 and 8. Iron, emissivity£"' 0.36 to 0.42
                                                          9. Aluminum, emissivity F = 0.45 to 0.49
defining heat source temperature. Results               10. Aluminum, emis5ivity F ==- 0.4 to 0.45
of the measurements are shown in Fig. 12.                11. Aluminum, emissivity c == 0.32 to 0.38
                                                         12. !ron, emissivity r ,_ 0.44 to 0.5
   The nonlinearity of the correlation
curve can he noticed in Fig. 12. Some of
the results differ significantly from
obtained results. The technique presented
above does not consider anisotropy of the
                                                Infrared Thermography of Electronic Components 669
characteristics for all directions of                                calculate the volume of such a solid, the
            observation. It is quite difficult to measure                        assumption that the cross sections of the
            total hemispherical reflectivity, so some                            reflectivity characteristic.~ nre elliptical is
            simplifications have to be made. To                                  introduced. To check the correctness of
                                                                                 this assumption, the cross section of the
FtGURE 13. Reflectivity characteristics for one sample with                      hemispherical reflectivity characteristics
anisotropy on surface for two perpendicular directions of                        have been measured for a metal sample
observations, radiation flux versus angle for two                                (l'ig. J4).
perpendicular directions.
                                                                                    The cross sections shown in Fig. 14
   100                                                                           have been obtained from characteristics of
                                                                                 reflectivity measured in different angles u
   90                                                                            of observation (a1, a 2, a 3) in the range
                                                                                 from 0 to 90 degrees. The change of the
   80                                                                            observation angle has been obtained by
                                                                                 rotating the sample about a given angle.
g 70                                                                             For each rotation angle, the reflectivity
                                                                                 characteristic E UTI =/(!>.$)has been
~ 60                                                                             measured and then the shapes
                                                                                 corresponding to equal values of energy
:f 50                                                                            have been drawn.
w  40
~                                                                                    The assumption of the ellipsoidal shape
~ 30                                                                             of the cross section is not valid in the case
                                                                                 of the samples with very high anisotropy.
   20                                                                            It leads to the errors in calculations of the
   10                                                                            FIGURE 15. Temperature map of converter from left side: two
                                                                                 diodes placed on radiators, transformer and resistive load:
   O L __ __ L_ _~----~~~===-+                                                   (a) before covering with black paint of emissivity£~ 1.0;
                                                                                 (b) after painting.
       0 5 10 15 20
                                                                                  (a)
            U<l' (degrees)
legend
   t\cf> =for first direction, angle between camera axis and norma! to object
  E01) ""characteristic of reflectivity
  "*-=direction 0 degrees
  -II-= direction 90 degrees
FIGURE 14. Cross sections of hemispherical reflectivity
characteristic for sample with anisotropy on surface.
      40
        30                                                                       (b)
-~
  i"
:"w3' 20
 6
  <l
        10
     0
         0 2 3 4 56 7 8
                                        .0.1112 (degrees)
legend
  .0,(])1 =for first direction, angle between ram era axis and normal to object
  .0.cf>2 =for second direction, angle between (amera axis and normal to
            object
      •=f=30JT
      ee£e40JT
      .1..=£=50)1
      +e£e60JT
      C =observation angle (t = 60 degrees
     0 =observation angle (( = 45 degrees
     i::J..= observation angle u = 30 degrees
670 Infrared and Thermal Testing
total reflected energy and hence of the     placed on the black painted radiator.
                    solid volume. An additional problem is       Transistors work in the final stage of the
                     how to choose the directions of
                     measurements properly.                      100 W power supply (Fig. 16).
                                                                    Emissivity of all these elements h<Js
                        To check correctness of the proposed
                     technique some measurements for             been measured with the reflection
                    different samples have been made. The        technique. The results in ·n1ble 1 take into
                     results have been compared with the ones    account the accuracy of the measurement.
                    obtained by calorimetry and by equalizing
                     the emissivity by painting the surface         Temperature maps for both objects has
                     with highly emissive coatings.              been corrected. To verify the results the
                                                                 second series of the measurements in the
              Emissivity Correction in                           same conditions have been made after
              Thermo~raphy of                                    covering all the elements with bl<Jck paint
              Electromc Circuits                                 (£ ~ 0.9).
                    Two power electronic circuits have been      TABLE 1. Measurements of emissivity using
                     measured using the technique described      reflection technique.
                     above. The first one is presented by
                     thermal images in Fig. 15. It consists of   Test Object               Emissivity
                     rectifier diodes on the metal radiator,
                     transformer and resistive load. The second  Metal radiator of diodes  0.3 to 0.4
                     circuit consists of a pair of power
                     transistors (laser diodes in a metal case)  Case of transistors       0.3 to 0.4
fiGURE 16. Temperature map of converter after correction of      Transformer and resistive load 0.9 to 1.0
emissivity: (a) emissivity£~ 0.3; (b) emissivity E ~ 0.4.
                                                                 FIGURE 17. Temperature map of power transistors in end
(a)                                                              stage of power supply unit (1 0 V, 10 A): (a) before covering
                                                                 with black paint of emissivity E ~ 1.0; (b) after painting.
                                                                 (a)
(b) (b)
                                                                 Infrared Thermography of Electronic Components 671
Thermographic measurements of the        (Fig. 18}. Because of the comple-x shapl'
                    power converter ·without emissivity          and many small details in the observed
                    correction suggest that the most heated      object, the results are not as
                    parts of the circuit are the resistive load  straightforward as in the previous case.
                    and diodes and that the transformer has a    Additionally, the parasitic reflection
                    much lower temperature {Hg. 15a). After      occurs, which is more important for an
                    covering all the elements with black paint   object of low emissivity. Nevertheless, the
                    (E "" 1) it can be seen that the diode has   evaluation of emissivity t from 0.3 to 0.4
                    the highest temperature (Fig. 15b),          gives signifh:zmt improvement of the
                                                                 temperature measurements.
                        Figure 16 shm\'S the temperature map
                    after correction using the measured values   Conclusions
                    of the emissivity.
