various thermocouples in sequence. All of     thermocouple type by simply changing
the volt meter and scanner wires arc          gain resistors.
copper, independent of the type of
thermocouple chosen. In fact, as long as          The advantage of the hardware
each thermocouple is known,                   compcmation circuit or electronic ice
thermocouple types can he mixed on the        point reference is that either reference
same isothermal junction block (often         ohviates computation of the reference
called a zone box) and the appropriate        temperature. This saves two computation
modifications in software can be made.        steps and makes a hardware
The junction hlock temperature sensor RT      compensation temperature measurement
is located at the center of the block to      somewhat faster than a software
minimize errors from thermal gradients.       compensation measurement. However,
                                              faster microprocessors and advanced data
   Software compensation is the most          acquisition designs have blurred the line
versatile technique for measuring             between the two techniques, with
thermocouples. Many thermocouples are         software compensation speeds challenging
connected on the same block, copper
leads are used throughout the scanner and     FIGURE 13. Equivalent circuits illustrate
the technique is independent of the types     hardware compensation: (a) circuit with
of thermocouples chosen. In addition,         battery insertedi (b) circuit with ice bathi
when using a data acquisition system          (c) diagram of equivalent circuit, showing
with a built~in zone box, the                 compensation voltage e.
thermocouple is simply connected as a
pair of test leads would be. All of the       (a}
conversions are performed by the
instrument software. The one
disadvantage is that it requires a small
amount of additional time to calculate the
reference junction temperature. For
maximum speed hardware compensation
can be used instead.
Hardware Compensation                         (b)
Rather than measuring the temperature of           + o-'C:"u'--j,  Fe
the reference junction and computing its
equivalent voltage as with software                 ,, I               T
compensation, a battery could be inserted
to cancel the offset voltage of the                1\-~1 Fe Cn
reference junction. The combination of                     I...----+-+--~
this hardware compensation voltage and
the reference junction voltage is equal to                          Ice bath at 273 K (0 oc = 32 °f-)
that of a 273 K (0 oc ~ 32 °F) junction       (c)
(Fig. 13).
                                              legend
   The compensation voltage e is a
function of the temperature sensing             Cn = constantan resistance alloy (50 to 65 percent
resistor, RT. The voltage F is now                       copper, 35 to 50 pNcent nickel)
referenced to 273 K (0 °C ~ 32 °F) and
may be read directly and converted to           Cu = copper
temperature by using tables from the             e = compensation voltage (V)
National Institute of Standards and
Technology.                                     Fe = iron
                                                 R1 = resistance measurement (0)
   Another name for this circuit is the          T = electrical terminal
electronic ice point.6 These circuits are         V = voltage 01)
commercially available for use with any
volt meter and with a \Vide variety of
thermocouples. The major drawback is
that a unique ice point reference circuit is
usually needed for each individual
thermocouple type.
   Figure 14 shows a practical ice point
referencE' circuil that can be used in
con junction with a relay scanner to
compensate an entire block of
thermocouple inputs. All the
thermocouples in the block must be of
the same type but each block of inputs
can accommodate a different
236 Infrared and Thermal Testing
those of hardware compensation in                             accurate direct readout of temperature,
              practical applications (Table 4).                             That is, the temperature display involves
                                                                            only a scale factor.
              Voltage-to-Temperature
              Conversion                                                       By examining the variations in the
                                                                            thermoelectric coefficient, it can easily be
              Hardware and software compensation has                        seen that using one consttmt scale factor
              been used to synthesize an ice point                          would limit the temperature range of the
              reference. Now all that is necessary is to                    system and restrict tlw system accmacy.
              read the digital volt meter and convert                       Better conversion accuracy can be
              the voltage reading to a temperature.                         obtained by reading the volt meter and
              Unfortunately, a thermocouples                                consulting the thermocouple tables of the
              relationship of temperature versus voltage                    National Institute of Standards and
              is nOt linear. Output voltages for some                       Technology. 4•5
              popular thermocouples are plotted as a
              function of temperature in Fig. 15. If the                       These lookup table values could he
              slope of the curve (the thermoelectric                        stored in a computer but they would
              coefficient) is plotted versus temperature,                   consume an inordinate amount of
              as in Fig. 16, it becomes quite obvious                       memory. A more practical approach is to
              that the thermocouple is a nonlinear                          approximate the table values using a
              device.                                                       power series polynomial:
                 A horizontal line in Fig. 16 would                         (7) r0 + c1x + r2 x2
              indicate a constant slope a and hence a                                      + ({-\.} + ... + cll;e'
              linear device. The slope of the type K
              thermocouple approaches a constant over                       FIGURE 15. Thermocouple temperature versus voltage.
              a temperature range from 273 to 1273 K
              (0 "C to 1000 "C; 32 "F to 1832 "F).
              Consequently the type K can be used with
              a multiplying volt meter and an external
              ice point reference to obtain a moderately
fiGURE 14. Practical hardware compensation.
                        Cu                   Fe
                               Cu            Cn
                       Ru
                   Cu
Volt meter I
                                                               Integrated   0  773    1273         1773             2273                   2773
                                                               temperature
                                                               sensor          (500)  (1000) (1500) (2000) (2500)
legend                                                                         [932)  [1832) [2732) [3632) {4532]
 Cn =constantan resistance aHoy (50 to 65 percent copper, 35 to                                          Temperature K C'C) [0 F}
        50 pNcent nkke!)
                                                                            legend
 Cu =copper
  Fe= iron                                                                    E =chrome!(+) versus constantan (coppl:'r nickel alloy)(-)
                                                                               J-= iron(+) versus constantan (copper nickel alloy){-)
    i =electrical current (A)                                                 K ~ chromel (+)versus alumel (-)
                                                                              R =platinum (+)versus platinum with 13 percent rhodium(-)
   J = electrical junction                                                    S "'platinum(+) versus platinum with 10 percent rhodiwn (-)
                                                                              T =-copper (-t) versus const;mtan copper nickel alloy,(-)
  RH := hardware compensation resistance
   V"' voltage Cl)
TABlE 4. Hardware compensation versus software compensation.
Compensation           Speed                     Versatility                   Configuration Ease
Hardware      fast                    one themocoup!e type                  hard to reconfigure- requires hardware
Software                                 per reference junction               change for new thermocouple type
              requires more software
                manipulation time     versatile - accepts                   easy to reconfigure
                                        any thermocouple
                                                                            Contact Sensors for Thermal Testing and Monitoring 237
where c = polynomial coefficients unique        higher system speed. ·nthle S is an
                                                                  example of the polynomials used in
                     to each thermocouple; 11 = maximum           conjunction with software compensation
                     order of polynomial; T90 = temperature       fw a data acquisition sy~tem. Rather than
                                                                  directly calculating tile exponentials, the
                  (kelvin); and x = thermocouple voltage          software is programmed to use the nested
                                                                  polynomial form to save execution time.
                     (volt).                                      The polynomial fit rapidly degrades
                        As the polynomialn increases/ the         outside the temperature wnge shown in
                                                                  TableS and should not be extrapolated
                     accuracy of the polynomial improves.         outside those limits.
                     Lower order polynomials may lJe used
                    over a narrow temperature range to obtain        Table 5 uses the temperature
                                                                  conversion equation:
FIGURE 16. Thermoelectric coefficient versus temperature.
                                                                  (8) T90  Co + c1.\ + C2X?
                                                                           + C;~X3 + ... + Cg;\'9
1                                                                 and the following form for a nested
>                                                                 polynomial (fourth order example):
3                                                                    The calculation of high order
                                                                  polynomials is time consuming, even for
~c                                                                today's high powered microprocessors. As
                                                                  mentioned above, time can be saved by
.~                                                                using a lower order polynomial for a
                                                                  smaller temperature range. In the software
~ 4o I-.ffli---.!:=-1-'='f----t:                                  for one data acquisition system, the
                                                                  thermocouple characteristic curve is
 0                                                                divided into eight sectors and each sector
 u                                                                is approximated by a third order
                                                                  polynomial (i'ig. 17).
~
                                                                     The data acquisition system measures
 ~                                                                the output voltage, categorizes it into one
                                                                  of the eight sectors and chooses the
.0                                                                appropriate coefficients for that sector.
                                                                  This technique is both faster and more
 ~                                                                accur<lte than the higher order
                                                                  polynomial.
~
                                                                      An even faster algorithm is used in
            0  773    1273              1773    2273              many new data acquisition systems. Using
               (500)  (1000) (1500) (2000)
               ]932]  [1832] [2732]             [3632J
legend
   E = chrome!(+) versus constantan (copper nickel alloy)(-)
   J = iron(+) versus constantan (copper nickel alloy)(-)
  K = chrome!(+) versus a!umel (-}
  R = platinum(+) versus platinum with 13 percent rhodium(-)
  S = platinum(+) versus platinum with 10 percent rhodium(-)
  T =copper(+) versus constantan (copper nickel alloy)(-)
TABLE 5. NIST ITS-90 polynomial coefficients.'
                      Thermocouple Type J                                  Thermocouple Type K
               --~673~to~2~73~K----           273to1033K            7=3~t-o~2=7~3~K~-        273 to 773 K
                     (-210 to 0 'C;              (0 to 760 'C;        (-200 to 0 'C;         (0 to 500 'C;
                                                                    -328 'F to +32 'F)       32 to 932 'F)
                 -346 'F to +32 'F)             32 to 1400 'F)
Polynomial                                                          ±0.04 K (0.04 'C = 0,07 'F) ±0.05 K (0.05 'C = 0.09 'F)
   Order    ±0.05 K (0.05 'C =0.09 'F)  ±0.04 K (0.04 'C =O.o7 'F)
                                                                    Eighth Order                   Ninth Order
                    Eighth Order               Seventh Order
Co 0 0 0 0
c,             -1.9528268 X lQ-2              -1.978425 X 10-2      -2.5173462 x 1o-2   -2.508355 X 10-2
c,             -1.2286185 X lQ-6              -2.001204 X 10-7      -1.1662878 x 1o-6   -7.860106 X 10---8
(3             -1.0752178 X lQ-9              -1.036969 X lQ-11     -1.0833638 X 10·9   -2.503131 X 10-10
(4             -5.9086933 X 1Q-13             -2.549687 X 10-1 6    -8.9773540 X lQ-13  -8.315270 X lQ-14
w-c,                                                                -3.7342377 X lQ-16
               -1.7256713 x 16                -3.585153 X 10-21                         -1.228034 X 1Q-1
c,             -2.8131513 X 10-20             -5.344285 X 1Q-26     -8.6632643 x 1o-2o  -9.804036 X 10-2.?
c,             -2.3963370 X lQ-24             -5.099890 X l0-31     -1.0450598 X 1Q-23  -4.413030 X 10-2(,
c, -8.3823321 x 1o- 29                                              -5.1920577 x w-28   -·1.057734 X lQ-30
c, -1.052755 X 10-35
238 Infrared and Thermal Testing
many more sectors ahd a series of first            to solve unique measurement problems.
              order equations, they can make hundreds,           Idiosyncrasies of the more common
              even thousands, of internal calculations           thermocouples are discussed here.
              per second.
                                                                    The term stnndard wire error refers to
                 All the foregoing procedures assume             the common commercial specifications
              the thermocouple voltage can be                    published by the American Society of
              measured accurately and easily; however,           Testing and lvfaterialsFJ The standard
              requirements of the system volt meter              wire error represents the allowable
              {Table 6) show that thermocouple output            deviation between the actual
              voltages are very small.                           thermocouple output voltage and the
                                                                 voltage predicted by tables published by
                 Even for the common type K                      the National Institute of Standards and
              thermocouple, the volt meter must be               Technology:t
              able to resolve 4 pV to detect a 0.1 K
              (0.1 "C ~ 0.18 "F) change. This demands            Noble Metal Thermocouples
              both excellent resolution (the more bits,          The noble metal thermocouples, types B,
              the better) and measurement accuracy               R and S, are CJII platinum or platinum
              from the digital multimeter. The                   rhodium thermocouples and hence share
              magnitude of this signal is an open                many of the same characteristics.
              invitation for noise to creep into any
              system. For this reason instrument                 Diffusion. Tvfetallir vapor diffusion at high
              designers use several fundamental noise            temperatures can readily change the
              rejection techniques, including tree               platinum wire calibration, hence platinum
              switching, normal mode filtering,                  wires should only be used inside a
              integration and isolation.                         nonmetallic sheath such as high purity
                                                                 alumina. The one exception to this rule is
              Thermocouple                                       prohibitively expensive- a sheath made
              Characteristics                                    of platinum.
              Over the years specific pairs of                   Stability. The platinum based couples are
              thermocouple alloys have been developed            by far the most stable of all the common
                                                                 thermocouples. Type S is so stable that it
FIGURE 17. junction voltage cancellation: V1 :::: V if V3 = V4.  is specified as the standard for
Curve divided into sectors for polynomial calculation.           temperature calibration between the
Ta = bx + cx2 + dx3.                                             antimony point, 903.89 K (630.74 "C ~
                                                                 1167.33 "F), and the gold point,
I                                           I                    1337.58 K (1064.43 "C ~ 1947.97 °F).
I                                       ·-~~                     Type B. The type B thermocouple i~ the
                                                                 only common thermocouple that exhibits
I                                               I                a double-valued ambiguity (Fig. 18).
II                                              I                Because of the double-valued curve and
r----,--, - · r                                 I                the extremely low thermoelectric
                                                                 coefficient at lmv temperatures, type B is
III                                         I                    virtually useless below 323 K
II                                                               (50 "C ~ 122 "1'). Hecause the output is
I                                                                nearly zero from 273 K (0 "C ~ 32 "I') to
                                                                 315 K (42 "C ~ 108 "F), type B has the
              Voltage (relative scale)                           unique advantage that the reference
                                                                 fiGURE 18. Double valued ambiguity of
                                                                 type B thermocouple.
TABlE 6. Required sensitivity for digital volt meter.
Thermocouple      Seebeck         Digital Volt
      Type                     Meter Sensitivity
                Coefficient
                                    for 0.1 K
                 at 278 K      (0.1 °Co0.18°F)
              (25 oc 0 77 °F)             (~V)
                   (~V-K- 1 )
E 61                                    6.1                      273 31S
                                        5.2                      (0) (42)
I 52                                    4.0                      132) 1108)
                                        0.6
K 40                                    0.6                           Temperature, K (0 C) [°FJ
                                        4.1
R6
s6
T 41
                                                                 Contact Sensors for Thermal Testing and Monitoring 239
junction temperature is almost               Types K and N. Type K has long been a
immaterial, as long as it is het\veen 273 K  popular thermocouple. It is especially
                                             suited to high temperature applications
(0 'C =32 'F) and 313 K (40 'C = 104 'F).    lJecaus.e of its reslstance to oxidation.
Of course, the measurillg jundioll              The type N thermocouple is gaining
temperature is typically very high.          popularity tiS a replacement for type K. It
                                             has a slightly lower output (smaller
Base Metal Thermocouples                     thermoelectric coefficient) than type K
                                             but an even higher resistance to
Unlike the noble metal thermocouples,        oxidation. The type N thermocouple
the base metal couples have no specified     output curve depends on wire size and
chemical composition. Any combination        there are two distinct nicrosil/nisil
of metals may be used that results in a      characteristic curves, the differences being
voltage-versus-temperature curve fit that    wire size and temperature range. 10 (The
is within the standard wire errors. This     term nisi/ refers to a nickel chrome
leads to some rather interesting metal       thermal alloy; nicrosil, to a nickel silicone
combinations. Constantan, for example, is    thermal alloy. These alloys are used to
not a specific metal alloy at all but a      measure high temperatures and exhibit
generic name for a whole series of copper    inconsistencies in thermoelectric voltage
nickel alloys. Incredibly, the constantan    in wire gages.)
used in a type T (copper constantan)
thermocouple is not the same as the          Tungsten. There arc three common types
                                             of tungsten thermocouples (Table 7). All
constantan used in the type 1 (iron          are alloyed with rhenium to make the
                                             metal more malleable. Tungsten
constantan) thermocouple:"                   thermocouples are used for measuring
                                             very high temperatures in either a
Type E. Although type E standard wire        vacuum or an inert atmosphere.
errors are not specified below 273 K
(0 'C = 32 'F), the type E thermocouple is   Practical Thermocouple
ideally suited for low temperature           Measurements
measurements because of its high
thermoelectric coefficient (58 V·K-1), low   Noise Rejection
thermal conductivity and high corrosion
resistance.                                  Tree Switching. Tree switching is a
                                             technique for organizing the channels of
   The thermoelectric coefficient for type   a scanner into groups, each lvith its own
E is greater than all other standard         main switch.
couples, which makes it useful for
detecting small temperature changes.             \-\'ithout tree switching, every channel
                                             can contribute noise directly through its
Type J. Iron, the positive element in a      stray capacitance. \'\1ith tree switching,
J thermocouple is an inexpensive metal       groups of parallel channel capacitance~
                                             are in series with a single tree switch
rarely manufactured in pure form.            capacitance. The result is greatly reduced
                                             crosstalk in a large data acquisition
J thermocouples arc subject to poor          system, because of the reduced
                                             interchannel capacitance {Fig. 19).
conformance characteristics because of
                                             Analog Filter. A filter may be used dir<.."rt!y
impurities in the iron. Even so, the J       at the input of a volt meter to reduce
thermocouple is popular because of its       TABLE 7. Percentage of rhenium in
high thermoelectric coefficient and lm\'     tungsten terminals. Tungsten
price.                                       thermocouples are used for measuring
                                             very high temperatures in either vacuum
   The 1 thermocouple should never be        or inert atmosphere.
used above 1033 K (760 'C = 1400 °F)         Type     Rhenium (percent)
because an abrupt magnetic
transformation can cause decalibration       Type c~  5 versus 26
even when returned to lower                  Type o~  3 versus 25
temperatures.                                Type GJ  0 versus 26
Type T. This is the only thermocouple        a. Not symbols of Amercan National Standard~
with published standard wire errors for         Institute.
the temperature region below 273 K
(0 oc ~ 32 °F); however, type E is actually
more suitable at very low temperatures
because of its higher thermoelectric
coefficient and lower thermal
conductivity.
