PART 1. Thermal Detectors
In thermal detectors the incident              temperature variations and thus need a
                                               chopper modulating the incoming
radiation heats the surface. This heating      radiation to maintain a signal output,
affects properties of the heated material      unless the system is panned over the
                                               scene. This added complexity is a severe
such as its electrical conductivity, which     drawback.
in turn causes the signal output to vary.
One characteristic specific to thermal            The figure of merit for pyroelectric
detectors is that the response is              detectors is the pyroelectric coefficient p
independent of the wavelength. To get a        defined as the slope of the material
wavelength band for a specific application     polarization P versus temperature T, at the
an interference filter rejecting radiation of  operating temperature:3
unwanted wavelengths will have to be
                                                           aP
placed in front of the detector.
   The limit of sensitivity of thermal         (3) aT
detectors is given by the effectit'e
conductivity GR:l
·where a= 5.67 x 10-12 V\'·cm-Z.K-4 is            This effect can be improved with the
Stefan's constant, Tis the detector            application of an electrical field bias. This
temperature and A is the detector              is referred to as the field enhanced
sensitive area. D* is the detectivity limit:
                                               pyroelectric effect or the ferroelectric
                                               bolometer effect. In such a case, p comes
                                               to the following:3
                                                               E  aedp
                                                                  aT dE
                                               f(4)
~ ~(2) D •                                     p ~ Po +
            4kT G                                              0
·where k (\'V·m-1-K-1) is the thermal          with Po being the pyroelectric coefficient
conductivity and G is the limit of GR.         \Vithout bias, the dielectric permittivity
   Theoretically a maximum of                  and E the applied electrical field.
                                               Pyroelectric elements can be made as
0" = 1.8 x 1010 cm·\'(Hz)·VV-1 can be          point or image detector.
obtained with a thermal detector;              Photonic Detectors
practical factors limit the effective          In photonic detectors the signal is
detector performance. Modern                   obtained by measuring directly the
technology has produced a detectivity          excitation generated by the incident
limit of D* ~ 7 x 108 cm·'-'(Hz·\V-1).         photons. Heating of the sensitive surface
                                               is unnecessary. Photonic detectors are of
Pyroelectric Detectors                         two types: photoemissive and quantum
                                               (photoelectric, photovoltaic or
Pyroelectricity is defined as the property     photoconductor).
of certain crystals to produce·a state of
electric polarity in response to a change in   Photoemissive Photonic Detectors
temperature. 2 A broad class of thermal
                                               For photoemissive plwtonic detectors, the
detectors are p}'roelectric detectors, for     signal observed expresses the measured
which electric charges are generated by        electron flow (that is measurement of a
                                               current i) pulled away from the
incident radiation absorption (heating)        photocathode under the effect of both the
below the curie temperature. The curie         incident photons and a static polarization
temperature is that below which there is a     (rig. 1). The spectral sensitivity depends
spontaneous magnetization in absence of        on the properties both of the material
an externally applied magnetic field. A        used for the photocathode and of the
change in detector temperature generates       outer envelope infrared transmittance.
a transient change in the surface charges      Typical values span from ultraviolet to
thus causing a transient current available
for pickup by the readout unit.
Pyroelectric detectors are sensitive only to
186 Infrared and Thermal Testing
near infrared: 0.2 to 1 pm. Solid state              made these detectors compact, reliable,
photoemissive detectors are also possible.           robust and consequently popular.
   In photomultiplier tubes electrons are               For photoconductive detectors an
accelerated and multiplied by secondary              external current is necessary to measure
emission from internal plates called                 conductivity change whereas
dynodes. Multiplication factors of 105               photoelectric (photovoltaic) detectors act
to 107 can be obtained for 10 stage tubes.           as power generators supplying a signal
These detectors are point detectors                  without need for polarization. Because
although image converter tubes are made              biasing current is needed for
as well, with such uses, for instance, as            photoconductive detectors, high charge
night vision image intensification for               capacity alkaline batteries can be used to
military and surveillance applications.              induce minimum noise and ripple. Low
                                                     noise is essential to achieve stable results.
Quantum Detectors                                    In this respect, because photovoltaic
                                                     detectors supply a signal by themselves,
Quantum detectors are solid state detectors          they are much more attractive than
in ·which photon interactions either                 photoconductor detectors requiring less
change conductivity (photoconductive                 complex readout circuits. Common
detectors) or generate voltage                       materials used in photoelectric sensors
(photoelectric detectors, or photovoltaic            (photodiodes and phototransistors)
detectors). Because no heating is needed             include silicon, indium arsenide, indium
as for thermal detectors, their response             antimonide and mercury cadmium
time is short. The solid state structure has         telluride.
FIGURE 1. Schematic diagram of                          Figure 2 presents the spectral
photoemissive detector: (a) side view;               detectivity curves for the most common
(b) axial view.                                      detectors. On these curves, sharp cutoff
                                                     response is observed at longer
(a)                                    Photocathode  wavelengths. This can be explained
                                                     because of the presence of different
     Glass envelope                                  energy levels, within the atomic structure.