                                                                 A technique has been developed for
                        Figure 17a shows the temperature map     practical applications of emissivity
                    of the final stage of the power supply (two  evaluation. The technique gives good
                    power transistors placed on same             results in the laboratory, where the
                    radiator). The situation seems to be         measurements can he done precisely and
                    paradoxical: the heat source has a lower     with good equipment. Two problems limit
                    temperature than the cooling fins. A real    the technique: (1) difficulty in very
                    temperature map obtained after painting      precise determination of the mirror angle;
                    the object is shown in Fig. 17b. On lhe      {2} parasitic reflections from objects with
                    basis of the measurements of the             complex shapes and low emissivity.
                    emissivity for the transistor enclosures,
                    the temperature has been corrected              This technique can be a good basis for
                                                                 classifying the objects for ones with high
FIGURE 18. Temperature map of power supply unit after            (£ "" 0.9) and low(£ "" 0.3) emissivity. The
correction of emissivity factor of upper side of transistors:    technique can be useful when the correct
(a) emissivity £ = 0.3; (b) emissivity£= 0.4.                    interpretation of the thermal state of the
                                                                 device (for example failure analysis) is
(a)                                                              needed rather than the measurements of
                                                                 the temperature with very high accuracy.
                                                                 The technique presented can be also used
                                                                 in the case of working circuits (devices)~
                                                                 for example, with high voltage but with
                                                                 the assumption that energy emitted by a
                                                                 part of the circuit is small in comparison
                                                                 with the total energy reflected from its
                                                                 surface.
(b)
672 Infrared and Thermal Testing
PART 4. Spectral Emissivity Evaluation of
Materials for Microelectronics
                     Introduction                                                                                                  various spectral ranges. Spectrc:1l emissivity
                     Emissivity is measured for materials used                                                                     may be useful for calculating heat
                     in electronics -for example, aluminum,                                                                        removal by radiation in microelectronic
                     semiconductors {silicon and germanium)
                     and diamondlike thin structures such as                                                                       devices. Emissivity needs to be evaluated
                     coatings. Additionally, emissivity needs to                                                                   whenever thermography is used to
                     be evaluated for semitransparent and                                                                          measure temperature. Emissivity depends
                     multilayered dielectric materials. The
                     measurement is performed using infrared                                                                       on many varying parameters:
                     spectrometry. For every sample the                                                                            temper(lture, wavelength, surface
                     reflected and transmitted energy are                                                                          oxidization, roughness etc. Although
                     measured in the direction normal to the                                                                       there are various techniques to measure
                     surface of the investigated material for                                                                      emissivity, it is hard to quantify emissivity
                                                                                                                                   precisely.5•6
                                                                                                                                       For opaque materials the directional
                                                                                                                                   emissivity can be evaluated:
FIGURE 19. Reflectivity and emissivity for aluminum in band from 2.5 to 14 f-Jffi: (a) unpolished aluminum; (b) aluminum with
diamondlike coating; (c) anodized aluminum, black; (d) anodized aluminum, not black.
~: -~1--=-=~±=L(a) 10,----~---                                                                         .-t_l----=- ----t----:J     (c)    1.0
       Ifl -                                                                                                                              0.9
                                                                                                                                      p"  0.8
r_- _:-:: -_- j- ___--1_--:_t~ .r-- '-- _I                                                                                            :~
o.51- ~--0           _I  -                                                                                                         -~     0.7
                               --'_ t-----·~_.-- f--.--                                                                  c-[              0.6
.      4  1          -+                                                                                                            c      0.5
                                                                                                                                          0.4
                                                                                                                                   b" O
                                                                                                                                   "0 -~
                                                                                                                                   oc "0
                                                                                                                                    a_
-ij~~~'--~+-----, .=c_i -L                                                                                                         :ep 0.3
                                                                                                                                             0.2
~ 1 I - f->-~-:_:~~-t ::-:-)~ .::-:: :__;-I •'\; 0.1
                                                                                                                                   "" 0
       24                      6         8                                                             10 12             14 16                    2 4 6 8 10 12 14 16
                               Wavelength ), (!-lm)                                                                                                          Wavelength }, (!-lm)
rl{b)                                                                                                                              (d)
                     ----~--~  - ~1-     T~:~                                                               ~---~(f~---  ;                .. _ j1.0
~:1.0  I-                             ~                                                                                                                              _r_ ~-~_:-]
                                                                                                                           i              l··-··0.9          +-H-j'i· .... _
       1
~- ~~---1- -f-- -r:: -:-- _J_ -1                                                                                                          0.8 - · - - -
                                                                                                                                                  I                                I
                                                                                                                                                         -~
                                                                                                                                          --! - -0.7 '-      - - '-'e·-- , -          I
                                                                                                                                          +-0.6              L - ;~ --~:: --~:
   r_- -_:~                    _t_                                                                     1- -1 -i-_r                        0.5 ~- ..
                                                                                                    1
I +-r-a_                       -iI -                                                                                                      0.41- -~~--        -~-_j_
          03                                                                                           . i - -L- j
     I0.2                      _, _      J.                                                                 _I_ J!_ .           :         0.3                                         i IIII -
           o.1
                                                                                                       -t-  I1 ,                          0.21                                     r
       o
                                                                                                                                          I0.1                                          II
       2 4 6 8 10 12 14 16                                                                                                                j _0 (___
                                                                                                                                                                                   - _ _ '__ j
                                  Wavelength ).. (I-'m)                                                                                           2 4 6 8 10 12 14 16
                                                                                                                                                             Wavelength A (jJm)
legend
  -=reflection
    .... ==emission
                                                                                                                                        Infrared Thermography of Electronic Components 673
(11) e(e) ~ 1 - p(e)                               Emissivity Measurements
             where p(9) denotes directional reflectivity        The rt"sulb of the reflection and
             for angle 9. For metals, the emissivity            transmission measurements and the
             strongly depends on the optical properties         calculated emission are presented in
             of each metal, especially on the reflective        Figs. J9 to 23. Aluminum samples with
             index typically expressed as a complex             different surface conditions and
             number 11:                                         semiconductors (silicon and germanium
                                                                covered by thin diamondlike layers) were
             (12) II ~ 11' + ik'                                chosen for measurements. All
                                                                measurements were done in a direction
             The problem is much more difficult for             normal to the surface of investigated
             semitransparent and multilayer structures          body, in the spectral range from 1.4 to
             in microelectronics. To evaluate the               14 pm.
             emissivity of such structures, material
             transmission and internal reflections must             For opaque materials like aluminum
             be considered.5 The electromagnetic ·wave          the normal spectral emissivity is
             propagation theory is widely applied in            calculated:
             such cases, especially for dielectric layers
             with a thickness of the same order as the          where p11 (),) denotes the normal spectral
             waveleng'th.                                       reflectivity. For semitransparent
FIGURE 20. Reflectivity and transmissivity for silicon in band  fiGURE 21. Reflectivity and transmissivity for germanium
from 2.5 to 14 ~m: (a) silicon; (b) silicon with diamondlike    from 2.5 to 14 11m: (a) germanium; (b) germanium with
                                                                diamondlike coating.
coating.