    'l)rpe T has the unique distinction of
having one copper lead. Thh can be nn
advantage in a specialized monitoring
situation ·where a temperatme difference
is t~ll that is desired.
    The advantt~ge is that the copper
thermocouple leads are the same metal as
the digital volt meter terminals, making
lead compensation unnecessary.
240 Infrared and T/lermal Testing
noise. It reduces interference dramatically                                 analog-to-digital converter to measure the
but causes the volt meter to respond more                                   thermocouple voltage. Integration is an
slowly to step inputs (l'ig. 20).                                           especially attractive analog-to-digital
                                                                            technique in light of recent innovations
Integration. Integration is an                                              have brought the cost in line with
analog-to-digital technique that                                            historically less expensive
essentially averages noise over a full line                                 analog-to-digital lt'chnologies.
cycle- thus pmver line related noise and                                    Isolation. A noise source common to both
its harmonics are virtually eliminated. lf                                  high and low measurement leads is called
the integration period is chosen to be less                                 common mode noise. Isolated inputs help
than an integer line cycle, its noise                                       to reduce this noise as well as protect the
rejection properties are essentially                                        measurement system from ground loops
negated.                                                                    and transients (Fig. 21).
   Because thermocouple drcuHs that                                             A thermocouple wire may he pulled
cover long distances are especially                                         through the same conduit as a 220 V
susceptible to power line related noise, it                                 alternating current supply line. The
is advisable to use nn integrating                                          capacitance between the power lines and
                                                                            the thermocouple lines will create an
FIGURE 19. Tree switching: (a) circuit before                               alternating current signal of
tree sWitching; (b) stray capacitance reduced                               approximately equal magnitude on both
nearly 20:1 by leaving tree switch 2 open;                                  thermocouple wires. This is not a problem
(c) approximately equivalent circuit.                                       in an ideal circuit but the volt meter is
                                                                            not ideal. It has some capacitance
(a)                                                                         between its low terminal and safety
                                                                            ground (earth). Current flows through
                                                                  Digital   this capacitance and through the
                                                                      volt  thermocouple lead resistance, creating a
                                                                            normal mode signal that appears as
                                                       TSl meter            measurement error.
                           (20 channels)                                        This error is reduced by isolating the
                                                                            input terminals from safety ground with a
sNouorcel;e~·~~~~                       TS2                                 careful design that minimizes the low
                                                                            earth capacitance. Nonisolated or ground
                     Next 20 channels  c                                    referenced inputs (single ended inputs are
                                       Digital                              FIGURE 20. Analog filter.
                                        volt
J-"'""(b)                                                                    Legend
l~T+~'f92'"'0-CJHC                     0                                      t "' time (s)
                                                                              I' = voltage (V)
                                       High
 Noise
source
~ i(b) r-:----~D~-~~;\''_j_-:.         meter
T~~g~~f---                             .
Noise                                  "'9"
source
Legend                                                                      Distributed
                                                                             resistJnce
   C = channel
  TS = tree ~witch                                                                                                         Digital
                                                                                                                         volt meter
                                                                            Contact Sensors tor Thermal Testing and Monitoring 241
often ground referenced) do not have the       square common mode noise source. They
                                               must withstand a peak offset of ±170 V
ability to reject common mode noise.           from ground and still make accurate
Instead, the common mode current flows         measurements. An isolated system with
through the !v\; !cad directly to ground,      electronic FET switches typically can only
                                               handle ±12 V of offset from earth; if used
causing potentially large reading errors.      in this application, the inputs would be
   Isolated inputs are particularly useful in  damaged.
eliminating ground loops created when             The solution is to use commercially
the thermocouple junction comes into           available external signal conditioning
                                               (isolation transformers and amplifiers)
direct contact lvith a common mode noise       that buffer the inputs and reject the
source.                                        common mode voltage. Another easy
                                               alternative is to use a data acquisition
   In Hg. 22 the temperature is measured       system that can float several hundred
at the center of a molten metal bath that      volts.
is being heated by electric current. The
                                                   Notice that the noise can also be
potential at the center of the bath is         minimized by minimizing series resistance
120 V root mean square. The equivalent         R5• This minimizing can be done by using
circuit is shown in Fig. 23.                   larger thermocouple wire that has a
                                               smaller series resistance. Also, to reduce
    Isolated inputs reject the noise current   the possibility of magnetically induced
                                               noise, the thermocouple should be
by maintaining a high impedance                twisted in a uniform manner.
between low and earth. A nonisolatcd           Thermocouple extension wires are
system (Fig. 24) completes the path to         available commercially in a twisted pair
earth and results in a ground loop. The        configuration.
resulting currents can be dangerously          Practical Precautions
high and can be harmful to both                The following concepts have been
instrument and operator. Isolated inputs       discussed: (1) the reference junction,
                                               (2) how to use a polynomial to extract
are required for making measurements           absolute temperature data and (3) what to
with high common mode noise.                   look for in a data acquisition system to
                                               minimize the effects of noise. Now it is
   Sometimes having isolated inputs is         useful to consider the thermocouple wire
not enough. In Fig. 23, the volt meter         itself. The polynomial curve fit relies on
inputs are floating on a 120 V root mean       the thermocouple wire being perfect; that
                                               is, it must not become decalibrated during
FIGURE 22. Measurement of temperature and      the act of measuring temperature.
center of molten metal bath heated by
electric current.                                 The pitfalls of thermocouple
                                               thermometry deserve consideration. Aside
         240Y                     ~            from the specified accuracies of the data
          root                                 acquisition system and its isothermal
         mean                                  reference junction, most measurement
         square                                error may be traced to one of these
                                               primary sources: (1) poor junction
]II      v~ ,'o-
                                               FIGURE 24. Nonisolated system completes
FIGURE 23. Inputs floating on 120 V root       the path to earth, resulting in a ground
                                               loop.
mean square common mode noise source
must withstand peak offset of ±170 V from
ground and still make accurate
measurements.
120V               Series         High                         Series    High
   root                           low                        resistance  low
         ,-------------,
 mean                                          l20V    Nolse current
square   ':'''' ~------J'''''                    root
         '
                                                mean
              Noise current                    square
242 Infrared and Thermal Testing
connection, (2) decalibration of                                  unintentionally altering the physical
thermocouple wire, (3) shunt impedance                            makeup of the thermocouple wire so that
and galvanic action, (4) thermal shunting,                        it no longer conforms to the National
(5) noise and leakage currents,                                   Institute of Standards and Technology
(6) thermocouple specifications and                               polynomial within specified limits.
(7) documentation.                                                Decalibration can result from diffusion of
                                                                  atmospheric particles into the metal,
Poor junction Connection                                          caused by temperature extremes. It can be
                                                                  caused by high temperature annealing or
There arc a number of acceptable ways to                          by cold working the metal, an effect that
connect two thermocouple wires,                                   can occur when the wire is drawn
especially soldering, silver soldering and                        through a conduit or strained by rough
welding. When the thermocouple wires                              handling or vibration. Annealing can
arc soldered together, a third metal is                           occur within the section of wire that
introduced into the thermocouple circuit.                         undergoes a temperature gradient.
As long as the temperatures on both sides
of the thermocouple are the same, the                                Robert J. Moffat explains that the
solder should not introduce an error. The
solder does limit the maximum                                     thermocouple voltage is actually
temperature to which this junction can be                         generated by the section of wire that
subjected (Fig. 25). To reach a high                              contains a temperature gradient- and
measurement temperature, the joint must                           not necessarily by the junction .12 For
be welded. But welding is not a process to                        example, if a thermal probe is in a molten
be taken lightly. 11 Overheating can                              metal bath, there will be t"wo regions that
degrade the wire; the welding gas and the                         are virtually isothermal and one that has a
atmosphere in which the wire is welded                            large gradient.
can both diffuse into the thermocouple
metal, changing its characteristics. The                              In Fig. 26, the thermocouple junction
difficulty is compounded by the very                              will not produce any part of the output
different nature of the two metals being                          voltage. The shaded section will produce
joined. Commercial thermocouples are                              virtually the entire thermocouple output
welded on expensive machinery using a                             voltage. If, because of aging or annealing,
capacitive discharge technique to ensure                          the output of this thermocouple were
uniformity.                                                       found to be drifting, then replacing only
                                                                  the thermocouple junction would not
    A poor weld can, of course, result in an                      solve the problem. The entire shaded
open connection, which can be detected                            section would have to be replaced because
in a measurement situation by performing                          it is the source of the thermocouple
an open thermocouple check. This is a                             voltage.
common test function available with
many data loggers and data acquisition                               Thermocouple wire obviously cannot
systems.                                                          be manufactured perfectly; there will be
                                                                  some discontinuities that will cause
Decalibration                                                     output voltage errors. These
                                                                  heterogeneities can be especially
Decalibration is a far more serious fault                         disruptive if they occur in a region of
condition than the open thermocouple                              steep temperature gradient.
because it can result in a temperature
reading that appears to be correct.                               FIGURE 26. Gradient produces voltage.
Decalibration describes the process of
fiGURE 25. Soldering of thermocouple point                        ! ! 1-;:: 473 K (200 "C = 392 ~F)
(lead, tin). junctions of iron to lead and of                                                  ~ 573 K (300 "C "'572 "F)
tin to constantan approximate that of iron                        - -~I I ---· 673 K(400 "C"'" 752 "F)
to constantan.                                                    - --    773 K(5 00 "C "'932 GF}
                       Fe                                         - -- -
                    Cn                                            Metal bath of 773 K (500 "C == 932 or)
                                                 Solder (Pb, Sn)
  legend
    Cn = constantan resistance alloy (50 to 65 percent
            copper, 35' to 50 percent nickel}
     Fe= iron
     Pb = lead
     5n= tin
                                                                  Contact Sensors for Thermal Testing and Monitoring 243
Because it is not known when.:'·<m           deviate from the published values. \'\1hen
imperfection will occur within a wire, the       using thermocouples at high
                                                 temperatures, the insulation should be
best thing is to avoid creating a steep          chosen carefully. Atmospheric cffecb can
                                                 be minimized by choosing the proper
gradient. Gradients can be reduced by            protective metallic or ceramic sheath.
using metallic sleeving or by careful
placement of the thermocouple wire.              Galvanic Action
Shunt Impedance                                  The dyes used in some thermocouple
                                                 insulation form an electrolyte in the
High temperatures can also take their toll       presence of water. This creates a galvanic
on thermocouple wire insulators.                 action, with a resultant output hundreds
Insulation resistance decreases                  of times greater than the thermoelectric
exponentially with increasing                    effect. Precautions should be taken to
temperature, even to the point that it           shield the thermocouple wires from all
creates a virtual junction. Assume a             harsh atmospheres and liquids.
completely open thermocouple operating
at a high temperature (Fig. 27).                 Thermal Shunting
   The leakage resistance RL can be              No thermocouple can be made without
sufficiently low to complete the circuit         mass. Because it takes energy to heat any
path and give an improper voltage                mass, the thermocouple will slightly alter
reading. Now assume that the                     the temperature it was meant to measure.
thermocouple is not open but a very long         If the mass to be measured is small. the
section of snwll diameter wire is being          thermocouple must naturally be small.
used (Fig. 28).                                  Hut a thermocouple made with small wire
                                                 is far more susceptible to the problems of
   If the thermocouple wire is small, its        contamination, annealing, strain and
series resistance Rs will be quite high and      shunt impedance. 13 To minimize these
under extreme conditions Rt. << Rs This          effects, thermocouple extension wire can
means that the thermocouple junction             be used. Extension ·wire is commercially
will appear to be at Rt and the output will      available wire primarily intended to cover
be proportional to T1 , not T2 .                 long distances between the measuring
                                                 thermocouple and the volt meter.
   High temperatures have other
detrimental effects on thermocouple wire.           Extension wire is made of metals
The impurities and chemicals within the          having thermoelectric coefficients very
insulation can actually diffuse into the         similar to a particular thermocouple type.
thermocouple metal and cause the                 It is generally larger in size so that its
dependence of voltage on temperature to          series resistance does not become a factor
                                                 when traversing long distances. It can also
FIGURE 27. Leakage resistance.                   be pulled more readily through conduit
                                                 than very small thermocouple wire. It
                                           Open  generally is specified over a much lower
                                                 temperature range than premium grade
                 1-                              thermocouple ·wire. In addition to offering
                                                 a practical size advantage, extension wire
 To digital volt meter                           is Jess expensive than standard
                                                 thermocouple wire, especially in the case
legend                                           of platinum based thermocouples.
   Rl"' leakage resistance                          Because the extension wire is specified
   T ==electrical terminal                       over a narrower temperature range and is
                                                 more likely to receive mechanical stress,
FIGURE 28. Virtual junction.                     the temperature gradient across the
                                                 extension wire should be kept to a
                    R, R,                        minimum. This expedient, according to
                                                 the gradient theory, ensures that virtually
     ~·.---~Ar--~                                none of the output signal will be affected
                                                 by the extension wire.
  To digital
 volt meter                                      Noise
                R, T,             R,             Line related noise as it pertains to the
                                                 data acquisition system has already been
legend                                           discussed. The techniques of integration,
  R1 ==leakage resistance (O)                    tree switching and isolation serve to
  Rs == series resistance                        cancel most line related interference.
   T ==electrical terminal                       Hroadband noise can be rejected with an
                                                 analog filter.
244 Infrared and Thermal Testing
The one type of noise the dat<i             can an operator tell when the
acquisition system cannot reject is a direct    thermocouple is producing erroneous
current offset caused by a direct current       results? It is necessary to develop a
leakage current in the system. Although it      reliable set of diagnostic procedures.
is less common to see direct current
leakage currents of magnitude sufficient           Through diagnostic techniques, R.P.
to cause appreciable error1 the possibility     Reed has developed an excellent system
of their presence should be noted and           for detecting a faulty thermocouple and
prevented, especially if the thermocouple       data channels. 15 Three components of this
\Vire is very small and the related series      system are the event record, the zom' box
impedance is high.                              test and the thermocouple resistance
                                                history.
Wire Calibration
                                                Event Record. The first diagnostic is not a
Thermocouple wire is manufactured to a          test at all but a recording of all pertinent
certain specification signifying its            events that could even remotely affect the
conformance with thermocouple tables.           measurements. Table 8 shows an example.
The specification can sometimes be
enhanced by calibrating the wire (testing          Examination of the sample program
it at known temperatures). Consecutive          listing reveals that measurand :tvf821 uses
pieces of. wire on a continuous spool will
generally track each other more closely         a type J thermocouple and that the data
than the specified tolerance1 although
their output voltages may be slightly           acquisition program interprets it as type .J.
removed from the center of the absolute         But from the event record, apparently
specification. If the wire is calibrated in an  thermocouple l'vf821 was changed to a
effort to improve its fundamental               type K and the change was not entered
specifications, it becomes even more            into the program. Although most
imperative that all of the aforementioned       anomalies are not discovered this easily,
conditions be heeded to avoid                   the event record can provide valuable
decalibration.                                  insight into the reason for an unexplained
                                                change in a system measurement. This is
Documentation                                   especially true in a system configured to
                                                measure hundreds of data points.
It may seem incongruous to speak of
documentation as being a source of              Zone Box Test
voltage measurement error but the fact is
that thermocouple systems, by their very        The zone box is an isothermal terminal
ease of usc, invite a large number of data
points. The sheer multitude of data can         block with a known temperature ust·d in
become unwieldy. \Vhen many data are
taken, there is an increased probability of     place of an ice hath reference. If the
error from mislabeling of lines1 using the
wrong thermocouple curve etc.                   thermocouple is temporarily short
    Because channel numbers invariably          circuited directly at the zone box, the
change, data should be categorized by
measurand, not just by channel number. H        system should read a temperature very
Information about any given measurand1
such as transducer type, output voltage,        close to that of the zone box, that is, close
typical value and location can be
maintained in a data file. This can be          to room temperature (Fig. 29).
done under personal computer control or
simply by filling out a preprinted form.        If the thermocouple lead resistance is
No matter hmv the data are maintained,
the importance of a concise system              much greater than the shunting
should not be underestimated1 especially
at the outset of a complex data gathering       resistance, the copper wire shunt forces
project.
                                                F = 0. In the normal unshorted case, T1 is
Diagnostics                                     measured:                                ·
1-·fost of the sources of error mentioned       (10) \f    (( (T_t - '/~el )
arc aggravated by using the thermocouple
near its temperature limits. These                 But, for the functional test, the
conditions will be encountered                  terminals are shorted so that V = 0 V. The
infrequently in most applications. But          indicated temperature "f1 is thus:
what about the situation where small
thermocouples are being used in a harsh         (11) 0
atmosphere at high temperatures? How
                                                TABLE 8. Example of event record.
                                                Time           Event
                                                10:43    power failure
                                                10:47    system power returned
                                                11:05    changed M821 to type K thermocouple
                                                13:51    new data acquisition program
                                                16:07    M821 appears to be bad reading
                                                Contact Sensors for Thermal Testing and Monitoring 245
Thus, for a digital volt meter reading of                  it is possible to deduce what has artually
              \1 == 0, the system will indicate the zone_,
              box temperature. First the temperature 11                  happened (Fig. 31 ).
              (forced to be different from Trer) is                         The resistance of the thermocouple will
              observed; then the thermocouple is
              shorted with a copper wire and it is                       naturally change with time as the
              verHied that the system indicates the zone                 resistivity of the wire changes because of
                                                                         varying temperatures. But a sudden
              box temperature instead of 7J.                             change in resistance is an indication that
                                                                         something is wrong. In this case, the
                 This simple test verifies that the                      resistance has dropped abruptly,
              controller, scanner, volt meter and zone                   indicating that the insulation has failed,
              box compensation are all operating                         effectively shortening the thermocouple
              correctly. In fact, this simple procedure
              tests everything but the thermocouple                      loop (Fig. 32).
              wire itself.                                                  The new junction will measure
              Thermocouple Resistance                                    temperature T5, not T1. The resistance
                                                                         measurement has given additional
              A sudden change in the resistance of a                     information to help interpret the physical
              thermocouple circuit can act as a warning                  phenomenon that has occurred. This
              indicator. If resistance versus time is
              plotted for each set of thermocouple                       FIGURE 30. Burning coal seam.
              wires, a sudden resistance change can
              immediately be spotted, which could be                     To data                                         => r,
              an indication of an open wire, a wire                      acquisition system
              shorted because of insulation failure,
              changes caused by vibration fatigue or                                                                          T= 573 K
              one of many other failure mechanisms.