                                                     At low energy (low valence level)
  ""                                                 electrons stay close to the nucleus. If
                                                     enough energy is supplied to electrons,
   Incident                                          they cross the forbidden baud, which frees
   photons                                           them from nucleus attraction and enables
                                                     them to participate in an electric current.
                                                     At Ions ·wavelengths the photons transmit
                                                     less energy to electrons:
                                                     (5)
                                          Vacuum     where lV is the radiated energy ~oule),
                                                     cis the velocity of light= 3 x 10 m·s-1,
                     Tube connections                II is Planck's constant= 6.63 x l0-34 J·s-1
(b)                                                  and A is the radiation wavelength (meter).
       Incident                                         Because electrons cannot cross the
       photons                                       forbidden band and thus stay in the
                                                     valence band, there is a sharp cutoff in
                                                     the spectral detectivity curves.
                                                        At srnall wavelengths, photons have
                                                     greater energy and penetrate deeper in the
                                                     substrate, passing through sensitive areas
                                                     of the semiconductor without interacting.
                                                     This causes a gradual loss of detectivity as
                                                     observed on Fig. 2. Imaging detectors are
                                                     discussed below.
                     Static polarization             Infrared Imaging Devices
                                                     A class of detectors lend themselves
                                                     without mechanical scanning operations
                                                     to imaging applications~ that is, to the
                                                     production of an array of points (also
                                                     called pictllre elements, or pixels) in either
                                                     one dimension, as in a line array, or in
                                                     Noncontact Sensors for Infrared and Thermal Testing 187
two dimensions, as in television image                      operation. Pyroelectric tubes are thermal
generation. Although infrared films such                    detectors where the signal is proportional
as liquid crystals made from specific dyes
sensitive in the 1 to 3 pm range are                        to the absorbed enerm•. For certain
available, they are impractical for real                    ferroelectric crystal materials such as
time imaging in nondestructive testing.                     triglydne sulfate that have a high
                                                            pyroelectric coefficient p, heating or
   In imaging applications the output of
the detector device produces the image in                   cooling of the crystal slice creates an
one dimension or two dimensions. Two                        accumulation of charges. This is the
main image forming processes exist:
(1) direct image formation with a detector                  pyroelectric effect, which results in a
array, pyroelectric detector or infrared                    change of polarization.5
film; (2) electromechanical scanning of
                                                               Pyroelectric tubes are similar to
the scene with a single detector.
                                                            standard vidicon television cameras
Pyroelectric Detectors                                      except for the face plate and target
Back in the 1960s1 the first successful                     material (Fig. 3). As the infrared image
infrared commercial products based on
pyroelectric detectors (vidicon tubes and                   impinges on the pyroelectric target1 a
single pyroelectric elements) were                          temperature distribution and in turn a
produced.4 The major advantage of this                      charge distribution appears on the
kind of thermal detector is the ambient or                  pyroelectric material. The electron beam
close to ambient temperature mode of
                                                            scans this material and two things may
                                                            happen. If no radiation has been absorbed
                                                            at the scanned spot there is no charge (no
                                                            polarization) and the electron beam is
                                                            redirected toward the mesh. On the
                                                            contrary, if radiation has been absorbed,
FIGURE 2. Spectral detectivity curves for infrared detectors. Atmospheric absorption is also
indicated.     Unit  conversions  for  temperature  scale:  K-  273  =  0       0  X 1.8) + 32 = 0 F. Unit
                                                                          (;  ((
conversion for measure of distance: em + 2.54 = in.
         1011                                                        n
                                                                                             Perfect
  i7                                                                                         photovo!taic
                                                                                             detector
  I
""1:                                                                            1- Perfect
  ~n~~~~~~~~~~l'~t--.~~[':0eE                                                                 photoconductor
  ~ 1010
  " ~"'                                                                          !"\. detectorth
*«
0                                                                                       , / GeHg (28 K)
               I'                 I                                                r'"'" "m'' d'''"O'
  0                                                                    '
                                                                     i 1-1, (77 K)
      JO'
                                                                                              Pyroe!ectric detector
                                                                                       Bolometer
                                       I I '"f                                 'J'-Thermopil
                                                                        ·: (<
                     2 3 4 5 6 7 8 9 10 11 12 13 14
                                       Wavelength /,, J-Im
  legend
       0 =atmospheric absorption (environment, T = 295 K f22 oc = 8 cfJ, 2 steradian)
       AuGe =gold germanium
       GeHg =germanium mercury
    HgTeCd =mercury telluride cadmium
         lnAs =indium arsenide
         lnSb =indium antimonide
          PbS =lead silicon
        PbSe = lead selenide
           PC = photoconductive
           PV = photovoltaic
188 Infrared and Thermal Testing
charges accumulate and the electron                                      Pyroelectric tubes have the following
                     beam reaches the signal electrode, thus                               drawbacks.
                     causing a current to appear. As the
                     elet·tron beam is scanned over the surface,                            1. Their dynamic range is small (30 dB).
                     the video signal appears at the tube                                   2. Their linearity is poor, with less
                     output.