(a)                                                             (a)
        0.7                                                          ::r·1~t~ ~tr~
.13~
JsH~r: -r~l!:i:f 0.6
        o.s                                                           -1 -I- 1-!- 1
c                         ~----l'\1)-~--)1-- I                       f-0.3
~~
        0.4  -- -_j_
~o
"U 'OJ
 cm
m'o     0.3                                                          t- T0.2                                      -1
        0.2
a.                                                                                                                - ---' -:
        0.1                                                          l T L Ii0.1 -!-
.·.,~                                                                                                             _j
        0 L..
 v
 ~
··~-~r:[i·t~'tj
~
                          __L~-' _j_          j__j                   0
                                                                          0 2 4 6 8 10 12 14 16
             0 2 4 6 8 10 12 14 16
                          Wavelength ), (~m)                                                 Wavelength). (tJrn)
(b)                                                             (b)
                                                                   + . . ·rr J-t- r-\07 ~-F ~-~-          -~-I
                                                                              0.6                I- f--t- !
                                                                     o.s
                                                                     0.4
                                                                     0.3
                                                                     0.2
                  02      4 6 8 10 12 14 16                          0.1                  2  46       Ii
                                Wavelength A (pm)                    0
legend                                                                                           8 10 12 14 16
  - =reflection                                                           0
          = transmission
                                                                                             Wavelength ), (prn)
                                                                legend
                                                                  - "' reflection
                                                                  ···---- = transmi~sion
674 Infrared and Thermal Testing
semiconductors with a diamondHke                                         (15) R                 I
         coating it is necessary to include                                                           p
         transmission energy as in Eq. 1. For
         emissivity recalculation the internal                                    (16) T
         reflections have to be taken into account.
         The part of the energy absorbed in every                                 By using Eqs. 14 and 16, reflectivity p and
         layer corresponds to the layer emissivity.                               transmissivity t can be evaluated as
                                                                                  functions of wavelength /,.Together with
            Assuming single semitransparent layer                                 Eqs. 1 and 2, these values can then be
         as shown in Fig. 24, the total absorption A                              used to evaluate the emissivity for any
         includes the reflection from the second                                  dielectric material with and without tile
         surface:"                                                                internal reflections. ~vfaterial thickness is
                                                                                  assumed to be much larger than the
         (14) A                               (1 - p)(1 - 1)                      applied wavelength (Eq. 16), or wave
                                                                                  interference must be considered, too.
                                                  1 - p1
                                                                                      For multilayer semitransparent
         Equation 14 was derived by a net                                         structures with thin coatings - for
         radiation technique, under the                                           example, silicon with diamondlike
         assumption of isothermal conditions                                      coating and germanium with diamondlike
         (absorption does not increase the                                        coating~ more complex formulas are
         temperature). Similarly, it is possible to                               used (Fig. 24):'·s
         measure the reflected and transmitted
         energy fractions experimentally.
FIGURE 22. Reflectivity and transmissivity for silicon in band                    FIGURE 23. Reflectivity and transmissivity for germanium in
from 1.4 to 2.5 ~m: (a) silicon; (b) silicon with diamondlike                     range from 1.4 to 2.5 11m: (a) germanium; (b) germanium
coating.                                                                          with diamondlike coating.
(a)                                                                               (a)
           0.6
0.5
0.4
0.3                                                                                                                                               I
0.2
0.1                                                                                                  i_1
0                       1.6 1.8 2 2.2                              2.4                    1.4 1.8 2 2.2 2.4
    1.4                                                                                                        Wavelength), (!-lm)
                                 Wavelength), (1-lm)
(b)                                                                               (b)
             0.7 i -.--. _: .. ,_
                                                                                                                            "l ;-- -1
0.61--                                                                                    0.71--j-                                                   JI
                                                                                          0.6 ~- - - -                      . ~-i·~ .J-.-~ ~I
0.5 --                                                                                    :: i=L~                           =l-1 i \
                             1             i                                              :: l.~ . ·.y__rr·                                       -- -1--l___J_'
0.4 ~ - ----·j                     -~
                             I
0.3 ' '-v.,__;-,__..::;..;_,:..•• ~-~:;:::::.. ·_j----.,                                                                                                   -,
0.2 ' --tI-                                               t.I - I           . II          o.1 1       _ '--........_-       ~I -+ 1
0.1 ,_ - ,
                                                          __.L      +f ~:                          '                   '-~  J _l_
0                                                           2 2.2  -j '                   0
   1.4 1.6 1.8
                                                                       2.4                '1.4 1.6 1.8                                            2.2 2.4
                                   Wavelength /, (l-Im)                                                                     Wavelength ). (!-lm)
legend                                                                            legend
  -=reflection                                                                      --=reflection
  ···-·--=transmission                                                              ....... = transmission
                                                                                       Infrared Thermography of Electronic Components 675
(17) T  (1 - Pt}(l - rz)t.                                       (19) II            Pt + (1 - 2pt)Pzt2
(18) A         - PIPzl2
                                                                                         1 - P1 pz-r 2
        (1- p,)(l- p,t)(l-t)
                                                                 where p1 and p2 arc reflectivities for both
               1 - PtPzt2                                        layers and tis the transmissivity for the
                                                                 upper layer.
FIGURE 24. Semiconductor structures for
emissivity evaluation: (a) semitransparent                          The results of measurements of
structure; (b) multilayer structures.
                                                                 emissivity for aluminum with different
(a)
                                                                 surface states are presented in Fig. 19. For
                                                                 aluminum the polynomial
                                                                 approximations of the emissivity are
                                                                 provided over the spectral range used by
                                                                 thermography, that is, 2.5 to 14 pm:
                                                                 (20) <(!.)
                    9,3           93                             where 'A :::: wavelength (pm) and E('A) is
                                                                 expressed as a percentage. See Table 2.