                                                                                                                         (300 <c = 572 'F)
                  For example, assume the thermocouple
              measurement shown in Fig. 30. For                                                           T= 1473 K
              example, suppose it is desired to measure
              the temperature profile of an                                                         (1200 oc"" 2192 "F)
              underground seam of coal that has been
              ignited. The wire passes through a high                    legend
              temperature region, into a cooler region.                    T := temperature (K)
              Suddenly, the temperature rises from
              573 to 1473 K (300 octo 1200 oc; 572 °F                    rl == electrical terminal
              to 2192 °F). Has the burning section of
              the coal seam migrated to a different                      FIGURE 31. Thermocouple resistance versus
              location or has the thermocouple                           time.
              insulation failed, thus causing a short
              circuit between the two wires at the point
              of a hot spot?
                  H a continuous history of the
              thermocouple wire resistance is available,
FIGURE 29. Shorting of thermocouples at terminals.                               ,,L_-----+----~
                                                                                            Time (relative scale)
                               Fe                                    r,
                  Copper wire short
                                                                         FIGURE 32. Cause of resistance change.
                                Cn
Volt meter l  Cu
                  Zone box isothermal block
legend                                                                   -~,,~,,
   Cn "'constantan resistance alloy (50 to 65 percent copper, 35 to      legend  "" Short
          50 percent nickel)
                                                                         T, =temperature at terminal of short
   Cu =copper                                                            T1 =-temperature at initial terminal
   Fe= iron
     T =electrical terminal
     V = voltage (V)
246 Infrared and Thermal Testing
failure would not have been detected by a      Summary
standard open thermocouple check.
                                               In summary, 'the integnty of <1
Measuring Resistance                           thermocouple system may he improved
                                               by following these precautions.
The checking of the thermocouple wire
resistance has been mentioned casually, as       1. Use the largest wire possible that will
if it were a straightforward measurement.           not shunt heat <~.way from the
\o\'hen the thermocouple is producing a             measurement area.
voltage, however, this voltage can cause a
large resistance measurement error.              2. If small wire is required, use it only in
Measuring the resistance of a                       the region of the measurement and
thermocouple is akin to measuring the               use extension wire for the region with
internal resistance of a battery. A                 no temperature gradient.
technique known as offset compensated
olim measurement can solve the problem.          3. Avoid mechanical stress and
                                                    vibration, which could strain the
   As the name implies, the data                    wires.
acquisition unit first measures the
thermocouple offset voltage ·without the         4. \A/hen using long thermocouple wires,
ohm current applied. Then the ohm                   use shielded, twisted pair extension
current source is switched on and the               wire.
voltage across the resistance is again
measured. The instrument firmware                5. Avoid steep temperature gradients.
compensates for the offset voltage of the        6. Try to use the thermocouple wire well
thermocouple and calculates the actual
thermocouple source resistance.                     within its temperature rating.
                                                 7. Use an integrating analog-to*digital
Special Thermocouples
                                                    converter with high resolution and
Under extreme conditions, diagnostic                 good accuracy.
thermocouple circuit configurations can          8. Use isolated inputs ·with ample offset
even be used. Tip branched and leg                  capability.
branched thermocouples are four*wire             9. Use the proper sheathing material in
thermocouple circuits that allow                     hostile environments to protect the
redundant measurement of temperature,                thermocouple wire.
noise voltage and resistance for checking       10. Use extension wire only at low
wire integrity (Fig. 33). Their respective           temperatures and only in regions of
merits are discussed in detail elsewhere.~-''        smal1 gradients.
                                               11. Keep an event log and a continuous
    Only severe thermocouple applications            record of thermocouple resistance.
require such extensive diagnostics but it is
comforting to know that there are
procedures that can be used to verify the
integrity of an important thermocouple
measurement.
FIGURE 33. Thermocouples: (a) leg branched
thermocouple; (b) tip branched
thermocouple.
(b)
                                               Contact Sensors for Thermal Testing and Monitoring 247
PART 3. Resistance Temperature Detectors
Background                                       !vfeyers' desjgn has been replaced by
                                              another laboratory standard: the bird cage
The same year that Seebeck made his           element proposed by Evans and Burns. 17
discovery about thermoelectricity,            The platinum element remains largely
Humphrey Davy announced that the              unsupported, which allows it to move
resistivity of metals showed a marked         freely when expanded or contracted by
temperature dependence. Fifty years later,    temperature variations. Strain induced
\Villiam Siemens recommended platinum         resistance changes caused by time and
as the element in a resistance                temperature are thus minimized and the
thermometer. Platinum is used to this day     bird cage becomes the ultimate laboratory
as the primary element in·all high            standard. Because of the unsupported
accuracy resistance thermometers. In fact,    structure and subsequent susceptibility to
the platinum resistance temperature           vibration, this configuration is too fragile
detector (PRTD) is used today as an           for industrial environments.
interpolation standard from the triple
point of equilibrium hydrogen, 13.803 K       Rugged Designs
(-259.347 'C ~ -434.824 'F), to the
freezing point of silver, 1234.930 K          A more rugged construction technique is
(961.78 'C = 1763.20 'F). Platinum is         shown in Hg. 35a. The platinum wire is
especially suited to this purpose, as it can  hifilar wound on a glass or ceramic
withstand high temperatures while             bobbin. The bifilar winding reduces the
maintaining excellent stability. A nohle      effective enclosed area of the coil to
metal, it shows limited susceptibi1ity to     minimize magnetic pickup and its related
contamination.                                noise. Once the ·wire is wound onto the
                                              bobbin, the assembly is then scaled with a
   The classical resistance temperature       coating of molten glass. Sealing ensures
detector (RTD) construction using             that the resistance temperature detector
platinum was proposed by C. H. Ivfeyers in    will maintain its integrity under extreme
1932. 16 He wound a helical coil of
platinum on a crossed mica web and            FIGURE 35. Resistance temperature detectors:
mounted the assembly inside a glass tube.     (a) sealed bifilar winding; (b) helical;
This construction minimized strain on the     (c) film.
wire while maximizing resistance
(Fig. 34).                                    (a)
   Although this construction produces a
very stable element, the thermal contact
between the platinum and the measured
point is poor and results in a slow thermal
response time. The fragility of the
structure limits its use mainly to that of a
laboratory standard.
FIGURE 34. Meyers resistance temperature      (b)
detector construction.
                                              (c)
248 Infrared and Thermal Testing
vibration but sealing also limits the          longer than a platinum element but its
expansion of the platinum metal at high        linearity and very low cost make it an
temperatures. Unless the coefficients of       economical alternative. Its upper
expansion of the platinum and the              temperature limit is only about 393 K
bobbin match perfectly, stress will be         (120 oc = 248 °F).
placed on the wire as the temperature
changes, resulting in a strain induced            The most common resistance
resistance change. This may result in a        temperature detectors are made of either
permanent change in the resistance of the      platinum1 nickel or nickel alloys. The
wire.                                          economical nickel derivative wires are
                                               used over a limited temperature range.
   There are partially supported versions      They are quite nonlinear and tend to drift
of the resistance temperature detector that    with time. For measurement integrity,
offer a compromise between the bird cage       platinum is the obvious choice.
approach and the sealed helix. One such
approach uses a platinum helix threaded        Resistance Measurement
through a ceramic cylinder and affixed via
glass frit (Fig. 35b). These devices will      The common values of resistance for a
maintain excellent stability in moderately     platinum film resistance temperature
rugged vibrational applications.
                                               detector range from 10 n for the bird
Metal Film Resistance
Temperature Detectors                          cage model to ±3 kn for the film
                                               resistance temperature detector. The single
In the ne'\\'est construction technique, a     most common value is 100 Qat 273 K
platinum or metal glass slurry film is         (0 °C = 32 °F). A representative standard
deposited or screened onto a small flat        temperature coefficient of platinum wire
ceramic substrate, is etched with a laser
trimming system and is sealed (Fig. 35c).      is a = 0.00385 K-1• For a 100 n wire this
The film resistance temperature detector
offers substantial reduction in assembly       corresponds to +0.385 .Q.K-1 at 273 K
time and has the further advantage of          (0 oc = 32 °F). This value for a is actually
increased resistance for a given size.         the average slope from 273 to 373 K (0 to
                                               100 oc; 32 to 212 °F). The more
   Because of the manufacturing                chemically pure platinum wire used in
technology, the small size of the device       platinum resistance standards has an a of
itself means it can respond quickly to step    +0.00392 K-1 (where increment of
changes in temperature. Film resistance        1.0 K = 1.0 oc " 1.8 °F).
temperature detectors are less stable than
their wire wound counterparts but are              Both the slope and the absolute value
more popular because of their decided          are small numbers, especially when it is
advantages in size, production cost and        considered that the measurement wires
ruggedness.                                    leading to the sensor may contribute
                                               ±3 n. A small lead impedance can
                                               contribute a significant error to
                                               temperature measurement (Fig. 36).
Metals                                         TABLE 9. Resistivities of common materials
                                               in resistance temperature detectors.
All metals produce a positive change in
resistance for a positive change in                             Resistivity
temperature. This1 of course, is the main
function of a film resistance temperature      Metal     n.mm 2·m-1  (See Note~)
detector. As will soon be seen1 system
error is minimized when the nominal            Gold      21.61       13.00
value of the film resistance temperature       Silver    14.63        8.80
detector resistance is large. This implies a   Copper    15.39        9.26
metal wire with a high resistivity. The        Platinum  98.08
lower the resistivity of the metal, the        Tungsten  49.87       59.00
more material must be used.                    Nickel    59.85       30.00
                                                                     36.00
   Table 9 lists the resistivities of common
resistance temperature detector materials.     a. English unit is kiloohm circular milliinch per foot.
   Because of their lower resistivities, gold  FIGURE 36. Effect of lead resistance.
and silver are rarely used for film                 lead 5 n
resistance temperature detector elements.
Tungsten has a relatively high resistivity        0-----'\1\f'v----
but is reserved for very high temperature
applications because it is extremely brittle   lead sn               lOOU
and difficult to work.                                               resistance
                                                                     temperature
   Copper is used occasionally as a                                  detector
resistance temperature detector element.
Its low resistivity forces the element to be
                                               Contact Sensors for Thermal Testing and Monitoring 249
A 10 Q lead impedance implies                                      resistors are replaced by one reference
10 + 0.385 at 299 K (26 'C = 79 'F) error                              resistor. The digital volt meter measures
in measurement. Even tlw t(•mperature                                  only the voltage dropped across the
coefficient ot the lead wire can contribute                            resistance temperature detector and is
a measurable error. The classical means for                            insensitive to the length of the lead wires
avoiding this problem has been a bridge                                (Fig. 39).
(Fig. 37).
                                                                          The one disadvantage of using a
    The bridge output voltage is an indirect                           four-wire resistor is that it needs one more
indication of the resistance temperature                               extension wire than the three-wire bridge.
detector resistance. The bridge requires                               This is a small price to pay for accmacy in
four connection wires, an external source                              temperature measurement.
and three resistors that have the same
temperature coefficient. To avoid                                      Conversion of Resistance
subjecting all three of the bridge                                     to Temperature
completion resistors to the same
temperature as the resistance temperature                              The resistance temperature detector is a
detector, a pair of extension wires                                    more linear device than the thermocouple
separates the resistance temperature                                   but it still requires curve fitting. The
detector from the bridge (Fig. 38a).                                   Callendar-Van Dusen equation has been
                                                                       used for years to approximate the
    These extension wires recreate the                                 resistance temperature detector curve: 19,20
initial problem: the impedance of the
extension wires affects tlle temperature                                        Ro a [T - s(....'!.:__ - 1)(....'!.:__)
reading. This effect can be minimized by                                                                  100 100
using a three-wire bridge configuration
(Fig. 38b).                                                                         ~ ( 1T00 - 1)[ 1T0"0]]
    If wires A and B are perfectly matched                             FIGURE 38. Extension wires separate
in length, their impedance effects will                                resistance temperature detectors from
cancel because each is in an opposite leg                              bridge to avoid subjecting it to same
of the bridge. The third wire C acts as a                              temperature as three bridge completion
sense lead and carries no current.                                     resistors: (a) impedance from bridge of two
                                                                       extension wires affects temperature
    The wheatstone bridge shown in                                     measurement; (b) three-wire bridge
Fig. 38b creates a nonlinear relationship                              minimizes impedance effects.
between resistance change and bridge
output voltage change. This bridge                                     (a)
compounds the already nonlinear
temperature resistance characteristic of                                f:
the resistance temperature detector by
requiring an additional equation to                                    (b)
convert bridge output voltage to
equivalent resistance temperature detector                              f:
impedance.
Four-Wire Resistor
The technique of using a current source
along with a remotely sensed digital volt
meter alleviates many problems associated
with the bridge. Because no current flows
through the voltage sense leads, there is
no drop in these leads and thus no lead
resistance error in the measurement.
   The output voltage read by the digital
volt meter is directly proportional to
resistance temperature detector resistance,
so only one conversion equation is
necessary. The three bridge completion
FIGURE 37. Wheatstone bridge.                                          FIGURE 39. Four-wire measurement of resistance (H).
                                                  Dig'1tal volt meter  tCurrent i           +  -<(- Current i = 0        100 u
                                                                                                                         resistance
    +                                                                              Digital     -<---- Current fo= 0      temperature
                                                                                   volt                                  detector
                                                                                   meter
250 Infrared and Thermal Testing
where           Rr =resi  stance  at t  emperat  ur  e  T·1     Self-Heating
     Rn =re          sistance  at T =  273                3  2 °F);
                                             K (0 oc  =              Unlike the thermocouple, the resistance
     a= tt?nlpernture coefficient at T = 0 oc                        temperature detector is not self-powered.
     (typically+ 3.92 x 10-3 Q.Q-I.K-1 where                         A current must be passed through the
                                                                     device to provide a voltage that can be
     increment of 1.0 K = 1.0 oc = 1.8 °F);                          measured. The current causes joule (il"R)
                                                                     heating within the resistance temperature
     S = 1.49 (typical value for 3.92 x JO<<                         detector, changing its temperature. This
                                                                     self-heating appears as a measurement
     platinum); ~ = 0 when T > 273 K                                 error. Consequently, attention must be
                                                                     paid to the magnitude of the
     (0 oc =32 °1') and typically p =0.11 when                       measurement current supplied by the
     T < 273 K (0 °C = 32 °F).                                       ohm meter. A typical value for
                                                                     self-heating error is 0.5 K·mV\T-1
     The exact values for coefficients a, ~                          (0.5 oc.mvv-1 = 0.9 °F·m\,Y-1) in free air.
     and 0 are determined by testing the                                 Obviously, a resistance temperature
                                                                     detector immersed in a thermally
     resistance temperature detector at four                         conductive medium vvill distribute its
                                                                     joule heat to the medium and the error
     temperatures and solving the resultant                          from self-heating will be smaller. The
                                                                     same resistance temperature detector that
     equations. This familiar equation was                           rises 1 K·m\'\'-1 i~1 free ~ir will rise only
                                                                     0.1 K·m\-\'-1 m atr flmvmg at the rate of
     replaced in 1968 by a twentieth order                           1 m-s-I.s
     polynomial to provide a more accurate                              To reduce self-heating errors use the
                                                                     minimum ohm measurement c'urrent that
     curve fit.                                                      will still give the required resolution and
                                                                     use the largest resistance temperature
     The plot of this equation shows the                             detector available that will still give good
                                                                     response time. Obviously, there are
     resistance temperature detector to be a                         compromises to he considered.
     more linear device than the thermocouple                        Thermal Shunting
     (Fig. 40).                                                      Thermal shunting is the act of altering the
                                                                     measurement temperature by inserting a
     Practical Precautions                                           measurement transducer. Thermal
                                                                     shunting is a problem more with
     The same practical precautions that apply                       resistance temperature detectors than with
     to thermocouples also apply to resistance                       thermocouples, as the physical bulk of a
     temperature detectors, i.e., use shields and                    resistance temperature detector is greater
     twi~ted pair wire, use proper sheathing,                        than that of a thermocouple.
     avOid ~tress ?nd steep gradients, use large
     extenston \\'Ire, keep good documentation                       Thermal Electromotive Force
     and use an integrating digital multimeter.
     In addition, the following precautions                          The platinum-to-copper connection that
     should be observed.                                             is made when the resistance temperature
                                                                     detector is measured can cause a thermal
     Construction                                                    offset voltage. The offset compensated
                                                                     ohm technique can be used to eliminate
     Because of its construction, the resiStance                     this effect. (See "!able 10.)
     temperature detector is somewhat more
     fragile than the thermocouple and
     precautions must be taken to protect it.
FIGURE 40. Resistance temperature detector more linear than
thermocouple.
16
    r~-f-f-f-.f-.-f---i-!-
12-
    ~-r-~~-+-+~-~ 0.390
/ v - --s 1- I_......  -+---+---!":::- 1=--  0.344
                                             o.293
4 V+-+---1,---+--                      --                            TAB.LE 10. Comparison of small and large
                                                                     resistance temperature detector.