                                                                                               effective beam readout toward the
                         Because charges are released only when                                target edge.
                     the temperature of the pyroelectric                                    3. Their life span is restricted, typically
                     material changes, such tubes cannot                                       10 000 h, or 13 months at 24 h per
                   produce images of a static scene. If only                                   day.
                     part of the scene is dynamic or moving, a                              4. Because pyroelectric materials are
                     flying aircraft for instance, only the                                    piezoelectric they require careful
                     moving part is observed. This effect can                                  mechanical design to avoid
                     be useful in applications such as fire                                    microphonic noise from excessive
                     detection where only the fast temperature                                 target vibrations.
                     changes of flames are seen. Another use
                     may be nondestructive testing of parts                                   Despite these drawbacks, pyroelectric
                     moving on a conveyor belt.                                            tubes are attractive because of the
                                                                                           following advantages.
                      If the requirement for a scene to be
                     dynamic is undesired, the camera can be                                1. They do not need cooling.
                     panned or the radiation can be modulated                               2. They do not consume much power.
                   using a mechanical chopper. Camera                                       3. They are relatively inexpensive..
                     panning has the advantage of simplicity                                4. They are not restricted to a fixed
                     and reliability because no part is moving
                     other than the panning mechanism.                                         image format, as are detector arrays.
                                                                                               Changing the electron beam scanning
                     In the chopped (shuttered) mode, a                                        rate suffices to obtain another video
                                                                                               format.
                     rotating chopper mounted in front of the
                     tube shuts off the scene during one field                                In the 1990s developments in
                     causing target cooling, a negative image is                           pyroelectric detectors made it possible to
                     then produced. 'A1hen the target is                                   produce pyroelectric arrays.6•7 These
                     exposed again, the radiation distribution                             two-dimensional arrays (32 x 32 in 1987;
                     heats the pyroelectric material and the                               100 x 100 in 1990) are made of
                    positive image is reformed. Although a                                 ferroelectric ceramic thin film such as lead
                     signal is continuously produced it cannot                             scandium tantalate. They offer high
                     be displayed in this form because it is                               detectivity yet produce slow scan images
                    composed of alternating fields causing                                 (1.0 Hz) without needing to cool.
                     heavy flickering of the useful positive                               Applications include low cost consumer
                     field. Special electronics make it possible                           products for detection of flames, detection
                     to overcome this problem by displaying                                of heat emitted by warm objects such as
                     the positive and reverted negative image.                             people (for intruder detection), medical
                                                                                           thermography and transport monitoring.
                        Pyroelectric material absorbs radiation                            Among advantages of these monolithic
                    evenly over a broadband wavelength                                     chips of pyroelectric ceramic are the
                     spectrum, so the tube sensitivity is mainly                           following.
                    determined by the input window
                    material. Germanium (3 to 5 pm and 7 to                                 1. They are more rugged than
                     20 pm) and zinc selenide (0.6 to 20 pm)                                   pyroelectric tubes with fragile glass
                     are the materials most commonly used for                                  envelopes.
                     tube windows.
                                                                                            2. They are easy to operate, with small
FIGURE 3. Schematic diagram of pyroelectric vidicon tube.                                      voltage requirements.
                                                                                  Cathode   3. They are compact.
                     ~Video signal                                                         For these pyroelectric arrays, rcsponsivity
                                                                                           variations from clement to element are
                                Amplifier                                                  typically less than 10 percent. Absolute
                                                                                           temperature measurement thus requires
                                                                                           individual calibration of each element
                                                                                           which degrades considerably the image
                                                                                           acquisition time.
                                                                                              Ferroelectric materials can be used in
                                                                                           two modes: pyroelectric mode or dielectric
                                                                                           mode. The more conventional mode is
                                                                                           pyroelectric for which the signal origin is
                                                                                           the change of polarization because of the
                                                                                           heating of the detector by the incident
                                                                                           radiation, as described above. In the
                                                                                           dielectric mode, the change of
                                                                                           permittivity with temperature is used: this
                                                                                           change of permittivity is sensed as a
                                                                                           change in voltage across the detector after
                                                                                           Noncontact Sensors for Infrared and Thermal Testing 189
a proper bias has been applied. The          Focal Plane Arrays: Schottky
drmvback of the dielectric mode of           Barrier Detectors
operation is the need to stabilize the
detector temperature.                        This type of detector was first proposed in
                                             1973 by Shepherd and Yang. 10 Since then
    Improved spatial resolution can be       large arrays (512 x 512) have been
obtained for pyroelectric imaging            commercially introduced by many
detectors by reticulating the detector       companies. Infrared cameras are also
surface to reduce the lateral heat spread.   fabricated as large one~dimensional arrays
This reticulation can be done by ion beam    such as 1024 x 1. 11 In this design,
machining a pattern of narrow groves at      horizontal scanning is done electronically
30 to 40 pm depth all over the               in the detector plane whereas the vertical
pyroelectric target.K                        scanning is achieved by optomechanical
                                             means, by camera panning12 or by scene
    In qualitative infrared nondestructive   displacement with parts moving on a
testing, pyroelectric based infrared         conveyor belt or air lifted.
cameras can be an excellent choice.