'/ \                                      SHkon, n,, '"
\ !0,2 9p2                                                           Both for the single and the multilayer
                                    Germamum, ncu -ree           structure R(J,) and T(J,) are measured as
                                                                 shown in Figs. 20 to 23. The quantity for
                                  \ Air, n~                      n()..) is yielded by using Eqs. 14 and 16
                                                                 and the following relation for
                                                                 reflectivity p:
                                                                 (21) p             (11 - 113 ) 2
                                                                                    {H + 113 ) 2
(b)                                                              where lla is the reflective index for air;
a\)'                                                             typically lla = 1. In more predse
                                                                 calculations naO•) can be provided 10 as the
                                                                 cauchy or sellmeier formula:
                                                    D!amondlike  TABLE 3. Radiatlon properties of semiconductors.
                                               coating, n0 tc
                                                                 Wavelength         RTA p                                     f     /)
                                             Silicon, n5,, ts,
                                           Germanium, nee, tee         (~rn)
legend                                                           Silicon            0.46    0.53         0.01  0.30     0.29  0.39  3.43
    n~ = refraction index for air                                  2.5 to 5.5 J.Jm  0.38    0.36         0.26  0.30     0.21  0.48  3.45
   nc "'" refraction index for diamond like coating                8to12J.Jm
                                                                                    0.54    0.46         0.00  0.37     0.37  0.26  4.10
  nee = refraction index for germanium                           Germanium          0.54    0.45         0.01  0.37     0.37  0.26  4.14
   nSJ = refraction index for silicon                              2.5 to 5.5 J.lm
    0, = angle of incident radiation                               8to12pm
    9 , = angle of reflected radiation
    '~1 = transmissivity for diamond like coating                R = reffQcted energy
  tee = transmissivity for germanium
   !~; = transmissivity for silicon                              T ==transmitted energy
                                                                 A = absorbed energy
                                                                 r = reflectivity
                                                                 r =transmissivity
                                                                 f' = emissivity
                                                                 n =refractive index
TABlE. 2. Coefficient for polynomial approximation of emissivity for aluminum.
        Test Object               Co c, c, c, c,                                                                 c,
Aluminum                           16.87    -5.64                 5.22              -1.37          0.13        -0.004
Anodized aluminum, black          -31.36    54.88                -2.04              -1.65          0.22        -0.008
Anodized aluminum, not black                20.04                 4.77              -2.13          0.22        --0.007
                                   22.75                                                                       -0.007
Aluminum with coating                       63.45                -1.23              -.t.63         0.19
                                  -37.61
676 Infrared and Thermal Testing
(22) ""          I + 5. 7:l87 x I 0""4 ),2     Conclusions
                         1? - 595260           In this chapter the measurements of the
                                               spectral emissivity for the semiconductors
where/, is wavelength (pm).                    and aluminum with different surface
                                               coatings are presented. For
   In Table 3 radiation proprieties for        semiconductors the emissivity is quite
silicon and germanium are presented.           low, except for that of silicon in the long
                                               wavelength range. This effect was not
Symbols U, T and A denote the fraction of      observed for germanium. A thin l<1yer of
the reflected, tr<lnsmitted and absorbed       diamond on the semiconductor docs not
energy. Absorbed energy property ;\            increase the emissivity very much but
corresponds to the emissivity of the           works as <mlireflective coating, especially
semitransparent window if the internal         in short wavelength range. For aluminum
reflection is taken into consideration .       widely used in electronics, both the
However, using Eqs. 14 and 16 can help         anodizing and the covering by the
find the reflectivity p, the transmissivity 1  diamond increases the emissivity
and the emissivity f for tile thick material   significantly. From the measurement it b
when there are no internal reflections.        possible to ide.ntify the wavelength
                                               dependent optical parameters of
   The obtained parameter values agree         semitransparent materials: n, p and 1.
with the values published and measured
by other techniques~ for example, the
refraction indexes10 ,_are Htit· = 3.99 and
nsi = 3.49. For multilayer semiconductors
the total amount of energy absorbed in
whole structure is provided (fable 4).
~vfore detailed investigations need to
include the incident and reflective ·wave
interference because the diamond
thickness is of the same order as the
infrared \\'avelength.
TABlE 4. Radiation proprieties of
semiconductor multilayers.
Wavelength              RT          A
     (pm)
Silicon with Diamondlike Coating
2.5 to 5.5 j.Jm  OAO 0.54 0.06
8to12pm          0.38 0.32 0.30
Germanium with Diamondlike Coating
2.5 to 5.5 j.Jm  0.43 0.54 0.03
8 to I 2 ~m      0.50 0.44 0.06
R"' reflected energy
T"' transmitted energy
A"" absorbed energy
                                               Infrared Thermography of Electronic Components 677
References
                  1. KOlzer, J., E. Oesterschulze and
                          G. Deboy. "Thermal Imaging and
                         ~vfeasurement Techniques for
                          Electronic Materials and Devices."
                          Microelectrooic Engineering. Vol. 31.
                          Amsterdam, Netherlands: Elsevier
                          Science Publishers (February 1996):
                         p 251-270.
                      2. Nishino, S. and K. Ohshima. "A Study
                          on Fault Detection for IC Boards Using
                        Thermography.11 Systems and Computers
                          in japan. Vol. 29, No. 5. Bognar Regis,
                          \"'est Sussex, United Kingdom: \-\'iley
                          lnterScience (May 1998): p 49-61.
                       3. Burggraaf, P. "Imaging: Microscopy
                          and Thermography." SeJninnuluctor
                         lntemational. Vol. 9, No. 7.
                          Des Plaines, IL: Cahners Business
                         Information Uuly 1986). p 58-65
                      4. Siegel, R. and]. Howell. Thermal
                        Radiation Heat Transfer. New York, NY:
                          Hemisphere Publishing (1989).
                     5. Sala, A. Radiation Heat Tnmsf'er lin
                          Polish). Warsaw, Poland: WNr (1982).
                       6. Burakowski, T. et al. Promienniki
                       PodC7.{'(Wieni lin Polish]. \'\7arsaw,
                          Poland: WNT (1970).
                       7. \Viecek, B. and lvL Grecki. "Technical
                          Method of Emmisivity Correction in
                          'l'hermography." Qilll11titatil'e l11(rared
                          Tllcrmograp/1)' (QIRT '94) [Sorrento,
                         Italy, August 19941. Eurotl!erm
                          Seminar 42. Paris, France: Editions
                          EuropCenncs Techniques et Industries
                          (1995): p 253-259.
                      8. ~vfadura, H., H. Polakowski and
                          ll. Wiecek. ''MWlR and LWIR
                          Emissivity !vfeters.11 Paper B3.