    - .. ... - -t---t-1---f-- !---!----j                             Performance         Small   large
                                                                      Parameter          Device  Device
    - - · -·            --"--+---"---+·-
                                                                     Response time       fast    stow
    0 473             673 873 1073                                   Thermal shunting    low     poor
              (200)  (400) (600) (800)                               Self-heating error  high    low
              )3921  [752] [11721 [14721
legend
                         type S thermocouple
  - - - "' platinum resistance temperature detector
                                                                     Contact Sensors for Thermal Testing and Monitoring 251
PART 4. Thermistors
Like the resistance temperature detector,       (14) T      1
the thermistor is also a temperature
sensitive resistor. Although the                        .'     1
thermocouple is the most versatile                      A + H(ln R) + C(ln R)'
temperature transducer and the platinum
resistance temperature detector is the           where Tis temperature (kelvin), R is
most stable, the ·word that best describes      thermistor resistance (ohm) and A, Band
the thermistor is sensitil'e. Of the three      C are curve fitting constants.
major categories of sensors, the thermistor
exhibits by far the largest parameter              A, B and C are found by selecting three
change with temperature.                        data points on the published data curve
                                                and solving the three simultaneous
   Thermistors are generally composed of        equations. \!\'hen the data points are
semiconductor materials. Although               chosen to span no more than 100 K
positive temperature coefficient units are      (100 °C == 180 °F) within the nominal
available, most thermistors have a              center of the thermistor's temperature
negative temperature coefficient; that is,      range, this equation approaches a rather
their resistance decreases with increasing
temperature. The negative temperature           remarkable ±0.020 K (±0.020 oc ~
coefficient can be as large as several
percent per kelvin, allowing the                ±0.036 °F) curve fit.
thermistor circuit to detect minute                Somewhat faster computer execution
temperature changes that could not be
observed with a resistance temperature          time is achieved through a simpler
detector or thermocouple circuit.               equation:
   The tradeoff for this increased              (15) T ~
sensitivity is loss of linearity. The
thermistor is an extremely nonlinear                         [(In R)-Aj- 1l
device highly dependent on process
parameters. Consequently, manufacturers         ·where A and n are again found by
have not standardized thermistor curves
to the extent that resistance temperature       selecting two (H,T) data points and
detector and thermocouple curves have           solving the two resultant simultaneous
been standardized (l'ig. 41).                   equations. This equation must be applied
                                                over a narrower temperature range to
   An individual thermistor curve can be        approach the accuracy of the
very closely approximated through the           Steinhart~Har~ equation. Microcontrollers
Steinhart~Hart equation:21                      are well suited for thermistor interfacing.
FIGURE 41. Plots of voltage or resistance       Measurement
versus temperature.
                                                The high resistivity of the thermistor
Thermistor                                      affords it a distinct measurement
                                                advantage. The four~wire resistance
                                  Resistance    measurement may not be required as it is
                                  temperature   ·with resistance temperature detectors. For
                                  detector      example, a common thermistor value is
                                  Thermocouple  5 kQ at 298 K (25 oc ~ 77 °F). With a
Temperature T (relative scale)                  typical Tc of 4 ·percent per kelvin, a
                                                measurement lead resistance of 10 n
                                                produces only 0.05 K (0.0.1 oc ~ 0.09 °F)
                                                error. This error is a factor of 500 times
                                                less than the equivalent resistance
                                                temperature detector error.
                                                Disadvantages
                                                Because they are semiconductors,
                                                thermistors are more susceptible to
                                                permanent decalibration at high
                                                temperatures than are resistance
                                                temperature detectors or thermocouples.
252 Infrared and Thermal Testing
Thermistors are generally limited to a few
hundred kelvin and manufacturers warn
that extended exposures even well below
maximum operating limits will cause the
thermistor to drift out of its specified
tolerance.
   Thermistors can be made very small,
·which means they will respond quickly to
temperature changes. Their small thermal
mass makes them especiaJiy susceptible to
self-heating errors.
   Thermistors are a good deal more
fragile than resistance temperature
detectors or thermocouples and must be
carefully mounted to avoid crushing or
bond separation.
                                                                    Contact Sensors for Thermal Testing and Monitoring 253
PART 5. Integrated Circuit Sensors and Data
Processing1
Monolithk linear                                 A data acquisition and control system
Temperature Transducers                       provides high speed temperature
                                              measurements where point count is high.
An innovation in thermometry is the           \'\'hen configured for temperature
integrated circuit temperature transducer.    measurements, it offers the follo\'·.'ing
These are available in both voltage and       capabilities.
current output configurations. Both
supply an output linearly proportional to         A scanning analog-to-digital convcrter
absolute temperature. Typical values are      with 64 channels can be configured for
1 pA·K-1 and 10 mV·K-1 (Fig. 42).             temperature measurements_ Scanning rate
                                              is 56 000 channels per second. Several
   Some integrated sensors represent          hundred chmmel configurations are
temperature in a digital output format        possible with multiple modules. A signal
that can be read directly by a                conditioning plug-on rides pigb')'back on
microprocessor.                               the analog-to-digital converter module
                                              and provides input for thermocouples.. An
   Except that they offer a very linear       external terminal block has a built-in
output with temperature, these integrated     thermocouple reference junction and
circuit sensors share all the disadvantages   terminal connections to the application.
of thermistors. They are semiconductor        Four-wire resistor plug-on offers offset
devices and thus have a limited               compensation for resistance ternperature
temperature range. The same problems of       detector and thermistor measurements. A
self-heating and fragility are evident and    built-in engineerlng unit offers
they require an external power source.
                                              FIGURE 42. Integrated circuit sensors, also
   These devices provide a convenient         known as monolithic linear temperature
way to produce an output easy to read         sensors: (a) sensor of current i; (b) voltage
and proportional to temperature. Such a       sensor 1 K == 1 °C == 1.8 °F.
need arises in thermocouple reference
junction hardware and in fact these           (a) +
devices are increasingly used for
thermocouple compensation.
Measurement System                                   yI i"'-l !1A¥·1
Data processing systems are available for            10 kn  lo digital volt meter
implementing thermocouple reference
junctions. Integrated circuit sensors can     (b) +
be used to perform software thermocouple
compensation.                                                         Todigit<JI
                                                                      volt meter
   Conversion routines built into
firmware accept type B, E, J, K, N, R, S and
T thermocouples; 2.2, S and 10 kQ
thermistors; and a wide range of
resistance temperature detectors.
   Data acquisition systems can
incorporate desirable features mentioned
above: internal digital multimeter;
integrated analog-to-digital conversion for
noise rejection; low thermal scanning
with built-in thermocouple reference
junctions; open thermocouple check;
built-in thermocouple, thermistor and
resistance temperature detector
linearization routines with conformity to
the International Temperature Scale;4
four-wire ohm function with offset
compensation; and isolated inputs that
float up to 300 V.
254 Infrared and Thermal Testing
conversions for thermocouple, thermistor
and resistance temperature detector
measurements.
   Such a data processing system offers
more than temperature measurements. It
provides a wide variety of
analog~to·digital input and output
capability required by designers of
electromechanical products and by
manufacturers needing stringent
monitoring and control of physical
processes.
   Instrumentation alternatives range
from small compact systems for portable
or remote operation to high speed
scanning systems that also provide
advanced control and analysis
capabilities.
Summary
Reliable temperature measurements
require a great deal of care in both
selecting and using the transducer, as well
as choosing the right measurement
system. \'\'ith proper precautions observed
for self-heating, thermal shunting,
transducer decalibration, specifications
and noise reduction, even the most
complex temperature monitoring project
will produce repeatable, reliable data. Data
acquisition systems assume a great deal of
this burden, allowing the operator to
concentrate on interpretation of test
results.
                                                            Contact Sensors for Thermal Testing and Monitoring 255
PART 6. liquid Crystals
More than a century ago, the discovery of      Nematic phases are thus typified by a
two unusual chemical compounds22,Z.1           certain directional order hut lacking a
exhibiting unusual behavior between the        layered structure, Nematic liquid cryst.:1ls,
crystalline solid and isotropic liquid state,  in particular the twisted nematics formed
was to change the understanding of the         by sandwiclling the liquid crystals
possible states of matter. Discovered          between plates of glass l\'ith a special
around the time of the birth and               surface finish, are very common in liquid
development of some of the world's             crystal displays of watches, calculators
biggest chemical industries, this new field,   .:md similar devices.
liquid crystals (LC), was to undergo a
long, slow gestation period, culminating       Cholesteric or Chiral Nematic
over the last 30 years of the twentieth        Phase
century in an amazing range of
inventions and industrial applications.        The physical properties of cholesteric, or
Even the membranes in the human body           clliraluematk~ liquid crystals, are in
depend on liquid crystals. The catalog of      almost all aspects similar to nematics,
known liquid crystals has grown to over a      except that the director axis assumes a
hundied thousand new substances,2'i            helical form of finite pitch equal to the
associated ·with remarkable discoveries        distance it takes for the director to rotate
and inventions in different branches of        one full turn in the helix. A byproduct of
the material and life sciences and in          the helical structure of the chiral nematic
engineering and industry.25-26 As pointed      phase is its ability to reflect light
out by Collings and Patel,27 the sheer         selectively at wavelengths equal to the
volume of material published on liquid         pitch length. A color wlll be reflected
crystals is now so large that an exhaustive    when the pitch is equal to the
summary and bibliography is virtually          corresponding wavelength of light in the
impossible.                                    visible spectrum. Temperature changes
                                               modify the director orientation and pitch
Thermotropic liquid                            length, resulting in an alteration of the
Crystals                                       wavelength of the reflected light, or color,
                                               with temperature, thus providing a basis
Thermotropic liquid crystals are among         for thermographic measurements.
the most widely used liquid crystals. They
exhibit various liquid phases as a function    Smectic Phase
of temperature and their linear and
non1inear optical behavior has been            The third group are the smectic
extensively studied.27·51 Although their       mesophases. }..folecules in this state show
molecular structure can be complicated,        a degree of positional order not present in
they are often represented as rigid rods.      the nematic or chiral nematic phases,
The molecules interact with one another        resulting in a more solid structure. Short
and, depending on the temperature and          range, quasilong range and long range
their makeup, form distinctive ordered         positional order all occur in smectic liquid
structured patterns, ranging over the          crystals,
nematic, cholesteric or chiral nematic and
smectic rnesophases.                               A large number of smectic phases have
                                               been discovered and classified, according
Nematic Phase                                  to their molecular order and structural
                                               symmetry properties (for example, smectic
Decreasing the temperature of a liquid         A to smeclic K and smectic C* to smectic
crystal from the isotropic liquid state, in    K*,27·52 The recent use of ferroelectric
which the molecules are randomly               liquid crystals (also known as smcctic C*
positioned, changes the material to the        liquid crystals) in providing time varying
nematic phase, where the molecules gain        measurements of surface shear stress in
a certain amount of orientational order        high speed wind tunnel testing is one
but no positional order. This orientational    example of nonintrusive testing using
order permits definition of an average         smeclic liquid crystals.sJ,S4
direction (director nxb:) of tl1e molecules.
256 Infrared and Thermal Testing
Liquid Crystal                                 Practical Procedures in Liquid
Thermography
                                               Crystal Thermography
By far the largest group of liquid crystals
                                               A great deal of useful info_rmation is now
are the thermotropic liquid crystals           readily accessible, on the mternet as well
                                               as in publications, providing background
(TLCs), with over 78 000 compounds             and references on types and formats of
                                               thermochromic liquid crystals, 41 .47,48 and
registerect.24 From the early days, the        practical procedures to follow. 49"51 •61 -h7
effect of temperature on the different         Materials
mesophases was a factor of key interest.       Thennochromic liquid crystals are
                                               avili1ahle in several forms: (1) sprayable
As a result, it is not surprising that most    microencapsulated liquid crystal coating
                                               for solid surfaces In air or water,
of the work on liquid crystals in              (2) coating systems for large area thermal
                                               mapping in air, (3) microencapsulated
nonintrusive measurements or                   liquid crystal slurries for use as tracer
                                                particles in flow field studies in aqueous
nondestructive testing have concentrated        liquids, (4) polyester sheets coated with
                                                microencapsulated liquid crystals for flat,
on temperature and heat transfer                solid surfaces in air or water and
                                                (5) unsealed liquid crystal compounds and
measurements.                                   mixtures for microscopic evaluation of
                                                small objects such as electronic
Early work suffered from the                    components.48
limitations of pure liquid crystals, which          Unsealed compounds allow spatial
                                                discrimination down to the micrometer
deteriorated rapidly and were particularly      level. However, because of their inherent
                                                oily form, pure thermotropic liquid
susceptible to degradation by                   crystals can be difficult to work with and
                                                their thermal performance can degrade
contamination and ultraviolet light Many        rapidly through contamination and
                                                exposure to ultraviolet radi<ltion. On the
of these problems were eliminated by a          other hand, microencapsulated liquid
                                                crystals are protected by being enclosed in
microencapsulation process.                     a strong, thin transparent wall, forming
~vHcroencapsulation also possessed the          small temperature sensing capsules of S to
                                                 10 pm in diameter. An tldvantage of this
added advantage of greatly reducing color        medium is that different microcapsules
                                                 can be mixed together to provide
variation due to viewing angle.                  independent or overlapping regions of
                                                 color play, besides reducing dependency
A review29 of some of the work before            on the lighting and viewing setup.
1975 includes applications of liquid                 The chemical makeup of a
                                                 thermotropic liquid crystal material fixes
crystals to check the following:           _     its color temperature response. The
irregularities on bonded structures, 30-J2       manufacturers typically provide a
                                                 two-color temperature code, indie<lting
regions of overheating on electronic             the starting temperature (el'mt
                                                 tempemture) and the red~to-blue start
equipment,:ll-33 flow blockages in heat          bandwidth (W). For example, R35CSH'
exchangers,3~ crack detection on aircraft        specifies a red (R) event temperature of
stwcture, 3~ the effectiveness of ·windshield
                                                 35 °C and a blue start, S "C higher, at
heater,33.J~ and thermal mapping in the
                                                 313 K (40 oc =- 104 "F). Thermochromic
medical fieldJS.:~o Over the next 15 years
                                                  liquid crystal formulations are available
many advances occurred in the tailoring          with red event temperatures ranging from
                                                 243 K to 373 K (-30 octo +100 oc; -22 OF
of the liquid crystals, in _particular in         to +212 "F); with narrow bandwidths
digital image processing.37•55                    down to around O.S K (0.5 "C = 0.9 "F);
                                                  and with broad bandwidths up to 30 K
There was not only a movement from                (30 °(: == 86 "F). This provides the user
                                                  ·with a range of choices off the shelf but
qualitative visuaJizations to more reliable       the manufacturers can also provide spec"Jal
and quantitative measurements3'H1                 mixtures designed for a particular
                                                  application.
requiring suitable calibration techniques,
but also a demand to extend the work to
cover time dependent phenomena. The
latter highlighted the important question
of the thermal characteristics and the
time responses of various liquid crystal
materials. 40
   Parsley41 summarized a number of
steady state and transient heat transfer
techniques, including studies of the
thermal performance of gas turbine
components,42,43 measurements of local
heat transfer coefficients on gas turbine
blades-14.45 and the response of
microencapsulated, chiral nematic, liquid
crystal films to surface temperature
changes.45,-J(, The experiments sh?w~d !he
response time of the thermotropic hqwd
crystal film to be no more than a few
millisecond. Liquid crystals developed for
surface shear stress measurements in
aeronautics are now also available with
response times in the submillisecond
rangeSJ-Oo and new ferroelectric liquid
crystals possess optical switching times
faster than a microsecond.27·52
                                               Contact Sensors for Thermal Testing and Monitoring 257
Because thermochromic liquid crystal       Wide Band Thermochromic liquid
thermography depends on assigning a            Crystal Formulations
temperature to the color reflected from
thermotropic liquid crystal coated surface,    An alternative to narrow band
care must be taken to avoid reflection of      thermochromic liquid crystals is to use a
the light transmitted through the crystals,    single wide band thermochromic liquid
by first coating the test surface with liquid  crystals to map the isocolor or isotherm
crystal compatible, black backing paints.      pattern of a surface from a single image.
In the case of liquid crystal sheets, a        These wide band techniques are useful
nonreflecting backing material forms part      when an object has large temperature
of the sheet, with the option of an            variations and when accuracy and high
additional peelable, sticky back layer for     spatial resolution are required. Practical
attaching the sheet directly to a flat test    applications of wide band techniques
surface.                                       include the investigation of surface
                                               temperature distributions in such areas as
Qualitative Temperature                        gas turbine blade cooling, electronic
Visualization Techniques                       components and the study of boiling heat
                                               transfer phenomena.
?vfany temperature applications only
require qualitative information. In this           Farina61 has summarized the
case, the two-color temperature                advantages and disadvantages of the two
descriptors of the thermochromic liquid        systems: narrow band and ·wide band.
crystal material, combined with the color      The advantages of the narrow band
response capabilities of human eyes, can       thermochromic liquid crystal technique
readily provide a simple solution.             are as follows.
Qualitative thermochromic liquid crystal
techniques are typically easy and                1. High accuracy is possible in both
inexpensive to implement and can                   absolute and relative temperature
provide high spatial resolution ·when              measurements.
properly used in an application that
provides suitable optical access to the         2. Implementation is inexpensive and
thermochromic liquid crystal coated                requires simple image processing
surface. A typical qualitative application         systems.
might be a quick investigation of the
temperature response of electronic             The disadvantages of the narrow band
components or electrical equipment to          thermochromic liquid crystal technique
natural or forced convection and               are as follows.
component orientation.61
                                                1. Construction of an isotherm pattern
Quantitative Narrow Band                            can be tedious and time consuming.
Thermochromic Techniques
                                                2. Full field capabilities of the
Most quantitative liquid crystal                   thermochromic liquid crystal coating
thermography applications have used                 are not used.
narrow band microencapsulated
thermochromic liquid crystal                   The advantages of the wide band
formulations or multievent temperature         thermochromic liquid crystal technique
mixtures consisting of a number of             are as follows.
narrow band thermochromic liquid
crystals, each having different event           1. It uses the thermochromic liquid
temperatures. Collected data from                   crystals bandwidth to map the entire
successive experiments at different surface         isotherm pattern of a surface from a
temperatures facilitates construction of           single image.
surface isotherm patterns using either
single or multievent formulations. Narrow       2. It is preferable in applications having
band thermochromic liquid crystal                   large temperature variations and
formulations permit (1) accurate                    requiring high spatial resolution.
verification of surface isotherms,
(2) relatively accurate surface temperature    The disadvantages of the wide band
measurements using simple image                thermochromic liquid crystal technique
processing systems and (3) higher              are the following.
accuracy with some in situ color
temperature calibration.                         1. Robust color temperature response
                                                    calibration is necessary for high
                                                    accuracy measurements.