Quantitative measurement is also possible.      The most common type is platinum
In some configurations the rotating          silicide detectors operating in the
chopper, which has an high emissivity        photoemissive mode and operating in the
surface, provides a knmvn temperature        3 to 5 J-Im band ·with cutoff wavelength of
reference from which scene temperature       5.6 pm. Gallium silicide is also available
can be determined. ~vfeasurement of the      in the 8 to 14 and 8 to 16 ~m bands.
chopper temperature is carried out           Platinum silicide detectors are often
indirectly by monitoring the signal from a   fabricated with an aluminum mirror over
single~element pyroelectric detector signal  the sensitive area and are illuminated
caused by a small blackbody target viewed    from the back. The mirror enhances the
through the chopper. The blackbody           platinum silicide responsivity but restricts
temperature is adjusted through a peltier    the response to wavelengths greater than
device so that no temperature differential   1 J-Im because of the absorption by the
is observable between the chopper and        silicon. 13,14 \-\'ith respect to intdnsic
the blackbody. The blackbody temperature     photon detectors such as indium
is then measured using a thermistor.9        antimonide, quantum efficiency of
                                             platinum silicide is rather small
Focal Plane Arrays (FPAs)                    (10 percent versus 85 percent).
for Infrared Testing
                                                The design is generally similar to video
In the 1970s a new imaging device began      charge coupled devices both for storage
revolutionizing the infrared community.      and readout circuits. The radiation
Large infrared arrays have simplified        induces charges that are stored in a
infrared camera construction. Because of     capacitor like insulating layer. Charges are
thh technology, all that are needed to       then transferred to the neighbor element
build an infrared camera are the optics,     under the effect of an electric field. Stored
the focal plane array, the associated        charges are next transferred in this
electronics and in some cases a cooling      fashion element by element up to the
unit. Similar to conventional video charge   array output where the signal is available.
coupled devices, these chips do not          A multiphase (2 or 3 phases) clock
require any electromechanical scanning       performs these step transfer processes. The
mechanism or other moving parts for          video signal is generated by sequentially
image forming and are less cumbersome        scanning all the rows in the array and by
and fragile than pyroelectric tubes. The     multiplexing each row. In Jarge arrays
video signal is obtained directly by an      (512 x 512), for compatible television rate
on~chip electronics drive. A variety of      signal, clock rate greater than 8 MHz is
technOlogies have emerged. The present       required to read all the detectors during
discussion reviews the schottky barrier,     one frame. The fill factor is greatly
superlattice, intrlnslc and Z plane          improved (up to 90 percent) if the readout
technologies.                                circuits are under the detector array.
   Because of the restricted applications       Charge injection devices are also used
(military, law enforcement,                  in focal plane arrays. Charge injection
nondestructive testing), the price of such   devices are similar to charge coupled
detectors, especially the silicon based      devices but the generation of the video
ones, has been slow to approach those of     signal is different. In charge injection
mass production consumer market              device detectors, the video signal
technologies such as the video tape          comprises the substrate current caused by
camcorder.                                   charge injection, rather than charge
                                             transfer as in charge coupled devices. This
                                             current is proportional to the received
                                             photons. Charge injection device
                                             detectors are less prone to blooming.
                                             Moreover, charges are Jess affected by
190 Infrared and Thermal Testing
radiation during device reading after the        because they generate charges
accumulation interval. Because of the            spontaneously under illumination by
addressing mode, cells can be read               incident radiation. Thermal charge
individually.                                    generations because of impurities in the
                                                 material degrade the signal, mainly
   Platinum silicide is the more mature          because of the shockley~read process and
schottky barrier detector. Its main              the auger process (charges generated
drawback is its need for cooling to 77 K         through impact ionization by carriers
(-196 "C ~ -321 "F). Other metal silicide        whose energy exceeds the forbidden band
arrays have been made to operate at              gap). Refinement in fabrication processes
longer wav('lengths; among them iridium          should improve these aspects.