                           Quantitative Infrared Then1wgmpl1)'
                          (QIRT '96) [Stuttgart, Germany,
                          September 1996). Eurotherm
                          Seminar 50. Stuttgart, Germany:
                          Universitat Stuttgart, lnstitut flir
                          Kunstoffprlifung und Kunststoffkunde.
                  9. \'\'iecek, ·n. and H. Madura. "Radiative
                          and Convective Heat Transfer in
                          "tvficroelectronit:s." Paper BS.
                        Quantitative In(rarecl Tflcn1WStafJI1)'
                          (QIRT '96) !Stuttgart, Germany,
                          September 1996j. Eurotherm
                          Seminar 50. Stuttgart, Germany:
                          Universitiit Stuttgart, Jnstitut fiir
                          Kunstoffprlifung und Kunststoffkunde.
                    10. Lide, D.L., ed.lland/Jouk o(Cimnistry
                        and Pllysics, 76th edition. New York,
                          NY: CRC Press (1995-1996).
678 Infrared and Thermal Tesflng
CHAPTER
Infrared and Thermal
       Testing Glossary
               Herbert Kaplan, Honeyhill Technical Company,
               Norwalk, Connecticut
               Jean-Claude Krapez, French National Aerospace
               Research Establishment (ON ERA), Chatillon, France
               Minh Phong Luong, Ecole Polytechnique, Paris, France
               Xavier P.V. Maid ague, University Laval, Quebec,
               Quebec, Canada
               Gary L. Orlove, FUR Systems, North Billerica,
               Massachusetts
               Nik Rajic, Defence Science and Technology
                Organisation, Melbourne, Australia
               Andres E. Rozlosnik, 51 Termografia lntrarroja, Buenos
               Aires, Argentina
PART 1 . Terminology
Introduction                                   acceptance level: In contrast to rejection
                                                   le\•el, te.':.l level above or below which,
Many of the definitions in this glossary           depending on the test p<lfameter, test
are adapted from the Nondestructive Testing
Handbook, second edition: Volume 10,               objects are acceptable.' Compare
Nundestructil'e Testing Oren•iew. 1 These and      rejection lcl'el.
other definitions in this glossary have        accuracy: Degree of conformity of a
been modified to satisfy peer review and
editorial style. References given in this          measurement to a standard or true
glossary should be considered not
attributions but rather acknO\\'ledgments          value.'
and suggestions for further reading.           adaptive thresholding: Threshold value
   The definitions in this Nondestructiv£'          varying with inconstant background
Testing Handbook volume should not be              gray Jevel. 1
referenced for inspections performed           agency: Organization selected by an
according to standards or specifications or         authority to perform nondestructive
in fulfillment of contracts. Standards              testing, as required by a specification
writing bodies take great pains to ensure           or purchase order. 1
that their documents are definitive in
wording and technical accuracy. People         algorithm: Prescribed set of well defined
working to written contracts or                    rules or processes for the solution of a
procedures should consult definitions               mathematical problem in a finite
referenced in real standards when                   number of steps. 1•5
appropriate.
                                               ambient light: Light in the environment
    This glossary is provided for                   as opposed to illumination provided
instructional purposes. No other use is             by a visual testing system. 1
intended.
                                               ambient operating range: Hange of
A                                                   ambient temperatures over which an
absolute temperature: Temperature                   instrument is designed to operate
     measured from absolute zero
     temperature, expressed in kelvin (K)           within published performance
     in 51. 1                                       specifications.3
                                               ambient temperature: 'Jemperature of
absolute temperature scale: Temperature
      measurement scale based on coldest            immediate surroundings and
      possible temperature equal to 0. (See
      rankine and kell•in).2                        environment where a lest or
                                                    measurement takes place. A parameter
absolute zero: Temperature that is zero
     on the kelvin or rankine temperature           used to compensate for radiation
     scales. The temperature at which no            reflected from test object and air in
     molecular motion takes place in a              the field of view.
     ,TiateriaL3                               ambient temperature compensation:
absorptivity (absorptancc): Proportion              Correction built into an instrument to
     (as a fraction of 1) of the radiant            provide automatic compensation in
     energy impinging on a material's
     surface that is absorbed into the              the measurement for variations in
     material. Par a blackbody, this is unity       instrument ambient temperature.3
     (1.0). Technically, absorptivity is the   amplitude response: That property of a
     internal absorptance per unit path
     length. fn thermography, the two               test system whereby the amplitude of
     terms have sometimes been used                 the detected signal is measured
     interchangeably.3                              without regard to phase.' ··1
                                               analog-to-digital converter: Circuit
                                                    whose input is information in analog
                                                    form and whose output is the same
                                                    information in digital form. 1•5
                                                anisotropy: A material's characteristic of
                                                    exhibiting different values of a
                                                    property (acoustic velocity, for
                                                    example) in different directions in the
                                                    material because of different
                                                    arrangements of atoms.1
                                                annealing: Process of healing and cooling
                                                    a material, usually to reduce residual
                                                    stresses or to make it softer. 1
680 Infrared and Thermal Testing
anomaly: Discontinuit)'. A variation from     B
    normal in product quality or material
    property. 1                               background noise: Signals that originate
                                                  from the test object, the test
AOQ: Average outgoing quality.                    instrument and their surroundings
                                                  and that interfere with test signals of
AOQL: Average outgoing quality limit.             interest. It may have electrical or
AQL: See acceptable quality level.                mechanical origins. Sometimes called
                                                  grass or hash.1
apparent temperature: Target surface
    temperature indicated by an infrared      background signal: Steady or fluctuating
                                                  output signal of a test instrument
    point sensor, line scanner or imager,         caused by the presence of acoustic,
    generally taking the emissivity into          chemical, electrical or radiation
                                                   conditions to ·which the sensing
      account.:~                                  element responds.1
arc: Luminous high temperature discharge      background temperature, instrument:
                                                  Apparent ambient temperature of the
    produced when an electric current             scene behind and surrounding the
    flows across a gap. 1                          instrument, as viewed from the target.
arcing: Electric current flow through a           The reflection of this background may
    gap, often accompanied by intense              appear in the image and affect the
                                                   temperature measurement. Most
     heat and light.'                              quantitative thermal sensing and
arc welding: See electric arc welding.             imaging instruments provide a means
artifact: In nondestructive testing, an            for correcting measurements for this
                                                   reflection.3
    indication that may be interpreted
    erroneously as a discontinuity. 1         background temperature, target:
artificial discontinuity standard: See             Apparent ambient temperature of the
    acceptance standard.                           scene behind and surrounding the
artificial discontinuity: Reference point,         instrument, as viewed from the
     such as a hole, groove, implant or
                                                  instrument. \-\'hen the rov of a point
     notch, that are introduced into a
                                                   sensing instrument is larger than the
     reference standard to provide                 target, the target background
     accurately reproducible sensitivity           temperature will affect the instrument
     levels for nondestructive test                reading.3
                                              backscattering, infrared: Reflection of
     equipment. A manufactured material             thermal energy - e.g., generated by
     anomaly. 1                                     the ground and reflecting off the
ASNT: The American Society for                      underside of clouds or inversion
     Nondestructive Testing.                        layers, or unwanted front surface
ASNT Recommended Practice No. SNT-                  reflections from a transparent optical
     TC-lA: Set of guidelines for employers         element.