                                                2. It is more expensive to implement
                                                    because more sophisticated image
                                                    processing systems are required.
                                               Color, lighting and Color
                                               Temperature Calibration
                                               Procedures
                                               The interpretation of color is very difficult
                                               and subjective.68-70 Basically color is
                                               related to the wavelength of the reflected
258 Infrared and Thermal Testing
light. In human eyes the rods and cones                      the raw (red green blue) values would vary
                    decompose color into a combination of                        from 0 to 255, with their values then
                    the red, green and blue (RGB) primary                        riormalized by dividing by 255.
                    colors. This red green blue tristimulus
                    decomposition is regularly used in                              However, the red green blue
                    modern machine vision systems.                               representation is not the moS:t appropriate
                                                                                 model when it comes to calibrating color
                        A large selection of charge coupled                      versus temperature. A more convenient
                    device digital color cameras, both single                    and practical approach is to transform the
                    shot and video, are available with high                      basic red green blue data into the hue
                    pixel discrimination and good                                saturation intensity (HSl) color modeJM-7°
                    performance, providing red green blue
                    outputs. The latter basically represent the                  (Fig. 44):
                   color field in the form of three RGB
                    matrices defined by the outputs from the                     (16) R+G+B
                    light sensitive pixels (picture sensing                                               3
                    elements) of the camera. A wide range of
                    frame grabber cards also exist for seizing                   (17) s  3[min(R + G + JJ)j
                    this information and transferring it to the
                    computer for storage and analysis. In fact,                               R+ G+ B
                    many personal computers now come
                    equipped with direct digital camera input                    FIGURE 44. Hue saturation intensity (HSI):
                    ports and internal signal processing                         (a) color triangle; (b) color solid.'0
                    hardware and programs for treating the
                    data.                                                        (a) Blue
                        'Ib use color, some suitable color model                                                                                         Green
                    must first be chosen. Basically, a color
                    model specifies a three-dimensional                          (b)
                    coordinate system and a subspace within
                    that system where each color is                                      I
                    represented by a point. The RGB color
                    model widely used in color monitors and
                    color video cameras uses a cartesian
                    coordinate system with the color subspace
                   consisting of a cube, with the values of
                    red, green and blue each ranging from 0
                     to I (Fig. 43). For example, using an
                     eight-bit (28 = 256) digital color camera
FIGURE 43. Red green blue (RGB) color cube. Points along the
main diagonal have gray values, from black at the origin to
white at point (1,1,1 ).7°
                                      B
                     Blue_;!_(O_.o_,1_>______, Cyan
                                                 (1, 1.1)        (0,1.0)
Magenta f.-----.-----c{.                                        __........... G
                                                         White  Green
                                 I
                                 I
                                 I
                                    I
                                    I
                                 I Gray scale
                        Black~<- ____ _
(1.0.0)                           /                                              legend
                              /
                           /                                                       C"' central color point
                         /                                                         H =dimensionless number representing hue
                                                                                    I = dimensionless number representing intensity
                    /                                                               P = two-dimensional point in color triangle
                 /
         ./.._/ _ _ _ _ _ _ _ _y
   /Red  Yellow
R
                                                                                 Contact Sensors for Thermal Testing and Monitoring 259
(18) H            LR-G) I(R-:_ll)              Summary of liquid Crystal
                                               Test Procedure
        COS-I -c~~-~2~-~-~
                                               l:arina49/i3,6.'l has summarized the main
              frR-G)2 +(11-B)(G-H)             guidelines to follnw when using liquid
                                               crystals for thermographic measurements.
where H =hue (dimensionless); J is
                                                1. Determine the expected minimum
intensity (dimensionless); Pis color point         and maximum temperatures of the
inside two-dimensional H and S color               surface(s) under investigation.
triangle; Sis saturation (dimensionless);
and R, G and R respectively represent red,      2. Select the appropriate thermochrom ic
                                                   liquid crystal mixture for this
green and blue data from the digital               temperature range ....,.. for exarnple,
camera.                                            narrow band, multievent or \Vide
                                                   band.
    Assuming that 1-/ is calculated in
degrees, replacing H by (360- H) if             3. Properly prepare and apply tlle black
                                                   background and thermochromic liquid
(JJ.J-') > (G·Y'), the hue is then                 crystal material to the test surface.
normalized to the standard range fO, 1J by
dividing by 360. Note that H is not             4. Provide adequate optical access to the
defined when S = 0. 70                             surface and minimize unwanted
                                                   reflections.
   A bright, stable light source is required.
                                                5. Provide an online lighting and
\VIlite light sources that remove infrared         vie\Ving arrangement if possible with
and ultraviolet radiation from their               crossed polarizers.
output spectrum are preferable, to avoid
unwanted radiant heating of the test            6. lVfinimize infrared and ultraviolet
                                                   radiation to the test surface.
surface and deterioration of the liquid
crystals from ultraviolet light.                 7. Calibrate the color versus temperature
                                                   response (for example, hue versus
   If possible, color temperature                   temperature) of the thermochromic
calibrations should be carried out with            liquid crystal and imaging system if
preca1ibrated secondary standards, such as         quantitative measurements are
thennocouplcs or thermistors, mounted               required.
on the test plate or test object. It is
important to ensure consistent light            8. Image or visualize the active
source settings and lighting viewing                thermochromic liquid crystal test
arrangements between calibration and               surface.
actual testing to minimize errors. A
coaligned primary lighting viewing              9. Oetennine the surface temperature
system, without any background or                  distribution using the appropriate
secondary lighting, is recommended,                color versus temperature calibration.
whenever possible. 63•65
                                               Conclusions
   A typical calibration procedure using
hue versus temperature is described in         The widespread application of liquid
detail in the Jiterature.fi6 A thermistor was  crystals is relatively modern (3ince 1970)
first calibrated against a platinum            and depends to a great extent on
resistance thermometer in a constant           developments and requirements in
temperature oven. The thermistor was           completely different branches of science
then mounted on a heated copper block          and engineering, such as computers,
with the liquid crystal coatings               optics and chemistry. The great increase
illuminated by white lights with               in the number, variety and knowlt>dge of
ultraviolet filters. Hue-versus~temperature    liquid crystal compounds, together with
calibrations were carried out using a          the rapid emergence of new technologies
charge coupled device camera with a red        such as microelectromechanical
green blue frame grabber and image             mechanisms and microelectrooptical
processing sofhvare. Figures 45 and 4666       devices, can facilitate the integration of
illustrate respectively three typical and      liquid crystals into many monitoring and
virtually identical initial calibrations and   measurement devices in the field of
a subsequent final calibration after three     temperature measurement.
weeks of testing. The calibrations exhibit
differences of two percent or less of the
temperature h<HHhvidth of the liquid
crystals.
260 Infrared and Thermal Testing
fiGURE 45. Three identical initial temperature versus hue calibrations for runs 9, 10 and 11.ti6
   r313 (40) {104]                      ----,----
   311 (38) {100]                       I                    '
                                        j                    1I ---
                                        I
E                                                  ----r---
E 309 (36) (97] - - - - "
l1'                                                1
 0                                                 '
                                                   I
   307 (34) [93) 1 - - - - - t - - - -
E                                                  I
~
   305 (32) (90]
   303 (30) (86]
                     0 0.1 0.2 03 OA 0.5 0.6
                                                           Hue (relative unit)
FIGURE 46, Calibration of temperature versus hue at start (run 11) and end (run 15) of test
program. 66
   313 (40) (104] f-        -!          -- - - - 1 - ------~----        I.  ------~
                     i                                                  I
                                                     1I                 i
                      I                                                 I
                                              II
   - - - - - t -311 (38) [100) C"i                                      i
                                                                  "'
                                1
                                               .. II - - - - -'r - - -
             I
                                                   i
"' 309 (36) (97]                                   I
'-"                                                !
                                                   I
                                                   I
~~ 307 (34) {93)                              I
~                                                                I
 0                                  ·I ~----~---
 OL
                                    0.2 0.3 OA
E
~                                            Hue (relative unit)
      305 (32) (90]
     303 (30) (86]          0.1                                              ___j
                         0
                                                                        0.5 0.6
legend
     - n· = run 11
   ~=-runl5
                                                   Contact Sensors for Thermal Testing and Monitoring 261
PART 7. Media with Calibrated Melting Points
Temperature Indicating                           Temperature ratings are in increments
Media                                         as small as 3.4 K (3.4 "C ~ 6.1 "F) but
                                              increments ranging from 14 K (14 oc =
Certain materials are used by industry to     25 "F) to 28 K (28 "C ~ SO "F) are typically
indicate temperature according to their       used for welding applications. For most
predictable melting points. These             applications, a jump of 28 K (28 oc =
temperature indicating materials are          FIGURE 47. Temperature indicating materials:
available in several media - typically as     (a) lacquer; (b) pellets; (c) sticks of differing
lacquer1 pellets or sticks (Fig. 47).         temperature sensitivity.
                                              (a)
   The lacquer is brushed on before
welding starts and is useful on highly        (b)
polished surfaces or for making large
marks vielved at a distance.                  (c)
    Heat indicating pellets, about the size
and shape of an aspirin1 have greater mass
than stick or lacquer marks (see Fig. 47b).
Pe1lets are sometimes selected for large,
heavy pieces requiring prolonged heating
- applications where stick or lacquer
marks could fade with time.
    A temperature indicating stick (chalk or
crayon) is typically made of materials
\'l'ith calibrated melting points and
temperature measuring accuracies to
±1 percent.
    Indicators are available in closely
spaced increments over a range from
311 K (38 "C ~ 100 "F) to 1643 K
(1370 "C ~ 2500 "1').
Stick Medium Procedure
The work piece to be tested is marked
with the stick. VVhen the work piece
attains the predetermined melting point
of the indicator mark, the mark instantly
liquefies, notifying the observer that the
work piece has reached that temperature.
    Premarking with a stick is not practical
under certain circumstances- ·when a
heating period is prolonged a highly
polished surface does not readily accept a
mark or the marked material gradually
absorbs the liquid phase of the indicator.
In such instances, the operator frequently
marks the work piece with the stick. The
desired temperaturr is noted ·when the
stick ceases to make dry marks and begins
to leave a liquid smear. A similar
procedure can be used to indicate
temperature during a cooling cycle. But a
melted mark, on cooling, will not solidify
at exactly the same temperature at which
it melted, so solidification of a melted
indicator mark cannot be relied on for
temperature indication.
262 Infrared and Thermal Testing
50 °F) to 56 K (56 oc = I 00 °F) and a range     Marking materials tised on austenitic
of sticks up to 923 K (650 °C = 1200 °F)      stainless steels typically have a certified
are usually adequate.                         analysis that meets the following specified
                                              maximum amounts of detrimental
   Temperature indicating sticks were         contaminants: (1) inorganic halogen
developed in America by a metallurgist        content less than 200 pg-g-1; (2) halogen
working on submarine hulls in the 1930s.      (inorganic and organic) content Jess than
At the lime, preheat was measured with        one percent by weight; (3) sulfur content
so-called melting point standards,            less than one percent by weight measured
granules of substances with known             in accordance with ASTM D 129;71 and
melting points used to calibrate heat         (4) total content of lm\' melting point
sensing instruments. The engineer used        metal (lead, bismuth, zinc, mercury,
the granules directly, spreading them on      antimony and tin) Jess than 200 pg·g-1 by
the preheated metal and using their melt      weight and no ii1dividual metal content
as a signal to proceed with welding.          greater than 50 pg·g-1• The certification
                                              typically indicates the techniques and
   The melting point granules were next       accuracy of analysis and the name of the
formed into sticks held together ·with        testing laboratory.
organic binders. Different temperature
ratings were added and some refinements       Applications for
have been made but the principle of           Temperature Indicators
indicators has remained unchanged. The
sticks make physical contact with the         Temperature indicators can be used for a
heated test object, reach thermal             variety of applications, especially in
equilibrium rapidly and do not conduct        process control: preheat temperature tests
heat away from the test surface.              and in annealing and stress relieving
                                              procedures, hardfacing, overlaying for
   For temperature ratings less than 613 K    corrosion resistance, flame cutting, flame
(340 °C :::: 644 °F), indicator marks can     conditioning, heat treating, pipe bending,
usually be removed with water or alcohol.     shearing of bar steel, straightening
For ratings above 613 K (340 oc = 644 oF),    hardened parts, shrink fitting, brazing,
water is preferred. If the mark has been      soldering and nonferrous fabrication. The
heated well above the rated temperature       indicators can help find hot spots in
and has become charred, abrasion may be       insulation and engines, help monitor
needed for complete removal.                  temperatures in curing and bonding
                                              operations and help check pyrometric
Certification of                              calibration.
Temperature Indicators
                                              Tests of Railway Bearings
Temperature indicating sticks are mixtures
of organic and inorganic compounds. The       Bearing breakdown can be detected by
purity of the source materials directly       using fluorescent temperature indicating
affects the accuracy of the predicted         pellets as heat sensors for inboard journal
melting point. There is the possibility of    boxes. The pellets are inserted in a
contamination with trace quantities of        specia1ly fabricated stainless stec1 holder
other elements, which may be detrimental      that contains two pellets. The holder is
to the accuracy of the indicator. In some     inserted into the hollow axle of each rail
cases, low melting point materials (lead,     car with an insertion tool. The tool has a
tin, sulfur, halogenated compounds) may       mechanical stop to ensure that the holder
be undesirable for the welding procedure.     is located at a predetermined depth. This
                                              permits proper monitoring of journal box
   Most manufacturers can provide             operating temperatures.
certification supported by analyses of
typical batches; Documentation indicates          Once a specified temperature is
which temperature ratings may contain         exceeded, in this case 373 K (100 °C =
contaminants that can be avoided by the       212 °F), the pellets melt and fluw
user.                                         completely out of the holder. The
                                              fluorescent material is easy to detect and
   In some critical applications (nuclear     clearly indicates that excessive heat has
fabrication, aircraft assembly), actual       been conducted 'from the bearing to the
chemical analysis of the specific lot         axle.
number of the temperature indicators
may be required. If the customer supplies     Verifying Oven Temperatures
a written certification requirement listing
the compounds to be tested for, most          Technicians can determine if self-cleaning
manufacturers will send lot numbered          ovens reach the proper cleaning
samples for laboratory analysis. The          temperature using pellets with
customer is usually expected to pay           precalibrated melting points at 723 K
laboratory charges for such specialized
requirements.
                                              Contact Sensors for Thermal Testing and Monitoring 263
(450 "C = 842 "F). The pellets are placed     sealing tape used in production. A visual
on a flat piece of aluminum foil situated     test of each seam after sealing indicates
on the oven's center rack (see Fig. 48). The  whether the seam temperature was ·within
cleaning cycle iS activated and as the        the required range, allowing visual
                                              verification of conditions for all dielectric
temperature reaches 723 K (450 oc =           seams.
842 "F), the peilets begin to melt.           Precise Postforming Heat Control
    \-\1hen the cleaning cycle is completed
                                              Temperature indicating materials are
and the oven has cooled, the pellets are      incorporated into many industrial
examined - complete melting of the            applications where- an indication is
tablet verifies that the nominal cleaning     needed to show that a critical temperature
temperature has been achieved.                has or has not been reached. A phase
                                              changing fusible liquid is used to indicate
Process Control of Ceramic                    optimum postforming temperatures when
lnsulat'ron                                   bending decorative laminate for the
                                              contoured edges of countertops, desks,
A gas tight seal is needed to prevent         tables and other surfaces (Fig. 49).
leakage of combustion gases through the
glass portion of a spark plug. lb obtain         Postforming is the process of bending a
optimum fusion properties, it is important    flat sheet of laminate around a radiused
to know and control the temperature           core material (particle board, plywood or
inside the ceramic insulator and this can     fiber board). The process is typically done
be done using a temperature indicating        after controlled heating monitored with
pellet. Sample insulators are loaded with     temperature sensitive liquids. Postfonning
pellets and processed with production         can be a manual or mechanical operation.
parts. Information obtained from              Hand postforming is used for unusual
analyzing the samples is used to adjust       configurations or limited quantity
furnace conveyor speed and temperature.       production; mechanical postforming is
                                              used for high quantity production. Both
Monitoring Fabric Seam                        techniques need a heat source, prepared
Temperature                                   cores, postforming grades of decorative
                                              laminate, pressuring guides and evenly
In the making of specialized doth             applied pressure.
(protective clotlling, aerostat balloons),
seam integrity iS an important                   A core is prepared by first shaping the
manufacturing function. A good                edges to be laminated. The core and
radiofrequency seal can be achieved on a      laminate are evenly coated with a contact
given fabric substrate only within a
specific temperature range, determined by     FIGURE 49. Postforming of laminate around
the minimum temperature needed to             radiused core.
ensure a complete seal and the maximum
temperature possible before material
degradation. Constant temperature
control and verification are required.
   This can be achieved using temperature
sensitive strips (one for the upper limit,
one for the lower limit) applied to the
FIGURE 48. Pellets used to verify oven
temperatures over 723 K (450 "C = 842 "F).