siliride, nk kel silicide and cobalt disilicide
are suitable for imaging applications.              As mentioned in the case of
Iridium silicide has been reported to have       superlattice detectors, hybrid technology
a cutoff \vavelength of 7.3 Jlnl at 62 K         where detector layers are fused or glued
(-211 "C ~ -348 "F), 9.6 pm at 40 K              on silicon readout circuits is attractive
(-233 "C ~ -388 "F) and 10.7 pm if the           because silicon process is a well
detector is biasect.t5,l 6 Iridium silicide      established fabricating process. Such
arrays are more difficult to fabricate           hybrid arrays are fabricated with mercury
because impurities have a strong influence       cadmium telluride detectors in other sizes,
on performance. Cooling below 60 K               such as 128 x 128, 8 to 12 pm19 and
(-213 "C ~ -352 "I') is also a problem for       256 X 256, 3 tO 5 pm.ZO
silicon technology because charge storage
is difficult at low temperatures. 17                An alternative fabricating technique is
                                                 to grow mercury cadmium te11uride cells
Focal Plane Arrays: Superlattices                on gallium arsenide buffers that are
                                                 themselves grown on silicon substrate
In superlattice detector arrays, alternating     containing bipolar preamp1ifier transistors
layers of different semiconductors of            and readout circuits. Advantages of this
different thickness makes it possible for        monolithic configuration include
the wavelength of absorbed radiation to          improved uniformity, reduced (-1 noise
be tuned: photoconduction occurs in a            and higher operating temperature.1
narrow range of wavelengths.                     1\•fonolithic focal plane arrays where
                                                 mercury cadmium telluride diodes are
   A promising technology is gallium             directly grown on silicon could also yield
arsenide-gallium aluminum arsenide, first        to larger arrays.21
proposed in 1987.18 Typical cutoff
frequencies are between 6 and 11 pm                  PhotovoJtaic indium antimonide
with detectivities D* of about 1010 to           hybrid focal plane arrays are fabricated as
IQ11 cm·~(Hz)·\·V-1 ·with proper cooling at      wen.zz For instance, a widely used
SO to 70 K (-223 to -203 "C; -370 to             commercial infrared camera of the 1990s
-334 °F). Other compositions have been           is designed around a 256 x 256 indium
reported such as indium arsenic                  antimonide array with high frame rate:
antimonide-indium antimonide and                 140 per second at 256 x 256 up to 1800 in
indium arsenide-gallium indium                   a 64 x 64 sub window. Other array
antimonide.                                      formats are also available
                                                 (320 X 256, 512 X 512, 640 X 512).
   The potential of this technology has
been evolving, especially with the                   Mercury cadmium telluride, indium
possibility of growing directly on the           antimonide, lead tin telluride and indium
silicon the detecting superlattice layers        gallium arsenide are common types of
that contain readout circuits. Indium            intrinsic detectors. Compositions such as
gallium arsenide detectors operate in the        mercury manganese telluride and mercury
0.8 to 2.6 pm band with important                zinc telluride have been developed.
applications in spectroscopy for real time
determination of chemical composition,               1v{ercury cadmium telluride and its
surveillance and fiber optic                     extension, the SPRJTE (signal processing
telecommunications (particularly at 1.3          in the element) sensor is a widely used
and 1.55 pm). One of the advantages of           detector. The SPRITE sensor was originally
indium gallium arsenide is the room              developed by Elliot at the Royal Signals
temperature operation for intrinsic              and Radar Establishment, United
detectors.                                       Kingdom. 19
Focal Plane Arrays: Intrinsic                        A SPRITE sensor is made of a strip of
Photon Detectors                                 mercury cadmium telluride mounted on a
                                                 substrate such as sapphire and is cooled at
Those detectors are in fact arrays of            cryogenic temperatures (Fig. 4). The long
photoconductive or photoelectric                 axis is in the direction of scan and the
(photovoltaic) detectors that have been          strip is biased so that the carrier drift
reviewed previously. Photoelectric               velocity matches the speed at which the
(photovoltaic) detectors are more useful         image is scanned. As a point in the image
                                                 moves along the strip, the charges it
                                                 induces move with it and the
                                                 accumulated charges are then read out at
                                                 Noncontact Sensors for Infrared and Thermal Testing 191
the end of the strip. Consequently, the       importance, but if quantitative data must
                     main advantage of the SPRITE sensor is        be extracted from the imaging array, some
                     that the signal is integrated on the focal    sort of uniformity correction has to be
                     plane by the detector itself, thus reducing   ccuried out.
                     the noise level and the timing
                     considerations. If a SPRITE sensor is used       Although this calibration process can
                     and then read out serially, the scanning      he done on chip in the case of the Z plane
                     rate js the same as ·with a single detector   technology, it is generally executed off
                     element. Hm\'ever, if several SPRI'I'E        chip. The array is exposed to a scene of
                     sensors are stacked together in a parallel    uniform temperature and an image is
                     fashion,. the scan speed is reduced because   recorded on computer memory. This
                     many rows cCin be integrated                  process is repeated for different scene
                     simultaneously.n                              temperatures. Next a calibration function
                                                                   either linear or of higher order for
                 Z Plane Technology for Focal                      nonlinear response to the photon flux is
                  Plane Arrays                                     computed pixel by pixeJ.25
                     Z plane technology has suggested ways to         For linear functions, two coefficients
                     improve infrared camera systems by            are obtained for every pixel. This is the
                     adding processing to the detection            so-called flvo-point teclmique: gain and
                     function of the array. Silicon circuits are   offset. Second order polynomials require
                     fabricated on a tiny ceramic board            three parameters and more coefficients are
                     typically 100 pm (0.004 in.) thick with a     needed for multiple points correction. In
                     detector attached on one edge. These          single-point compensation average of several
                     boards are then stacked to form complete      images recorded over a uniform
                     arrays. Among possible added processing       background ·with a defocused lens is
                     functions are convolution operations,         subtracted (in real time) from live video to
                     edge extraction and blobs dctection.24        remove nonuniformity. This· process is
                                                                   however less effective than other
                        Silicon multiplexer technology makes       techniques such as two and multiple
                     it possible for analog-to-digital converters  points techniques. 13•14 During normal
                     to be incorporated on chip in each            operation of the array these computed
                     column for higher data rates and low          coefficients serve to correct images.