                                              black body: See blackbod)'.
     to establish and conduct a               blackbody: Hypothetical radiation source
     nondestructive testing personnel              that yields the maximum radiation
     qualification and certification               energy theoretically possible at a given
     program. SNT- TC-lA was first issued in       temperature. A blackbody will absorb
                                                   ail incident radiation falling on it. By
     1968 by the Society for Nondestructive        definition it has an emissivity of 1.0.
     Testing (SNT, now ASNT) and has been          See also emissivit)1• 1
     revised every few years since. 1          bolometer, infrared: Thermal infrared
                                                   detector in which electrical
atmospheric temperature: Temperature               conductivity changes with
     of atmosphere sensed by scanner.              temperature.
                                              borcscope: Industrial mdoscope.
atmospheric windows (infrared):                borescopy: Technology of the borescope
     Spectral intervals ·within the infrared       and its application to 11011destructiw
                                                   testing.
     spectrum in which the atmosphere          burning: Extreme overheating of a metal.
                                                   Makes gralns excessively large and
     transmits radiant energy we1l                 causes the more fusible constituents of
     (atmospheric absorption is a                  steel to melt and run into the grain
     minimum). These are roughly defined           boundaries or it may leave voids
     as 2 to 5 ~m and 8 to 14 pm. 3                between the grains. Steel may be
attenuation: Decrease in signal                    oxidized to the extent that it is no
     magnitude during energy transmission          longer usable and cannot be corrected
     from one point to another. This loss          by heat treating but may he remelted. 1
     may be caused by absorption,
     reflection, scattering of energy or
     other material characteristics or may
     he caused by an electronic or optical
     device sucl1 as an attenuator.1
automated system: Acting mechanism
     that performs required tasks at a
     determined time and in a fixed
     sequence in response to certain
     conditions and instructions. 1
                                              Infrared and Thermal Testing Glossary 681
c                                              certification: Process of providing written
                                                    testimony that an individual is
 calibration: Adjusting an instrument so            qualified. See also crrlifkd. 1
     that its readings agree ·with a
                                               certified: Having written testimo11y ol
        standard.:~                                 qualification. See also certi{ication.J
 calibration accuracy: Accuracy to which       charge coupled device (CCD): Solid state
     a calibration is performed, usually            optical sensor widely used in imaging
     based on the accuracy and sensitivity          inspection systems for its accuracy,
     of the instruments and references used         high speed scanning and long service
     in the calibration.-~                          life. 1 Incoming radiation induces
                                                    electrical charges stored in a
 calibration check: Routine check of an             capacitor-like semiconductor
     instrument against a reference to              structures and later transferred to
     ensure that the instrument has not             ide'rltical neighbor structures, ready for
     deviated from calibration since its last       reading.
     use. 3
                                               closing: In image processing, dilation
calibration reflector: Reflector with a             followed by erosion. A single pixel
     known dimensioned surface                      closing connects a broken feature
     established to provide an accurately           separated by one pixel. 1 See also
     reproducible reference level. 1                matllematical mU!plwlugy and opening.
calibration sourcc1 infrared: Blackbody        code: Standard enacted or enforced as a
     or other target of known temperature           Ia--w. 1
     and effective emissivity used as a
     calibration referencc.3                   coefficient of thermal expansion: Linear
                                                    expansion or contraction per unit
candela: Base unit of measure in SI for             length per degree of temperature
     measuring luminous intensity. The              change between specified lower and
     luminous intensity in a given                  upper tempewture limits. 1
     direction of a source that emits
                                               coefficients of the filter: Values in a
     monochromatic radiation of frequency           mask that serves as a filter in image
     540 x 1012 Hz and that has a radiant           processing. 1
     intensity in that direction of
     1.4641 m\·V·sr1• Symbolized cd.           color: Aspect of visible light sometimes
     Formerly known as candle. 1                    used to identify wavelength or spectral
candle: Former name for candela. I                  band, as in ht'u-culor mdiometry
capacitance, thermal: Amount of heat                (meaning a method that measures in
     that an object can store. The term            two spectral bands); also used
    thermal capacitance is used to describe        conventionally (visual color) as a
     heat capacity in terms of an electrical       means of displaying a thermal image,
     analogy, where loss of heat is                as in color thermogram.3
     analogous to loss of charge on a
     capacitor. Structures with high thermal   colored body: See nunsmybody.
     capacitance change temperature more       complete testing: Testing of an entire
     slowly than those with low thermal
     capacitance.3                                 production lot in a prescribed manner.
capacity, heat: Ability of a material or           Sometimes complete testing entails
     structure to store heat. The product of       the inspection of only the critical
     the specific heat and the density of          regions of a part. One hundred
     the material. This means that denser          percent testing requires the inspection
     materials generally will have higher          of the entire part by prescribed
     heat capacities than porous materials.J       methods. Compare smnpli11g, partiaJ.l
     Heat capacity is the amount of energy     conduction: Heat transfer occurring when
                                                   more energetic particles collide with
    O·m-3-K-1) required to elevate by one          -and thus impart some of their heat
                                                   energy to- adjacent less energetic
    degree a given volume of material.             (slower moving) particles. This action
    Among common materials, 'i\'ater has           is passed on from one atom (or free
    one of the highest heat capacities; air,       electron) to the next in the direction
    one of the lowest.                             of cooler regions. Thus, heat always
casting: Object of shape obtained by               flows from a warmer to a cooler
     solidification of a substance in a mold.      region. 1
CCD: See charge coupled device.                conductivity, thermal (k): Material
celsius (centigrade): Temperature scale            property defining the relative
                                                   capability to carry heat by conduction
   based on 273 K (0 oc ~ +32 °F) as the           in a static temperature gradient.