264 Infrared and Thermal Testing
adhesive, preferably a spray. The laminate   that the correct temperature for coating
is positioned and registered with the core,  has been reached.
allowing the laminate to overhang the
radius. Postforming grades of decorative     Preheating before Welding
laminate are formable between
temperatures of 429 K (156 oc = 313 oF)      Heating to the proper temperature before
and 436 K (163 oc = 325 °F).                 welding lessens the danger of crack
                                             formation and shrinkage stresses in many
    A popular example of hand                metals. Hard zones near the weld are
postfonning is the 180 degree edge wrap.     reduced and lessen the possibility of
In this example, radiant heat is applied to  distortion. Preheating also helps diffuse
the decorative surface of the laminate       hydrogen from steel and helps reduce the
with the work supported over the heat. To    likelihood of subsequent hydrogen
determine the proper postforming             inclusions.
temperature, the temperature indicating
liquid is painted in stripes onto the            The need for preheating increases with
laminate. \'\'hen the liquid changes from a  the mass of the material being \Yelded. It
dry (matte) to a wet (melted) appearance,    is most useful for the thkk, heavy
the assembly is wiped into the cavity of a   weldments used in bridge construction,
fixture to form the 180 degree radius. The   shipbuilding, pipelines and pressure
fixture is a U channel made by two boards    vessels. Preheating is also recommended
attached to a base. The dimenSion of the     for (1) welding done at or below 25.1 K
U channel is the thickness of the core plus  (-18 oc = 0 °F), (2) when the electrode is a
the thickness of the laminate, allowing      small diameter, (3) when the joined pieces
about 0.5 mm (0.02 in.) clearance.           are of different masses, (4) when the
                                             joined pieces are of complex cross section
   Another example of handforming is         and (S) for welding of high carbon or
known as a full wrap. In this application,   manganese steels.
the core is positioned over radiant heaters
with temperature indicating stripes             The most common use for temperature
painted on the adhesive in the area of the   indicators is the measurement of preheat,
radius. When the melt indicates forming      postheat and interpass temperatures for
temperature has been reached, the            welding. In a typical application, the
assembly is moved back onto a flat           welder marks the test surface \Vith an
supporting surface. The wrapping action      indicating stick of a specific temperature
uses the flat surface as a pressure point.   rating (Fig. 47c). \'\'hen the mark changes
                                             phase (melts), the material has reached
   An example of mechanical postforming      the correct temperature and is ready for
is the roll forming machine. Radiant         welding. It is important for the user to
heaters are located above an assembly        understand that change of color has no
supported by a moving carrier. VVhen the     significance; only the actual melting of
forming temperature has been reached,        the mark should be considered.
slanted forming bars wipe the laminate
over the radius. After the laminate has          Oxyacetylene equipment cannot be
been formed, a succession of rollers         used for welding or cutting of high
maintains pressure until the assembly has    strength steels used in automotive
cooled. In this application, temperature     components because too much heat can
sensitive liquid is painted onto the         reduce their structural strength. However,
laminate to verify that the dwell time       in some instances an oxyacetylene torch
under heat has been sufficient for           may he used if the critical temperature of
reaching forming temperature.                1033 K (760 oc = 1400 °F) for high
                                             strength steel is not exceeded.
Pipeline Coatings
                                                VVhen preheat temperatures are 643 K
Epoxy powders are specially formulated to    (3 70 °C = 700 °F) or when heating is
enhance corrosionproof resistance of         prolonged, an indicating mark could
utility pipe: that is, pipe usually buried   evaporate or cOuld be absorbed by the test
underground, where it is subject to widely   material. Under these conditions, marks
varying pipeline operating conditions.       should be added periodically during
Intimately bonded to the pipe, the           heating. \'\'hen the rated temperature i:c.
bonded epoxy is unaffected by widely         reached, the stick leaves a liquid streak
varying soil compaction, moisture            instead of a dry mark and ·welding can
penetration, fungus attack, soil acids and   begin.
chemical degradation.
                                                To ensure accurate temperature
   To achieve a long lasting bond of         indication with no override, two or more
epoxy coating to metal pipe, the pipe        indicators can be used to alert the
must be preheated very carefully to the      operator that the test object is
recommended preheat of 273 K (0 °C =         approaching the correct temperature.
32 °F). A spot on the pipe needs to be       \o\1hen a range of recommended preheat
touched with the stick; its melting shows    temperatures is given, several indicators
                                             might be appropriate. For example,
                                             carbon molybdenum steel should be
                                             Contact Sensors for Thermal Testing and Monitoring 265
preheated to between 366 K (93 oc =
                     200 °F) and 478 K (205 oc = 400 °F). A
                    bundle of indicators with ratings at 366,
                    393, 448 and 478 K ('J.l, 120, 150, 175
                     and 205 °C; or 200, 250, 300, 350 and
                    400 °F) might be useful for determining
                    how much of the test object is within the
                   preheat temperature range.
266 Infrared and Thermal Testing
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                                             Contact Sensors for Thermal Testing and Monitoring 269
60. Red a, D.C., M.C. Wilder, R. Mehta      69. Foley, ].D., A. Van Dam, S.K. Feiner
     and G. Zilliac. "Measurement of the        and ].F. Hughes. Computer Graphics:
     Continuous Pressure and Shear              Principh's and Practice, second
     Distributions Using Coating and             edition. Upper Saddle River, N.j:
     Image Techniques." AIAA /Olmwl.
     Vol. 36, No. 6. Reston, VA: American        Addison-VVesley Longman (1993).
     Institute of Aeronautics and           70. Gonzalez, R.C. and H.E. Woods.
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                                                Digital lmnge Processing. Upper
61. Farina, D.). and R.j. Moffat. A              Saddle River, N.j: Addison-\Vesley
     System for Making Temperature
     Measurements Using                          Longman (1992).
     Thermochromic Liquid Crystals.         71. ASTM D 129, Standard Test lvletllud
     Report No. HMT-48. Stanford, CA:
     Stanford University, Department of         fOr Sulfur Petroleum Products (Gmeral
     Mechanical Engineering,                     Bomb lvletlwd). \'\'est Conshohocken,
     Thermosciences Division (September          PA: American Society for Testing and
     1994).
                                                 Materials (1995).
62. Peterson, 0., S.H. Hu, C.D. Richards
     and R.E Richards. Tile Measurement
     ofDroplet Temperature Using
     Tllennochromic Liquid Ctystals.
     VVashington State University,
     Mechanical Engineering Department
    fwww.mme. wsu .edu/tlc/asmeseanJ
     (1995):
63. Farina, DJ, "Making Surface
     Temperature Measurements Using
     Liquid Crystal Thermography."
     Electronics Cooling
     f\vww.electronics-cooling.com].
     Marlborough, MA: Electronics
     Cooling Online (October 1995).
64. Azar. K. and D.j. l~arina. "Measuring
     Chip Temperatures with
     Thermochromic Liquid Crystals."
     Eleclrmzics Cooling
     [www.electronics-cooling.com].
     Marlborough, MA: Electronics
     Cooling Online Oanuary 1997).
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     Thermal Imaging System." Sensors
     Magazine. Vol. 15, No. 7.
     Peterborough, NH: Advanstar
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     p 12-16.
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     Distribution on Flat and Ribbed
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     Using Thermochromic Liquid
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     second edition. New York, NY: John
     Wiley & Sons (1982).
270 Infrared and Thermal Testing
CHAPTER
         Equipment for Infrared
             and Thermal Testing
                                                 Herbert Kaplan, Honeyhill Technical Company,
                                                 Norwalk, Connecticut (Parts 1 to 4)
                                      Leonard J. Bonnell, Vipera Systems, Incorporated,
                                                 Huntingdon Valley, Pennsylvania (Part 5)
                                      Thomas J. Brukilacchio, Innovations in Optics,
                                                 Incorporated, Woburn, Massachusetts (Part 5)
                                                 Dennis C. Leiner, Light House Imaging, Peterborough,
                                                 New Hampshire (Part 5)
The United States government retains a nonexclusive right to reproduce Part 5.
PART 1. Infrared and Thermal Instrumentation
Equipment for temperature measurement         Thermochromic Liquid Crystals
and thermography includes contacting as
well as noncontacting devices. Contacting     Thermochronlic liquid crystals (also called
devices for temperature measurement           cholesterol crystals) change color lvith
include thermopiles, thermocouples,           temperature. Coatings made of liquid
liquid thermometers, gas expansion            crystals arc commonly used as
devices (bourcton gas thermometers),          temperature threshold indicators.
liquid crystals (cholesterol crystals), heat  Depending on the mixture, a coating
flux indicators and fiber optic sensors.      applied to a surface will change color
Aside from some specialized instruments,      predictably when the surface exceeds a
the vast majority of noncontacting            threshold temperature. The color change
temperature measurement devices are           may be reversible or irreversible, and the
infrared radiation sensing instruments        sensing range for most mixtures is limited
and systems.                                  to a narrow temperature span. Typically, a
                                              set of liquid crystal markers provides a
    Infrared sensing instruments and          selection of transition temperatures. This
systems are divided into point sensors        allows the user to select the appropriate
(radiation thermometers), line scanners       marker for the desired temperature.
and thermal imagers.
                                              Thermocouples and Thermopiles
    This chapter begins with a review of
contacting thermal measurement                Thermocouples are contact temperature
instruments and a discussion of the basic     sensors based on the tllermoelectric effixt,
configurations of infrared sensing and        or see/Jeck effect. Thomas Seebeck
imaging instruments. This is followed by a    discovered that, vvhen two dissimilar
discussion of performance parameters          metals are joined at both ends and these
and, finally, descriptions of currently       ends are at different temperatures, a
available commercial thermal sensing and      predictable direct current will flow
imaging equipment, thermographic irnage       through the circuit. The thermoelectric
processing software and image hard copy       coefficient determines the relationship
recording accessories. 1                      between this current and the temperature
                                              difference between the two junctions.
Contacting Thermal                            This coefficient is known for each type of
Measuring Devices                             thermocouple.
The most commonly used contacting                To configure a thermometer, the circuit
devices include bimetallic thermometers,      is broken and the open circuit voltage h
thermochromic liquid cryStals,                measured by a volt meter. One of the two
thermocouples, resistance thermometers        junctions is then held at a reference
(R'I'Ds), thermistors and heat flux           temperature, such as an ice bath, and the
indicators. These devices are discussed       voltage is calibrated to indicate the
briefly here and in more detail in a          temperature of the other junction, which
separate chapter.                             then becomes the temperature sensing
                                              junction.
Bimetallic Thermometers
                                                 'fhermopiles are banks of
Bimetallic thermometers are sensors           thermocouples connected in parallel or in
constructed of dissimilar metallic strips     series to increase the output gradient. The
bonded together. Typically, different iron    reference temperature is important
nickel alloys are used. The strips differ in  because of the thermocouples' nonlinear
temperature coefficient of expansion such     response.
that temperature changes result in
predictable bending of the assembly.          Resistance Thermometers
Arranged in a spiral or helical
configuration, one end of the bimetallic      Rcsi:;;tance temperature detectors (RTDs)
element is fixed and the other end is         are contact sensors that measure
attached to a pointer. Properly calibrated,   temperature by a prcdictt1blc change in
tile angular position of the pointer can he   resistance as a function of temperature.
made to indicate temperature on a scale.      Platinum is Uw most popular resistance
                                              temperature detector material because of
                                              its excellent stability and its linecu
272 Infrared and Thermal Testing
response to temperature change. Other                      device. Transient heat flux can be related
materials used include nickel, copper,                     to the transient thermopile output and to
tungsten and iridium. In operation, the                    the geometry of the device.
resistance temperature detector may be
placed in a bridge circuit such that the                   Optical Pyrometers
bridge output voltage is a measure of the
resistance and hence the temperature at                    Optical pyrometers include brightness
the resistance temperature detector. A                     pyrometers and infrared pyrometers.
more accurate measurement may be                           Infrared pyrometers are also called
achieved by using a constant current                       infrared radiation thermometers. V<iriou:-.
source and a digital volt meter (DVM),                     types are discussed else\vhere.
such that the digital volt meter reading is
proportional to the resistance temperature                    Brightness pyrometers arc also called
detector resistance and hence the                          matching pyromctcrs. They incorporate a
temperature at the resistance temperature                  calibrated light source (lamp) powered by
detector.                                                  a calibrated current supply. Looking
                                                           through a viewer, the operator matches
   Thermistors are also sensors that                       the brightness of the target to be
measure temperature by a predictable                       measured with the brightness of the
change in resistance as a function of                      calibrated lamp. The adjustment control h
temperature. Thermistors are made of                       calibrated in temperature units, such that
semiconductor materials. \'\1hereas                        when the brightnesses are matched, the
resistance temperature detectors are low                   control indicates the temperature of the
impedance devices, thermistors are high                    target to be measured.
impedance devices. Thermistors are
typically more sensitive to temperature                    Basic Configurations of
changes than resistance temperature                        Infrared Radiation Sensing
detectors are but thermistors are not as                   and Imaging Instruments
stable.
                                                           In terms of configuration and operation,
Heat Flux Indicators                                       most thermal imagers are considered to be
                                                           extensions of radiation thennorneters or
Heat flux indicators are heat flow meters                  radiation thermometers plus scanning
and arc used to measure rates in                           optics. The performance parameters of
conduction, convection, radiation and                      thermal imagers arc extensions of the
phase change systems such as building                      performance parameters of radiation
walls, boiler tubes and air conditioning                   thermometers. To aid comprehension, the
ducts. A typical heat flux indicator                       basic measurement problem is discu~sed
consists of a sensitive thermopile,                        in this chapter in terms of the
composed of many fine gage                                 measurement of a single point. It is then
thermocouples connected in series on                       expanded to cover thermal scanning and
opposite sides of a flat core with known                   imaging.
and stable thermal resistance. The entire
assembly is covered with protective                            Figure 1 illustrates the basic
material.                                                  configuration of an infrared sensing
                                                           instrument (infrared radiation
   The voltage generated across the
thermopile is calibrated to be a measure of
the steady state heat flux through the
FiGURE 1. Basic configuration of infrared radiation thermometer.
         Target surface emits            Optics            Detector
                                                           converts
           infrared energy       ~                         infrared      Electronics
                               Lens Filter passes          energy to     amplifies
         I
                                                                             and
                               collects          selected                conditions   Dete<:t
                                                                         the signal
                               energy            spectral band
 I       II                    \                           '"electrical
Target   II I'-. Held                            I Isignal               J Measure
   size
             1 of                                                                   Output
         J / view                                                                     Monitor
         II
                                                                                      Control
                                                           Equipment for Infrared and Thermal Testing 273
thermometer), showing the components          detectors usually operate at or near room
necessary to make measurements.               temperature, whereas photon detectors
CoHecting optics (an infrared lens, for       are usually cooled to optimize
example) are necessary for gathering the      performance.
energy emitted by the target spot and
focusing this energy onto the sensitive          The mercury cadmium telluride
surface of an infrared detector. The          (HgCdTe) detectors in Fig. 2 are photon
processing electronics unit amplifies and
conditions the signal from the infrared       detectors cooled to 77 K (-196 oc =
detector and introduces corrections for
such factors as detector ambient              -321 "I:) for operation from 8 to 12 ~m
temperature drift and target effective
surface emissivity. Generally, a readout,     and to 195 K (-78 oc = -109 °F) for
such as a meter, indicates the target
temperature and an analog output is           operation from 3 to 5 ~m. Because of
provided. The output signal is used to        their fast response these detectors are used
record, display, alarm, control, correct or   extensively in high speed scanning and
any combination of these.                     imaging applications.
Infrared Detector                                In contrast to the mercury cadmium
                                              telluride detector, the radiation
An infrared detector is at the heart of       thermopile shown in l;ig. 2, is a broad
every infrared sensing and imaging            band thermal detector operating
instrument, whatever its configuration.       uncoolcd. It is used extensively for spot
Infrared detectors can sense infrared         measurements. Because it generates a
radiant energy and produce useful             direct current electromotive force
electrical signals proportional to the        proportional to the radiant energy
temperature of target surfaces.               reaching its surface, it is ideal for use in
Instruments using infrared detectors and      portable, battery powered instruments.
optics to gather and focus energy from
the targets onto these detectors are             The lead sulfide detector is typical of
capable of measuring target surface           those used in radiation thermometers that
temperatures with sensitivities better than   measure and control the temperature of
                                              very hot targets. Its peak sensitivity at
0.10 K (0.10 oc = 0.18 °F) and with           3 pm matches the peak energy emitted by
                                              a 1000 K (727 °C = 1340 °F) graybody.
response times in the microsecond range.      Because of the atmospheric absorption
An instrument that measures the               considerations discussed above, most
temperature of a spot on a target in this     infrared thermal imagers operate in either
manner is called an infrared radiation        the 3 to 5 pm or the 8 to 12 pm spectral
thermometer. An instrument that               region.
combines this measurement capability
with a means or mechanism for scanning        FIGURE 2. Response curves of various infrared detectors.
the target surface is called an infrared
thermal imager. It can produce thermal          } 1Q12
maps, or thermograms, where the
brightness intensity or color hue of any       ~
spot on the map represents the apparent
temperature of the surface at that point.      -?
    Figure 2 illustrates the spectral          E
responses of various infrared radiation
detectors. Radiant energy impinging on          -'0
their sensitive surfaces causes all infrared
detectors to respond with some kind of                       0.51 2 3 4 5 6 7 8 9 10 11 12 13 14
electrical change. This may be an
impedance change, a capacitance change,                                             Wavelength ),, ).Jm
the generation of an electromotive force
(EMF), known as voltage, or the release of       legend
photons, depending on the type of                  A Silicon, 298 K (25 ~c"' 77 cf).
detector. Infrared detectors are divided           B. Indium antimonide, 77 K(-196 ~c = -321 ~F).
into thermal detectors and photon detectors.       C. lead sulfide, 298 K(25 oc"' 77 or).