                     noise.                                        Platinum silicide arrays exhibit better
                                                                   uniformity; more sensitive, intrinsic
                  Uniformity Correction for Focal                  photon detectors have Jess uniformity,
                  Plane Arrays                                     about 10 percent.
                     One problem with large arrays is the             The nonuniform response is more
                     nonuniformity of response among               easily handled in the case of a
                     detector cells caused by the fabrication      single-detector based infrared camera. fn
                     process. For qualitative applications this    this case a more complete correction
                     nonuniformity may be of little                procedure can be carried .out to correct
                                                                   vignetting and radiometric
FIGURE 4. Principle of operation of SPRITE (signal processing      discrepancies.2S,l6 Periodic recalibration is
in the element) detector.                                          needed because of system instabilities in
                                                                   time, aging, unstable bias voltages, pixel
                                 lncom·1ng radiation               non linearities and (-1 noise. For static
                                                                   scenes a quantitative measure of image
         Charge carriers            Readout region                 drift can be, for instance, the time
                                                                   evolution of the spatial variance in the
Biasing  ; - - - Drift region --~:                                 image. This could help in deciding when
current                                                            to recalibrate. 'When applicable, noise
source                                                             reduction techniques such as running
                                                                   averages contribute to reduce spatial noise
                                                                   level although periodic recaJibration is
                                                                   stili required for accurate quantitative
                                                                   measurement. Z7,28
                                                                   Summary
                                                                   The different technology characteristics of
                                                                   infrared detector arrays may be
                                                                   summarized briefly.
                                                                       Platinum silicide is the more mature
                                                                   technology- large two-dimensional
                                                                   arrays (512 x 512) are fabricated and
                                                                   complete infrared camera systems are
                                                                   commercially available. They operate in
                                                                   the 3 to 5 pm hand and need cooling to
192 Infrared and Thermal Testing
77 K (-196 oc ~ -321 °F). Cooling may
not be a problem, for a compact stirling
engine cooling _u,njt can be integrated
with the detector array.
   Thermal detectors operate at room
temperature but their detectivity is not as
high as for photonic detectors. Because
they respond to the rate of change in
scene temperature, a chopped mode of
operation or panning is needed for
viewing of static scenes.
   Superlattices and Z plane technology
are more recent and have improved, with
operating temperatures close to 77 K
(~196 °C = -321 °F) possible in the long
wavelength band. Intrinsic photonic
detectors such as hybrid indium
antimonide and mercury cadmium
telluride are now common with operation
in both atmospheric bands (3 to 5 pm
and 8 to 12 pm) and 'With respectable size
although 77 K (-196 oc ~ -321 °!') cooling
is required.
                                                                   Noncontact Sensors for Infrared and Thermal Testing 193
PART 2. Scanning Radiometric Imaging
Detectors
The difference between a scanning                               must be observed because thermal
radiometer and an· ordinary infrared                            information registered at different times is
camera is that, for a radiometer, the                           mixed together. On way to solve this
infrared signal is temperature calibrated                       problem is to split the video signal in its
thanks to the presence of internal                              basic fields and process them knmving the
temperature references seen by the                              time interval between each of them.
detector element durjng the image                               IIowever, this kind of analysis requires
formation process. This calibration signal                      careful manipulation of the signal.