                                                   Conductivity varies slightly with
    freezing point of ·water and 373 K             temperature in solids and liquids and
                                                   with temperature and pressure in
   (100 oc ~ 212 °F) as the boiling point          gases. It is high for metals (copper has
                                                   a k of 380 \V-nr1·K-1) and low fo1
    of water at standard atmospheric               gases and porous materials (concrete
    pressure. A relative scale related to the      has a k of 1.0 \·V·m-l.K-1).:~
   kelvin scale (0 oc = 273.12 K;
     1 °C ~ 1 K)-'
682 Infrared and Thermal Testing
continuous annealing furnace: Furnace         crack: (1) A break, fissure or rupture,
    in which castings are heat treated, by        usually V shaped and relatively narrow
                                                  and deep. A discontinuity that has a
    being passed through different heat           relatively large cross section in one
    zones kept at constant temperatures. I        direction and a small or negligible
                                                  cross section when viewed in a
continuous casting: Casting technique in          direction perpendicular to the first. 1
    which an ingot, billet, tube or other         (2) Propagating discontinuities caused
    shape is continuously solidified while        by stresses such as heat treating or
    being poured so that its length is not        grinding. Difficult to detect unaided
                                                   because of fineness of line and pattern
    determined by mold dimensions.I               (may have a radial or latticed
contrast: Difference in visibility                appearance). 1
    (brightness, color or temperature)        crater: (1) In machining, a depression in
                                                   the cutting tool face eroded by chip
    between an indication and the                 cont<JCt. (2) In arc or gas fusion
    surrounding surface.1                          welding, a cavity in the weld bead
                                                   surface, typically occurring when the
convection: Type of heat transfer that             heat source is removed and
    takes place in a moving medium and             insufficient fil1er metal is available to
                                                   fill the cavity. 1
    is almost always associated with
    transfer between a solid (surface) and a  C-scan: Data presentation technique
                                                  applied to reflection and transmission
    moving fluid (such as air), whereby            techniques. It yields a
                                                   two-dimensional plan view of the
    energy is transferred from higher              object but no depth indications unless
    temperature sites to lower temperature         special gating procedures arc used. 1
    sites. 3
cooling stresses: Residual stresses           cutoff frequency: Upper or lower
    resulting from nonuniform                      frequency corresponding to the
                                                  spectral response of a filter or
    distribution of temperature during             amplifier, at a specified amount less
    cooling. 1                                    (usually 3 dB power or 6 dB
corrosion: Deterioration of a metal by             voltage/amplitude) than the
    chemical or electrochemical reaction           maximum response.1
    with its environment. Removal of          D
    material by chemical attack, such as
                                              D* (detcctivity star): Detectivity
    the rusting of automobile                      expressed inversely so that higher D*s
    components. 1                                  indicate better performance.
crack, cold: Cracks that occur in a casting       Sensitivity figure of merit of an
                                                   infrared detector. })* is taken at
    after solidification, due to excessive         specific test conditions or chopping
                                                   frequency and information bandwidth
    stress generally resulting from                and displayed as a function of spectral
    nonuniform cooling.1                           wavelength. 3 D* is the detectivity
crack, cooling: Cracks in bars of alloy or         scaled to the unit sensitive detection
                                                   area, with detectivity corresponding to
    tool steels resulting from uneven              the inverse of the nobe equivalent
                                                   flow.
    cooling after heating or hot rolling.
    They are usually deep and He in a         defect: Discontinuity ·whose sin·, shape,
                                                   orientation or location make it
    longitudinal direction, but are usually        detrimental to the useful servke nf its
    not straight.1                                 host object or which exceeds an
crack, grinding: Thermal cracks caused             accept/reject criterion of an applicable
                                                   specification.1 Note that some
    by local overheating of the surface            discontinuities may not affect
    being ground.1                                 :-.erviceability and are therefore not
crack, hot: Cracks that develop before the         defects. 1 Compare dismntinuity and
                                                  i11dicatiou. 1
    casting has completely cooled, as
    contrasted with cold cracks, that         deformation: Change of '>hape under
    develop after solidification. 1 Also           load. 1 See aho creep and elastic
    called Jwt fear.                               de(umwlion.
crack, transverse: Cracks at right angles     delamination: l_aminJI disc011linuity,
    to the length of the test ohject. 1            gener<~lly an area of unbund('d Jay('r;:;
                                                   of matnial.\. 1
crack, weld: Cracks in weld fusion zones
    or adjacent base metal. Usually a result
    of thermal expansion or contraction
    stresses related to temperature changes
    during welding. I
                                              Infrared and Thermal Testing Glossary 683
depth of field: In photography or               discontinuity, artificial: Reference
     thermography, the range of distance            discontinuities such as holes,
                                                    indentations, cracks, grooves or
     over which an imaging system gives             notches that are introduced into a
     satisfactory definition when its lens is       reference standard to provide
                                                    accurately reproducible indications for
     in the best focus for a specific               determining sensitivity levels. 1
     distance. 1
depth of fusion: Depth to which the base        discontinuity, primary processing: In
     metal melted during welding.l                  metals processing, a material anomaly
                                                    produced from the hot or cold
detector, infrared: Transducer element              working of an ingot into forgings, rod
     that converts incoming infrared                and bar. 1
     radiant energy impinging on its            discontinuity, service induced: I\•laterial
                                                    anomaly caused by the intended use
     sensitive surface to a usehli electrical       of the part.'
     signal. 3
diffuse reflector: Surface that reflects a      display resolution, thermal: Precision
     portion of the incident radiation in           with which an instrument displays its
                                                    assigned measurement parameter
     such a manner that the reflected               (temperature), usually expressed_ in
                                                    degrees, tenths of degrees, hundredths
     radiation is equal in all directions. A        of degrees and so forth.J
     mirror is not a diffuse reflector.::~
diffusion, heat: See thermal diffusion.         dissipation: Generation of heat by plastic
diffusion, mass: Process by which                   deformation.