Thermal detectors have broad, uniform
spectral responses, somewhat lower               D. Mercury cadmium le!luride, 77 K(-196 cc =. 321 'F).
sensitivities and slower response times
(measured in millisecond); photon                  E. lead selenide, 243 K (-30 "C = -22 "F).
detectors (also called plwtodete(tors) have         F. Mercury cadmium telluride, 215 K {-58 oc-"- -73 or).
limited spectral responses, higher peak            G. Thermopile; 298 K(25 °( = 77 <f).
sensitivities and faster response times
(measured in microsecond). Thermal
274 Infrared and Thermal Testing
Infrared Optics - Lenses, Mirrors                                corrections for factors such as detector
and Filters                                                      ambient temperature drift and effective
                                                                 target surface emissivity. In radiation
There are two types of infrared optics;                          thermometers, a meter is usually provided
refractive (lenses, filters, windows) and                        to indicate the target's apparent
reflective (mirrors). Refractive optics                          temperature. An analog or dig!taLoutput
transmit infrared wavelengths of interest.                       signal is provided to record, display,
\-\'hen used for higher temperature                              alarm, control, correct or any
applications, their throughput losses can                        combination of these.
usually be ignored. When used in low
temperature measurement instruments                              Scanning and Imaging
and imagers, absorption is often
substantial and must be considered when                          When problems -in temperature
making accurate measurements. Reflective                         monitoring and control cannot be solved
optics, which are more efficient, are not                        by the measurement of one or several
spectrally selective and somewhat                                discrete points on a target surface, it
complicate the optical path. Reflective                          becomes necessary to spatially scan -
optics are used more often for low                               that is, to move the collecting beam or
temperature applications, where the                              the instrument's field of view - relative
energy levels cannot warrant throughput                          to the target. This is usually done by
energy losses.                                                   inserting a movable optical element into
                                                                 the collecting beam (Pig. 3).
    \Vhen an infrared radiation
thermometer is aimed at a target, energy                         line Scanning
is collected by the optics in the shape of a
solid angle determined by the                                    \'\'hen the measurement of a single spot
configuration of the optics and the                              on a target surface is not sufficient,
detector. The cross section of this                              infrared line scanners can be used to
collecting beam is called the field of view                      assemble information concerning the
(FOV) of the instrument and it determines                        distribution of radiant energy along a
the size of the area (spot size) on the                          single straight line. Quite often, this is all
target surface that is measured by the                           that is necessary to locate a critical
instrument at any given working distance.                        thermal anomaly. The instantaneous
On scanning and imaging instruments                              position of the scanning clement is
this is called the instantaneous field of                        usually controlled or sensed by an
view (IFOV) and becomes one picture                              encoder or potentiometer so that the
element on the thermogram. An infrared                           radiometric output signal can be
interference filter is often placed in front                     accompanied by a position signal output
of the detector to limit the spectral range                      and be displayed on a recording device
of the energy reaching the detector. The                         and/or fed out to a computer based
reasons for spectral selectivity will be                         process control system.
discussed later in this chapter.
                                                                     A typical high speed commercial line
Processing Electronics                                           scanner develops a high resolution
                                                                  thermal map by scanning normal to the
The processing electronics unit amplifies                         motion of a moving target such as a paper
and conditions the signal from the
infrared detector and _introduces
                     ...- ,- ~
FIGURE 3. Infrared radiation thermometer with addition of scanning element(s) for imaging.
                          Optics
        ,.....----..,Target surface emits
        /infrared energy                                            Detector       Electronics
                                  Filter                            converts       amplifies
                                                                    infrared      ood
                          Lens passes                               radiation to   conditions   Detect
                                                                    electrical     signal       Measure
                          collects selected                         signal
                                                                                  I
r 'spectral                                                      I
                                                           band
Target                                                                            Output
size
l II                                                                                            Monitor
                                           scanners or 1mager~                                  Control
                                                                 Equipment for Infrared and Thermal Testing 275
web or a strip steel process. The resulting                           real time scanning rate is increased.
output is a thermal strip map of the                                  Ivfultidetector scanners reduce the
process as it moves normal to the scan                                constraints on detector performance by
line. The scanning contiguration is                                   adding detector elements that share the
illustrated in Fig. 4. The output signal                              temporal spatial burden, allowing for
information is in a real time computer                                faster frame rates with no reduction in
compatible format and can be used to                                  signal~to~noise ratio or improving the
monitor, control or predict the behavior                              signal~to~noise ratio with no decrease in
of the target.                                                        frame rate.
Two-Dimensional Scanning                                              Electronic Scanning - Pyroelectric
- Thermal Imaging                                                     Vidicon Thermal Imagers
Three common imaging configurations                                   Electronically scanned thermal imaging
that produce infrared thermograms are                                 systems based on pyrovidicons and
optomeclwnical scanning, electronic scmmi11g                          operating primarily in the 8 to 14 pm
and focal plaue array imaging. Of the three,                          atmospheric window are widely used.
optomechanical scanning was the most                                  They provide qualitative thermal images
common until the mid~1990s. Focal plane                               and are classified as thermal vie\vers. A
array imagers have replaced scanning                                  pyroelectric vidicon or pyrovidicon is
imagers in most applications.                                         configured the same as a conventional
                                                                      video camera tube except that it operates
Optomechanical Scanning                                               in the infrared (2 to 20 pm) region instead
                                                                      of the visible spectrum. Image scanning is
To scan optomechanically in two                                       accomplished electronically in the same
dimensions generally requires hvo                                     manner as in a video camera tube.
scanning elements. Although an almost
infinite variety of scanning patterns can                             Focal Plane Array Imaging
be generated using two moving elements,
the most common pattern is rectilinear.                               First introduced to the commercial market
This scanning pattern is most often                                   in 1987, cooled infrared focal plane army
accomplished by two elements, each                                    imagers have evolved into compact,
scanning a line normal to the other. A                                qualitative and quantitative thermal
representative rectilinear scanner is                                 imagers wHhout scanning optics. These
illustrated in Fig. 5. Its scanning                                   devices have been replacing
mechanism comprises two oscillating                                   optomechanically scanned imagers for
mirrors behind the primary lens, a high                               many applications. The first uncooled
speed horizontal scanning mirror and a                                infrared focal plane array imagers lwve
slmvcr speed vertical scanning mirror.                                been used by the military for several years
                                                                      and became available to thcrmographers
   One performance limitation of                                      in 1997. Hgure 6 is a schematic of a
single~detector optomechanical scanners                               representative uncooled infrared focal
is a tradeoff between speed of response                               plane array imager.
and signal~to~noise ratio of the detector.
These instruments require high speed                                   FIGURE 5. Optomechanically scanned infrared imager.
cooled photodetectors that are pushed to
their performance limits as the desired                                                                                                  Horizontal
FIGURE 4. line scanner scanning                                                                                                                      mirror
configuration.
                                                                      Incoming
                            Target                                      infrared
                          distance
                                                                      radi~
                                                              Target
                                                              plane                        Objective
                                                                                                lens
sector
                                  Scan line width= spot size
276 Infrared and Thermal Testing
Performance Parameters                         thermographic instruments, therefore, do
of Infrared Sensing and                        not include temperature accuracy,
Imaging Instruments                            temperature repeatability and
                                               measurement spatial resolution
To select an appropriate instrument for an     (IFOVmeas).
application or to determine whether an
available instrument will pefform                  Generally, instruments that include the
adequately, it is necessary for the            capability to produce quantitative
thennographer to understand its                thermograms are more costly than
performance parameters.                        qualitative instruments and require
                                               periodic recalibration. Many applications
    The performance parameters for point       can be solved without the time and
sensing instruments {infrared radiation        expense of quantitative thermography;
thermometers) are temperature range,           others require true temperature mapping.
absolute accuracy, repeatability,
temperature sensitivity, speed of response,    Performance
target spot size and working distance          Characteristics of Point
(field-of-view spatial resolution), output     Sensing Instruments
requirements, sensor environment and           (Radiation Thermometers)
spectral range.
                                               The American Society for Testing and
    For scanners and imagers the               :~vlaterials defines infrared point sensing
performance parameters include                 instruments as infrared radiation
temperature range1 absolute accuracy,          thermometers even though they do not
repeatability, temperature sensitivity, total  always read out in temperature units.
field of view (TFOV}, instantaneous field      Some read out directly in apparent radi;:mt
of view (IFOV), measurement spatial            power units such as \'\'·nr2·s-J (or
resolution (IFOVmeas), frame repetition        llTU·ft-2.Jr1), some provide a closure or
rate, minimum resolvable temperature           alarm signal at a selectable temperature
(MRT), temperature sensitivity, image          and others others provide only difference
processing software, sensor environment        indications on an light emitting diode
and spectral range.                            display. 2
Qualitative versus Quantitative                Temperature Range
Thermography
                                               Temperature range is a statement of the
For scanners and imagers, one distinction      high and lnw limits over which the target
based on instrument performance                temperature can be measured by the
limitations is that between qualitative and    instrument. A typical specification would
quantitative thermography. A qualitative       be, for example, "temperature range 273
thermogram displays the distribution of        to 1273 K (0 to 1000 "C; 32 to 1832 "F)."
infrared radiance over the target surface,
uncorrected for target, instrument and         Absolute Accuracy
media characteristics. A quantitative
thermogram displays the distribution of        Absolute accuracy, as defined by the
infrared radiosity over the surface of the     National Institute of Standards and
target, corrected for target, instrument       TechnolObl)' (NIST) standard,3 entails the
and media characteristics so as to             maximum error, over the full range, that
approach a graphic representation of true      the measurement will have ·when
surface temperature distribution.
Performance parameters of qualitative
FIGURE 6. Typical uncooled infrared focal plane array imager.
Optics  Iris                                   Array bias
                  Window
                                    -=-~       Array address generator
                                               Preamplifiers                       Digital
                                                                                 processor
        Infrared local plane array                            Analog.to.digital
                                                                  converters
                                                              Equipment for Infrared and Thermal Testing 277
compared to this standard blackbody             (0.25 oc = 0.45 °F) at a target temperature
reference. A typical specification would
be, for example, "absolute accuracy:            of 298 K (25 oc = 77 °F)." In this case, the
±0.5 K (±O.S oc or ±0.9 °F) ±1 percent of       sensitivity of the instrument would
                                                improve for targets hotter than 275 K
full scale."
                                                (2 oc = 36 °F).
Repeatability
                                                Speed of Response
Repeatability describes how faithfully a
reading is repeated for the same target         Speed of response is how long it takes for
over the short and long term. A typical         an instrument to update a measurement.
specification would be, for example,            It is defined as the time it takes the
"repeatability (short and long term) of         instrument output to respond to a step
±0.25 K (±0.25 °C; ±0.45 °F)."                  change in temperature at the target
                                                surface. Figure 7 sl1ows this graphically.
   Temperature range and absolute               'fhe sensor time constant is defined by
accuracy will always be interrelated. For       convention to be the time required for
example, the instrument might be                the output signa) to reach 63 percent of a
expected to measure a range of                  step change in temperature at the target
temperatures from 273 to 473 K (0 to            surface. Instrument speed of response is
                                                usually specified in terms of a large
200 oc; 32 to 392 °F) ·with an absolute         percentage of the fuH reading, such as
                                                95 percent. As illustrated in Hg. 7, this
accuracy ±2 K (±2 oc = ±3.6 °1:) over the       takes about five time constants and is
entire range. This could alternately be         general1y limited by the detector used (on
specified as ±1 percent absolute accuracy       the order of microseconds for
over full scale.                                photodetectors and milliseconds for
                                                thermal detectors).
   On the other hand, the best accuracy
might be required at some specific                  A typical speed of response
                                                specification would be, for example
temperature, say at 373 K (100 oc =
                                                "speed of response (to 95 percent)='
212 oF). In this case, the manufacturer
should be informed and the instrument           0.05 s."
could be calibrated to exactly match the            It should be understood that there -is
manufacturer's laboratory calibration
standard at tlwt temperature. Because           always a tradeoff between speed of
absolute accuracy is based on traceability      response and temperature sensitivity. As
to the NIST standard,3 it is difficult for a    in all instrumentation systems, as the
manufacturer to comply with a tight             speed of response for a particular device
specification for absolute accuracy. An         becomes faster (instrumentation engineers
absolute accuracy of ±0.5 K (±0.5 °C =          call this a ·wider information bandwidth) the
±0.9 oF) or±1 percent of full scale is about    sensitivity becomes poorer (lower
as tight as can he reasonably specified.        signal-to-noise ratio). If the speed of
Repeatability, on the other hand, can be        response is specified to be faster than h
more easily ensured by the manufacturer         necessary for the application, the
and is usually more important to the user.      instrument may not have as good a
                                                temperature sensitivity as might be
Temperature Sensitivity                         possible otherwise.
Temperature sensitivity defines the             FIGURE 7. Instrument speed of response and time constant.
smallest target temperature change the
instrument will detect. Temperature                        Time-          About five
sensitivity is also called tllermal resolution             constant  time constants
or noise equil•alenl temperature difference
(NETD). It is the smallest temperature               100
change at the target surface that can be
clearly sensed at the output of the             "•"  90
instrument. This is almost always closely
associated ·with the cost of the                >    80
instrument, so unnecessarily fine                    70
temperature sensitivity should not be
specified. An important rule to remember        "c 60
is that, for any given instrument, target
sensitivity wHl improve for hotter targets      0"'
where there is more energy available for
the instrument to measure. Temperature          ~c
sensitivity should therefore be specified at
a particular target temperature near the        •~
low end of the range of interest.
                                                •~
   A typical specification for temperature
sensitivity would be, for example,                   10 -
"temperature sensitivity of 0.25 K
                                                                     Time (s)
278 Infrared and Thermal Testing
Target Spot Size and Working                  (radian). A 17.5 mrad (I degree) field of
Distance·                                     view means a d·D- 1 ratio of 60 to 1 and a
                                              35 mrad (2 degree) field of view means a
Target spot size D and working distance d     d·D-1 ratio of 30 to 1.
define the spatial resolution of the
instrument. In a radiation thermometer,       Output Requirements
spot size is the projection of the sensitive
area of the detector at the target plane. Jt  Output requirements for radiation
may be specified directly, "10 mm at 1m       thermometers can vary widely- from a
(0.4 in. at 3 ft)/' for example, but it is    simple digital indicator and an analog
usually expressed in more general terms       signal to a broad selection of output
such as a field of view solid angle           functions, including digital outputs
(10 mrad, 1 degree, 2 degree) or a            (binary coded decimal); high, low and
field-of-view ratio (ratio of spot size to    proportional set points; signal peak or
working distance~ for example, d/15,          valley sensors; sample and hold circuits;
d/30 or d/75). A milliradian (mrad) is an     and even dosed loop controls for specific
angle with a tangent of 0.001. A d/15         applications. On-board microprocessors
ratio means that the instrument measures      provide many of the above functions on
the emitted energy of a spot one-fifteenth    even inexpensive standard portable
the size of the working distance: 30 mm       models of radiation thermometers.
at 450 mm (1.2 in. at 18 in.), for example.
Figure 8 illustrates these relationships and  Sensor Environment
shows hmv spot size can be approximated
quickly based on working distance and         The sensor environment includes the
field-of-view information furnished by the    ambient extremes under which the
manufacturer. A typical specification for     instrument will perform within
spot size would be, for example, "target      specifications and the extremes under
spot size= 2 degrees from 1.0 m (39 in.)      which it can be stored without damage
                                              when not in operation. For a portable
to=.''                                        radiation thermometer, a typical
    This would take into account the          specification for sensor environment
                                              would be as follows.
shortest working distance at which the
instrument could be focused (1 m or             1. Operating temperature is 273 to 310 K
39 in.). For some instruments designed for         (0 to 37 oc; 32 to 100 °!').
very close working distances, the simple
d·D- 1 ratio does not always apply. If          2. Humidity is at 20 to 80 percent
closeup information is not clearly                 relative (not condensing).
provided in the product literature, the
instrument manufacturer should be               3. Atmospheric pressure is at -610 m to
consulted. For most applications and for           +2440 m (-2000 to +8000 ft) above sea
middle and long working distances                  level.
(greater than 1 m or than 3 ft), the
following simple calculation (Fig. 8) will      4. Storage (nonoperating) temperature
closely approximate target spot size:              ranges from 258 to 333 K (-15 to
=(1) D  u.d                                      +60 oc; s to 140 °F).
where D is about spot size, dis distance to       Frequently in process control
target and a is field-of-view plane angle     applications, the sensor must be
                                              permanently installed in a somewhat
                                              more extreme environment of smoke,
                                              soot, high temperature and even
                                              radioactivity. For these applications,
fiGURE 8. Determination of instrument's field of view.  Target
         j~ d                                                   ~~
                                                                       D ud
                                                                     I
legend
  D "' target spot size
  d :=distance to target
  u "'field of view (rad)
                                                        Equipment for Infrared and Thermal Testing 279
manufacturers provide a ·wide range of         wavelengths to reach the detector. (A
enclosures that offer special protective       combination of a spectrally selective
features such as air cooling, water cooling,   detector and a filter can also be used.)
pressurization, pmge gases and shielding.      This can make the instrume·nt highly
                                               selective to a specific material whose
Spectral Range                                 temperature is to be measured in the
                                               presence of an intervening medium or an
Spectral range denotes the portion of the      interfering background.
infrared spectrum over which the
instrument will operate. The operating            For general purposes and for measuring
spectral range of the instrument is often
critical to its performance and, in many       targets cooler than about 770 K (500 oc ~
applications, can be exploited to solve
difficult measurement problems. The            930 °F), most manufacturers of radiation
spectral range is determined by the            thermometers offer instruments operating
detector and the instrument optics             in the 8 to 14 pm atmospheric ·window.
(Fig. 9). Here, the flat spectral response of  For dedicated use on hotter targets,
a radiation thermopile detector is             shorter operating wavelengths are
combined with that of a germanium lens         selected, usually shorter than 3 pm. One
and an 8 to 14 pm band pass filter. The        reason for choosing shorter wavelengths is
instrument characterized is suitable for       that this enables manufacturers to use
general purpose temperature                    commonly available and less expensive
measurement of cool targets through            quartz and glass optics, which have the
atmosphere. The transmission spectrum of       added benefit of being visibly transparent
a 0.3 km (0.19 mi) atmospheric ground          for more convenient aiming and sighting.
level is also shown.                           Another reason is that estimating
                                               emissivity incorrectly \'l'ill result in smaller
   An infrared interference filter is often    temperature errors 'vhen measurements
placed in front of the detector to limit the   are made at shorter wavelengths.
spectral range of the energy reaching the      Thermographers have learned that a good
detector. The follmving three classes of       general rule to follow, particularly when
filters are common.                            dealing with targets of low or uncertain
                                               emissivities, is to work at the shortest
 1. High pass filters pass energy only at      wavelengths possible without
    ·wavelengths longer than a designated      compromising sensitivity or risking
    \\'avelength.                              susceptibility to reflections from visible
                                               energy sources.