permits recovery of the absolute
temperature after proper processing. In                         Cooling
such an instrument, the image is
electromechanically scanned over the                            As pointed above and shown on Fig. 2,
detector surface (single piece or SPRITE)                       superior detectivity can be achieved,
by means of the synchronous rotation of                         especially for photonic detectors, if
mirrors or prisms (Fig. 5).                                     cooling is used. Such a cooling is needed
                                                                to reduce the noise to an acceptable level
   'lb accommodate the standard video                           as seen above. There are different ways to
signal format of 30 frames per second (25                       cool the detector: liquefied gas, cryogenic
in Europe), a very high scanning rate is                        engine, gas expansion or thermoelectric
required. This imposes a wide bandwidth                         effect. Cryogenic coo1ing uses a 1iquefied
from the associated electronics for the                         gas stored in a vacuum vessel called a
noise level to be kept small. To overcome                       dewar (from James Dewar, 1842-1923,
this problem, some manufacturers use                            Scottish physicist who was the first to
slower scanning rates and have frames                           liquefy hydrogen, in 1892). Dewars are
made of several fields with one field                           constituted of two envelope ·walls ·with
update at each scan (once every four                            evacuated space maintained between
scans, for example). As a result, the                           them; moreover, to prevent heat wall
output obtained, comprising several fields,                     losses the surfaces facing the vacuum are
is not updated in real time (that is at 30
or 25 Hz). This lack of updating may
cause problems when fast thermal events
FIGURE 5. Internal view of infrared radiometer.                 Filter
                                                                selection
                                       liqu"1d n·1trogen
                                       coolant at 77 K
                                        (-196 "C = ~321 CF}
    Dewar
                                                                           Aperture control
                                                                           Internal blackbody
                                                                           temperature reference
                                                                                  Objective
Infrared detector
                                  Collimation      Horizontal   Vertical scanning prism
                                           Iem  scanning prism
194 Infrared and Thermal Testing
heat reflective (Fig. 6). Metal dewars are   -187 °C = -305 °1') at the tip of the
unbreakable, but relative porosity of metal  expansion nozzle (on which the detector
welds restrict life span unless vessels me   is fastened). As a gas, argon occurs freely
repumped regularly. Generally,               in the atmosphere to the extent of
manufacturers provide a valve for this       0.935 percent. This mechanism permits
purpose ·whereas a cryopump or a             greater autonomy than dewar operation
diffusion pump with vacuum rated in the      but is noisy and the gas tank may be
                                             cumbersome.
5 x 1o-6 torr range is recommended for
                                                For applications where refilling is not
pumping. Dewar repumping is required         practical, such as in remote areas or on
when sweating or condensed water vapor       the production line, a closed stirling cycle
is observed on the outside of the dewar      engine with cryostat can be used. This
and when rapid boiloff causes nitrogen       machine cools through repetitive
gas to escape rapidly from the fill port.29  compression and expansion cycles of gas
Glass dewars do not have this problem,       by a piston: it compresses gas at a low
but they are very fragile.                   temperature and allows it to expand at a
                                             high temperature. Because of the cycling
   In a popular configuration, the           operation, strictly speaking the cooling is
detector is directly mounted on the cold     not constant but temperature variations
surface \Vith a cold shield and an infrared  can be made small (or large) depending of
transparent window. Because some             the cycle characteristics. Although either
detectors (such as mercury cadmium           rotary or linear motors can be used, a
telluride) tend to sublimate when exposed    linear motor positioned at right angle to
to the vacuum, a protective coating such     the detector plane causes less vibration in
as zinc sulfide can be applied on the        integral stirling engines. Split cycle
sensitive surface to expand the life span.   machines are also available for remote
The most commonly used and cheapest          and low vibration operation. Typical
liquefied gas is liquid nitrogen at a        input pm\'er is around 4 VV for 150 m\,V of
temperature of 77 K (-196 oc = -321 oF).     cooling for a small engine (0.5 kg)
Some 70 percent of the Earth's               whereas a large engine (2 kg) ·wm deliver
atmosphere is nitrogen. Liquid hydrogen      1 VV of cooling for 40 W of input power.
                                             lvfany manufacturers offer infrared
(20 K =-253 oc =-424 oF) and liquid          cameras with stirling cycle engines.
helium (4.2 K =-269 oc =-452 oF) are
                                                Another mode of cooling infrared
more exotic because of their price and       detectors is using thermoelectric elements
because a typical 1.0!. (1.0 dm3 =           based on the peltier effect. This
0.26 gal) dewar will keep liquid gas for 3   phenomenon was discovered in 1834 by
to 4 h, thus requiring a regular refilling.  ].C.A. Peltier: at the junction of two
                                             dissimilar metals carrying a current,
   Joule-thompson gas expansion is           temperature rises or falls depending upon
another way to cool detectors. In this case  the current direction. Vigure 7 shows that
the quick expansion of high pressure gas     peltier effect is used for cooling,
(such as nitrogen or argon) produces, after  thermoelectric effect is used for
a few minutes of operation, droplets of      temperature measurement with
liquid nitrogen or liquid argon (86 K=       thermocouple and thompson effect is
                                             used for power generation. These three
FIGURE 6. Schematic diagram of dewar with
windowed aperture at angle 8.
                                             FIGURE 7. Three processes of direct conversion of heat into
                                             electricity or of electricity into heat.