     molecules intermingle as a result of       distal: In a manipulative or interrogating
    concentration gradients or thermal              system, of or pertaining to the end
    motion. 1 Spreading of a gas through            opposite from the eyepiece and
    other gases "\Vithin a volume.                  farthest from the person using the
                                                    system. Objective; tip. 1
diffusivity, thermal: See thermal
    dif{usivity.                                E
dilation: In image processing, the              effective emissivity (e*): Measured
    condition of a binary image where the           emissivity value of a particular surface
    pixel in the output image is a 1 if any         under existing measurement
    of its eight closest neighbors is a 1 in        conditions (rather than the generic
                                                    tabulated value for the surface
    the input image. See also closing,              material) that can be used to correct a
    erosion, mathematical morphology and            specific measuring instrument to
     opeHing. 1                                     provide a correct temperature
directional properties, material:                   measurement.3
     Properties whose magnitudes depend         cffusivity, thermal: Ability of heat to
    on the relation of the test axis to the         escape from a body, expressed as a
                                                    characteristic of that body.~ Square
    specific direction in the metal,                root of the product of thermal
     resulting from preferred orientation or        conductivity, mass density and specific
                                                    heat.
     from fibering in the structure. See
    anisolropy. 1                               elasticity: Ability of a material to resume
directional properties, radiation:                  its former shape after deformation. 1
    Radiation properties (emissivity,
                                                electric arc \\'elding: Joining of metals by
    absorptivity, reflectivity) as referenced       heating with electric arc. Also called
    to a particular direction. See also              arc weldi11g. 1
     llemispllerical properties, radiatio11. 1
direct viewing: Viewing of a test object in     electromagnetic interference: Sec
                                                    EMI!RFI noise.
    the viewer's immediate presence. The
                                                EMI/RFI noise: Disturbances to electrical
    term direct viewing is used in the fields       signals caused by electromagnetic
    of robotics and surveillance to                 interference (EtvH) or radio frequency
                                                    interference {RFI). In thermography,
    distinguish conventional from remote            this may cause noise patterns to
    viewing. 1                                      appear on the display:{
discernible image: Image capable of
    being recognized by sight without the
    aid of magnification. I
discontinuity: Intentional or
    unintentional interruption in the
    physical structure or configuration of a
    part.IA After nondestructive testing,
    unintentional discontinuities
    interpreted as detrimental in the host
    object may be called flaws or de{ect~.
    Compare defiYl, dislocalion and
     indication. 1
684 Infrared and Thermal Testing
emissivity: Variable ratio of the total       external discontinuities: Discontinuities
    energy radiated by a given surface at a       on the outside or exposed surface of a
                                                  test object. 1
    given temperature to the total energy
    radiated by a blackbody at the same       F
    temperature. Emissivity can be total,
    directional or hemispherical. EmissivHy   fahrenheit: Temperature scale based on
    is a surface phenomenon depending             32 oF as the freezing point of water
    on surface condition and composition.         and 212 °F as the boiling point of
                                                  water at standard atmospheric
    Smooth materials have lower                   pressurei a relative scale related to the
    emissivities than rough or corroded           rankine scale 10 oF= 459.67 R; 1 °F
    materials. 1 Emissivity values range           (DT) ~ 1 R (DT)] 3
    between 0 for a perfect reflector to 1.0
                                              false indication: Test indication that
    for a blackbody.                              could be interpreted as originating
                                                   from a discon.tinuity but which
endoscope: Device for vle\ving the                 actually originates ·where no
    interior of objects. From the Greek            discontinuity exists. 1 Distinct from
    vwrds for inside view, the term                nonrelevant indication.1 Compare
    endoscope is used mainly for medical           de(ect. 1
    instruments. Nearly every medical
    endoscope has an integral light source;   feature extraction: From an enhanced
                                                   image, derivation of some feature
    many incorporate surgical tweezers or         values, usually parameters for
    other devices. Compare borescope. 1            distinguishing objects in the image. I
environmental rating: Rating given an
    operating unit (typically an electrical   fiber optic, infrared: Flexible fiber made
                                                   of a material that transmits infrared
    or mechanical enclosure) to indicate           energy, used for making noncontact
    the limits of the environmental                temperature measurements when
                                                   there is not a direct line of sight
    conditions under which the unit will           between the instrument and the
    function reliably and within published         target.3
    performance specifications.3
                                              fiber optics: Technology of light
erosion: (1) Loss of material or                   transmission through fibers such as
    degradation of surface quality through         plastic, glass or quartz.I
    friction or abrasion from moving          field: In video teclmology, one of two
    fluids, made worse by solid particles ln       video picture components that
                                                   together make <J frame. Each picture is
    those fluids or by cavitation in the          divided into two parts called fields
    moving fluid. (2) In image processing,         because a frame at the rate of thirty
                                                   frames per secoi1d in a standard video
    condition of a binary image where the          output would otherwise produce a
    pixel in the output image is a 1 if each       flicker discernible to the eye. Each
                                                   field contains one half of the total
    of its eight neighbors is a 1 in the           picture elements. Two fields are
    input image. See also closing, dilation,       required to produce one complete
    mathematical morphology and openins. 1        visible light picture or frame so the
eutectic liquid: Liquid having a                   field frequency is sixty fields per
     proportion of metals such that two or         second and the frame frequency is
                                                   thirty frames per second. 1 In infrared
    more solid phases form at the same             technology there can be four fields.
     temperature during coo1ing.l             field of vie·w: Range or area where things
eutectic point: Temperature and                    can be seen through an imaging
                                                   system, lens or aperture.1 Angular
     proportion of metals· at which two or         subtcnse (expressed in angular degrees
                                                   or radians per side if rectangular, and
     more phases of a eutectic liquid form.        angular degrees or radians if circular)
    Compare eutectoid. 1                           over which an instrument wiJl
eutectoid: Similar to eutectic but in a            integrate all incoming radiant energy.
     solid system during cooling. 1                In a radiation thermometer, the field of
evaluation: Process of determining the             l'iew is the target spot size; in a
                                                   scanner or imager the field ofview is
     magnitude and significance of a               the scan angle or picture size or total
     discontinuity after the indication has        field of view (TI;OV).3 Compare depth
                                                   o f field.
     been interpreted as relevant.
     Evaluation determines if the test
     object should be rejected, repaired or
    accepted. See indication and
    inteJpretati011. 1
examination: Process of testing materials,
     interpreting and evaluating test
     indications to determine if the test
     object meets specified acceptance
     criteria. 1
exfoliation: Corrosion that progresses
     approximately parallel to the outer
     surface of the metal, causing layers of
     the metal to be elevated by the
     formation of corrosion product. 1
exitance, radiant: See mdiosity.
                                              Infrared and Thermal Testing Glossary 685