 2. Low pass filters pass energy only at
    wavelengths shorter than a designated      Performance Characteristics of
    wavelength.                                Scanners and Imagers
 3. Band pass filters (like that in Fig. 9)    Because an infrared thermogram consists
    pass radiation ·within a designated        of a matrix of discrete point
    spectral band (8 to 14 pm, for             measurements, many of the performance
    example).                                  parameters of infrared thermal imagers are
                                               the same as those of radiation
   Spectrally selective instruments use        thermometers. The output of an infrared
band pass filters to allow only a very         Jine scanner can he considered as one line
specific broad or narrow band of
FIGURE 9. Spectral response of instrument determined by detector and optics spectra.
            General purpose
             band pass filter
                (8 to 14 1-1m)
       100
:!<    90                                                                     Them>C•pHc· (29H K)
       80
cc     70                                                                   Transmission of
       60                                                                   germanium
8.·~   50                                                                   (uncoated single
       40                                                                   optics)
  ~~   30
       20
~·~    \0
0c
v "~.
  w~
~'0'
"De
wW
,_> ~
·~ ~
~
                                  5 10 1S                               20
                                                  Wavelength /,. (IJm)
280 Infrared and Thermal Testing
of discrete point measurements. The           35 percent of the modulation lmlls{i'r
parameters of temperature range, absolute     (unction test used to check imaging spatial
accuracy, repeatability, sensor               resolution. Verification of imaging spatial
environment and spectral range are            resolution is described in detail later in
essentially the same for radiation            this chapter. The simple expression, D =
thermometers, line scanners and imagers.      adf can he used to estimate imaging spot
Others are derived from or are extensions     size at the target plane from
of radiation thermometer performance          manufacturer's published data by
parameters.                                   substituting the published instantaneous
                                              field of view for a.
   Qualitative thermal imagers (also called
thermal viewers) differ from quantitative     Measurement Spatial Resolution
thermal imagers (also called imaging          (IFOVmeas)
radiometers) in that thermal viewers do
not provide temperature or thermal            Measurement spatial resolution
energy measurements. For                      (IFOVmeas) is the spatial resolution of tlw
thennographers requiring qualitative          minimum target spot size on which an
rather than quantitative thermal images,      accurate measurement can be made in
therefore, some performance parameters        terms of its distance from the instrument.
are unimportant.                              An example of a typical measurement
                                              spatial resolution specification would be
Total Field of View                           uiFOVmeas = 3.5 mrad at 0.95 SRF." The
                                              0.95 SllF refers to 95 percent of the slit
For scanners and imagers, the total field of  response function test used to check
view (TFOV) denotes the image size in         measurement spatial resolution. This is
terms of total scanning angles for any        described in detail below. The simple
given lens. An example of a typical total     expression, D =ad can again he used to
field of vie"w specification would be         estimate measurement spot size at the
"TFOV = 20 degree vertical x 30 degrees       target plane from manufacturer's
horizontal" ('with standard lx lens) and      published data hy substituting published
would define the thermogram total target      measurement spatial resolution for a.
size by a simple trigonometric
relationships:                                Frame Repetition Rate
(2) I'                                        Frame repetition rate replaces speed of
                                              response and is defined as the number of
                                              times every point on the target is scanned
where d is working distance, H is total       FIGURE 10. Determination of total field of view for infrared
horizontal image size, Vis total vertical     imager.
image size, x is horizontal scanning angle
and y is vertical scanning angle. This is                     I
illustrated in Fig. 10.
                                                    ~,.:r--·~~-~ r
   The total field of view for a line
scanner consists of one scan line as shown     legend
in Fig. 4. The horizontal image size His                d =mean distance to the target (em, ft)
equal to the scan sector. The vertical                 H"' total horizontal image size=- d f2 tan (x/2}]
image size V equals the instantaneous
field of view. All other parameters are the        IFOV "'instantaneous field of view
same as for an imager.                            TFOV "' total field of view (target size)"' V x II
Instantaneous Field of View                             V =total vertical image size"' d (2 tan (y/2)]
                                                        x =image horizontal angular subteme (degrees)
Instantaneous field of vie''' (IFOV) in an              y =image vertical angular subtense (degr€es)
imager is very similar to that for a point
sensing instrument: it is tile angular
projection of the detector element at the
target plane. In an imager, however, it is
also called imaging spatial resolution and
represents the size of the smallest picture
element that can be imaged. An example
of a typical instantaneous field of vie\\'
specification would be "U:OV = 1.7 mrad
at 0.35 1vfTF. 11 The 0.35 MTF refers to
                                              Equipment for Infrared and Thermal Testing 281
in one second. This should not be             Descriptions of Thermal
confused with field rate. Some imagers are    Sensing and Imaging
designed to interlace consecutive fields,     Equipment
each consisting of alternate image lines.
This results in images less disconcerting to  Point Sensors (Radiation
the human eye. The frame rate in this         Thermometers)
case would be half the field rate. An
example of a typical frame repetition rate    Point sensors (radiation thermometers)
specification for an imager would be          can be further divided into temperature
"frame repetition rate::: 30 frames per       probes, portable hand held devices, online
second.11 For a line scanner, the term line   process control devices and specially
scan rate is used and is expressed in lines   configured devices.
per second.
                                              Temperature Probes
Minimum Resolvable Temperature
Difference                                    Temperature probes are low priced, pocket
                                              portable, battery powered devices that
Minimum resolvable temperature (MRT)          usually feature a pencil shaped sensor
or minimum resolvable temperature             connected to a small, basic readout unit.
difference (MRTD) replaces temperature        Generally, they are optically preadjusted
sensitivity and is defined as the smallest    for minimum spot size at a short vwrking
blackbody equivalent target temperature       distance. A S.O mm (0.2 in.) spot at a
difference that can be observed out of        20 mm (0.8 in.) working distance is
system noise on a thermogram. As in           typical. Temperature usually ranges from
radiation thermometry, this difference        about 253 to 573 K (-20 to 300 "C; -4 to
improves (becomes smaller) with
increasing target temperature and is          570 "F) and a sensitivity of ±1 K ( ±1 oc =
expressed in those terms. An example of a
typical minimum resolvable temperature        ±1.8 °F) is achieved easily. Probes are
difference specification for a line scanner   designed for closeup measurements such
or an imager would be ''MRTD = 0.05 Kat       as circuit board analysis, troubleshooting
297 K target temperature (0.05 "Cat           of electrical connections, inspection of
25 "C; 0.09 "Fat 77 "F)."                     plumbing systems and biological and
                                              medical studies.
    Minimum resolvable temperature
difference may also depend on the spatial     Portable Hand Held Devices
frequency imposed by the test discipline.
The test technique for checking minimum       Portable hand held radiation
resolvable temperature difference is          thermometers are designed for middle
described elsewhere.                          distance measurements and, with few
                                              exceptions, operate in the 8 to 14 pm
Thermal Imaging Display and                   spectral region and are configured like a
Diagnostic Software Overview                  pistol for one-handed operation and
                                              aiming. They are usually optically
Thermography applications often require       preadjusted for infinity focus. A typical
extensive thermal imaging display and         2 degree field of view resolves a 75 mm
diagnostic software. Thermal imagers           (3.0 in.) spot at a 1.50 m (60 in.) working
feature image processing capabilities that    distance and a 300 mm (1 ft) spot at a
may be divided into five categories, one      9 m (30 ft) working distance. Most
or more of which may be used in the            instruments in this group incorporate
same application. These categories are         microcomputers with limited memory
quantitative thermal measurements of          and some have data Jogging capabilities.
targets; detailed processing and image         An open or enclosed aiming sight is
diagnostics; image recording, storage and      provided and, in some more recent
 recovery; image comparison (differential      models, a projected laser beam is used to
or multispectral thermography); and            facilitate aiming of the instntment as
database and documentation.                    shown (Fig. 1 1). Note that the laser beam
                                               does not represent the field of view.
                                                  A measurement readout is always
                                               provided and usually the temperature is
                                               shown on a digital liquid crystal display.
                                               These instruments are powered with
                                               disposable batteries and have low power
                                               drain. Temperature ranges are, typically,
                                               from 270 to 1270 K (0 "C to 1000 "C;
                                               30 oF to 1800 °1:). Temperature sensitivity
                                               and readability are usually 1 percent of
                                               scale (1 K or 1 oc or 2 °F) although
282 Infrared and Thermal Testing
sensitivities on the order of 0.1 K (0.1 oc  specific target, this type of instrument
                                             remains there for the life of the
or 0.2 oF) are achievable. Response times    im.trument or process. With few
arc on the order of fractions of a second,   exceptions, these instruments operate on
usually limited by the response of the       line power. The measurement value can
readout.                                     be observed on a meter but is more often
                                             used to trigger a switch or relay or to feed
   Hand held radiation thermometers are      a simple or sophisticated process control
used extensively in applications where       loop. Most of online monitoring and
spot checking of target temperatures is      control sensors send signals to universal
sufficient and continuous monitoring is      indicator/control units that accept inputs
not required. Hand held radiation            from various types of industrial sensors.
thermometers have become an important
part of many plant energy conservation          Because this instrument group is
programs. Process applications include       selected to perform a specific task; a
monitoring mixing temperatures of food       shopping list format is provided to the
products, cosmetics and industrial           customer by the manufacturer so that all
solvents. lvHcrocomputers enable hand        required features can be purchased,
held instruments to incorporate special      including environmental features such as
features such as the ability to store 60     water cooled housings, air purge fittings
readings for future retrieval and printout.  and air curtain devices. Emissivity set
                                             controls, located in a prominent place on
Online Process Monitoring and                a general purpose instrument, are more
Control Devices                              likely to be located behind a bezel on the
                                             sensor on these dedicated units, where
Online monitoring and control sensors        they are set once and then locked. The
arc for dedicated usc on a product or a      spectral interval over which the sensing
process. Permanently installed where it      head operates is selected to optimize the
can measure the temperature of one           signal from the target, to reduce or
                                             eliminate the effect of an interfering
FIGURE 11. Infrared radiation instruments:   energy source or to enable the instrument
(a) hand held infrared radiation             to measure the surface temperature of
thermometer with laser aiming and            thin films of material that are largely
(b) infrared focal plane array imager for    transparent to infrared radiation. The
qualitative thermography.                    capability for spectral selectivity has made
(a)                                          these instruments important in the
                                             manufacture of glass and thin film
(b)                                          plastics.
                                             Devices with Special
                                             Configurations
                                             Special configurations of infrared
                                             radiation thermometers include (1) ratio
                                             pyrometers (also called two·color
                                             pyrometers), (2) infrared radiometric
                                             microscopes, (3} laser reflection
                                             pyrometers and (4) fiber optic coupled
                                             pyrometers.
                                             Equipment for Infrared and Thermal Testing 283
1. Two-color pyromders, or ratio pyrometrrs,                    line scanners are in this configuration.
   are a special case of the online                             The output signal information is in a real
   instrument. Ratio pyrometers are                             lime computer compatible format and can
                                                                be used to monitor/ control or predict the
   particularly useful in high temperature                      behavior of the target.
   applications above 573 K (300 °C =
                                                                   Like the online point sensor, these line
   572 °F) and in measuring small targets                       scanners are usually permanently installed
   of unknown emissivity, provided the                          where they monitor the temperature
                                                                profile at one site of the process,
   background is cool, constant and                             remaining there for the life of the
   uniform. The emissivity of the target                        instrument or the process. Likewise, they
   need not be known if it is constant                          are usually fitted with environmental
   and reflections are controlled. The                          housings and preset emissivity
   target does not need to fill the field of                    compensation sets. The best applications
                                                                for this scanner are in online, real time
   vkw provided the background is cool,                         process monitoring and control
   constant and uniform. The                                    applications where they are integrated
   measurement is based on the ratio of                         with the process host computer system. lt
   energy in two spectral bands, so                             is not unusual to find line scanners at
                                                                multiple locations in a process with all of
   impurities in the optical path resulting                     them linked to the host computer.
   in broad band absorption do not affect
   the measurement. Ratio pyrometers                               In the 1990s, infrared line scanners
   are usually not applicable to                                based on linear focal plane arrays came
   measurements below 573 K                                     into use. This type of instrument
                                                                frequently uses an uncooled array of
  (300 oc ~ 572 °F).                                            thermal detectors (radiation thermopiles).
                                                                This scanner has no moving parts. The
2. Infrared radiometric microscopes are                         linear array is oriented perpendicular to a
   configured like a conventional                               process or a target moving at a uniform
   microscope and, by using reflective                          rate. The scanner output may be used to
   microscope objectives and beam                               develop a thermogram or the data for
   splitters, the operator can                                  each pixel can he fed directly to a host
   simultaneously view and measure                              computer and used to monitor and
   targets down to 10 pm in diameter                            control the process. Instruments of this
   with accuracy and resolution of about                        type have been used to monitor moving
   0.5 K (0.5 °C" I 0 1').                                      railroad cars for overheated wheels and
                                                                brake assemblies.
3. Laser reflection pyrometers use the
   reflected energy of an active laser to                       Special Purpose Devices
   measure target reflectance. A built-in
   microcomputer calculates target                              Special purpose configurations of line
   effective emissivity and uses this figure                    scanners include one type of portable line
   to provide a corrected true temperature                      scanner and a number of aerial mappers
   reading. This instmment, though                              that scan a line normal to the motion of
   expensive, is useful for measurement                         the aircraft and develop a thermal strip
   of high temperature specular target                          map. ~,fany of these mappers have been
   surfaces in adverse environments.                            replaced by low cost fonwmf looking
                                                                infrared scanners based on staring focal
4. Fiber optic coupled pyrometers make                          plane arrays.
   possible the measurement of normally
   inaccessible targets by replacing the
   optic with a flexible or rigid fiber optic
   bundle. This limits the spectral
   performance and hence the
   temperature range to the higher values
   but has allowed temperature
  measurements to be made ·when
   previously none \vere possible.1
              Line Scanners
                   Line scanners are divided into online
                   process control devices and special
                   purpose scanners.
                Online Process Control Devices
                   Online (monitoring and control) line
                   scanners are high speed, online
                   commercial line scanners that develop
                   high resolution thermal maps by scanning
                   normal to the motion of a moving target
                   such as paper web or a strip steel process.
                   The vast majority of commercial infrared
284 Infrared and Thermal Testing
PART 2. Thermographic Imagers
Imagers (thermographic instruments)          visible spectrum. Aside from the tuhe and
include both qualitative and quantitative    germanium lens, which are expensive,
imagers.                                     these systems use television recording
                                             accessories. In comparison with other
Qualitative Thermographic                    infrared imaging systems, the picture
Imagers                                      quality and resolutiot~ are good,_ .
                                             approaching conventional televtswn
Qualitative thermal imagers are also called  format. The thermal image can be viewed
thermal viewers. They include                or videotaped with equal convenience
mechanically scanned, electronically         and no cooling is required.
scanned (pyrovidicon) and staring focal
plane array imagers.                            Pyrovidicon systems do not
                                             intrinsically offer quantitative
Mechanically Scanned Thermal                 measurement capability but some
Viewers                                      manufacturers offer models in which an
                                             integrated radiation thermometer is bore
Mechanically scanned thermal viewers are     sighted with the scanner and its
moderately priced battery powered            measurement is superimposed on the
scanning instruments that produce a          video display along with a defining reticle
qualitative image of the radiosity over the  in the center of the display. Thermal
surface of a target. The battery packs are   resolution of flicker free pyrovidicon
rechargeable and usually provide 2 to 3 h    instruments is between 0.2 and 0.4 K (0.2
of continuous operation. These one-piece,    and 0.4 oc; 0.4 and 0. 7 °1').
lightweight instruments, designed to be
simple to operate, feature thermoelectric       Pyroelectric devices have no direct
detector cooling provided by a battery       current response and a basic pyrovidicon
powered cooler. Although not designed        imager's display will fade when the device
for absolute temperature measurements,       is aimed at an unchanging thermal scene.
they can demonstrably sense temperature      Early pyrovidicon imagers needed to be
differences of tenths of degrees and can be  panned to retain image definition. To
used for targets from below 273 to 1773 K    enable fixed monitoring, crude, flag type
(0 to 1500 oc; 32 to 2372 °F). Typically,    choppers were devised to interrupt the
the total field of view is from 6 to 8       image at adjustable chop rates. However,
degrees high and from 12 to 18 degrees       this resulted in a blinking image that was
wide, with spatial resolution of 2 mrad,     disconcerting to the eye. These choppers
10 mm at 2.0 m (0.4 in. at 7 ft). Images     have been replaced by synchronous
are video recorded by means of a             choppers that chop the image in
conventional video tape recorder output      synchronism with the electronic scan rate
jack and video recorder accessories.         and produce flicker free images on the
                                             display. Pyrovidicon viewers operate well
   The broad applications for thermal        in the 8 to 14 pm atmospheric
viewers are generally limited only to those  transmission window. Operating costs are
in which the temperature measurements        very low because no cooler or coolant is
are not critical and recording quality does  required.
not need to be optimum. The
combination of a thermal viewer (to          Staring Infrared Focal Plane Array
locate thermal anomalies) and a hand         Thermal Viewers
held thermometer (to quantify them) can
be a powerful and cost effective             Staring infrared focal plane array thermal
combination.                                 viewers arc direct adaptations of devices
                                             developed for military and aerospace
Electronically Scanned Viewers               night vision and missile tracking
(Pyrovidicon Imagers)                        applications. For these applications,
                                             performance emphasis is on picture
Pyrovidicon (pyroelectric vidicon) imagers   quality rather than measurement
are electronically scanned video cameras.    capability.
The camera tube is sensitive to target
radiation in the infrared rather than the       Instruments using cooled platinum
                                             silicide {PtSi) staring arrays with as many
                                             as 512 x 512 elements are available.
                                             Instruments using cooled indium
                                             Equipment for Infrared and Thermal Testing 285