                                                     A                             Ampere meter
                                                                                    (thermocouple,
                                             r,                                     thermoelectric effect)
                                                    A                     /o'
                                                         B                 • - Battery (power generation,
                                                                                    thompson effect)
                                                                          ~0>
                                                                                    Generator (cooling, pe!tier
                                                                                   effect)
Evacuated                                    legend
5pace
                                               A,B "" dissimilar metal!>
                                                rh == high temperature
                                                 11 "" low temperature
                                             Noncontact Sensors for Infrared and Thermal Testing 195
phenomena are in fact three applications       important criteria for band selection are
of the same physical phenomenon of             operating distance, indoor/outdoor
direct conversion of heat into electrical      operation, temperature and emissivity of
t'tH.'1gy, or the reverse. Because of the low  the bodies of interest. As Planck's law
efficiency of the conversion process           stipulates high temperature bodies emit
peltier elements draw high current and         more in the short wavelengths, so long
are generally stacked upon each other to       wavelengths will be of more interest to
achieve sufficient heat removal and            observe near room temperature objects.
temperature gradient (Fig. 8). Peltier         Emitted radiation from ordinary objects at
elements are unattractive, however, for        ambient temperature (300 K) peaks in this
temperatures below 200 K                       long wavelength range. Long wavelengths
                                               are also preferred for outdoor operation
(-73 oc ~ -100 °!').                           where signals are less affected by solar
                                               radiation. For operating distances
   Most infrared camera manufacturers          restricted to a few meters in absence of
offer their products with an optional          fog or water droplets, the atmosphere
choice among those various means of            absorption has little effect.
cooling. For laboratory operation,
nitrogen cooling with metal dewar is              Spectral emissivity is also very
perhaps the best choice because of             important because it conditions the
reliability, quiet operation and the low       emitted radiation. I'igure 9 shows spectral
                                               emissivity cun•es for common materials.
temperature 77 K H 96 oc = -321 °!')           Also plotted on these curves are the more
                                               useful infrared bands of interest. Polisl1ed
achieved. For remote operations                metals with emissivity smaller than 0.2
thermoelectric cooling is preferred            can not be observed directiy1 for they
because it does not need any refilling and     reflect more than they emit. A high
its lack of moving parts makes it reliable.    emissivity coating (such as black paint) or
For the production environment, good           a reflective cavity must be used.31 <B
choices are the stirling engine cooling,
joule-thompson gas expansion cooling or           Although no specific rule can be
thermoelectrical cooling.                      formulated 1 generally the most u·seful
                                               bands are 3 to 5 pm and 8 to 12 pm
Selection of Atmospheric                       because they match the atmospheric
                                               transmission bands. Most of the infrared
Band                                           commercial products fall in these
                                               categories •whereas the near infrared (0.8
Because the atmosphere has not perfectly       to 1.1 pm) part of the spectrum is easily
flat transmission properties (Fig. 2), the     covered by standard ambient operation
selection of the operating wavelength          temperature silicon detectors.
band will be conditioned by the final
application. For the majority of                  Another important point to consider is
nondestructive testing applications, the       the detectivity D* of the detector used.
useful portion of the infrared spectrum        From Hg. 2, for instance it is seen that a
lies in tile 0.8 to 20 pm range; beyond        77 K (-196 oc ~ -3Z1 ol') cooled indium
20 pm, applications are more exotic such
as high performance fourier transform          antimonide detector operating in the 3 to
spectrometers operating near 25 pm.3o          5 pm range has a seven fold higher
The choice of an operating wavelength
band dictates the selection of the detector    detectivity than a 77 K (-196 oc ~
type as Fig. 2 shows. Among the
                                               -321 °F) cooled mercury cadmium
FIGURE 8. Multiple stage thermoelectric        telluride detector operating in the 8 to
calling unit using peltier effect.             12 pm range. That means that even if, for
                                               a specific application, the emitted
                       Absorbed heat           radiation (temperature of interest or
                                               spectral emissivity) is higher in the 8 to
Current                                        12 pm range, the contrast obtained may
                                               be stronger in the 3 to 5 pm range
         Rejected heat                         because of the superior D* of an indium
                                               antimonide detector.
                                                   As a final notice we may point that
                                               dct;!iled studies34·3f' have concluded that
                                               for temperature in the 263 to 403 K
                                               (-1 0 °C to +130 oc; 14 to 266 °F) interval,
                                               measurements can be done without much
                                               difference in both bands (3 to 5 pm and 8
                                               to 12 pm). For some special applications
                                               such as military, bispectral cameras
                                               operating simultaneously in both bands
                                               have been developed to characterize more
                                               accurately target thermal signatures.
                                                   'Jb summarize, there are two main
                                               categories of detectors: thermal and
196 Infrared and Thermal Testing
photonic. In thermal detectors the signal               values r into thermal values G (gray level).
is proportional to the absorbed energy
whereas in photonic or quantum                          In recent infrared cameras, pixel coding is
detectors the response is a funrtion of the             performed on 12 or even 14 bits yielding
number of absorbed photons. Figure 2                    respectively to 4096 (~ 212) or 16384
shows different detector response curves                (== 214) possible values. Thermograms from
as a function of wavelength.                            such systems do not require any further
                                                        conversion because the available span of
Radiometric Temperature                                 values covers directly the whole dynamic
Measurement                                             range of the infrared cameras. Older
                                                        systems digitizing infrared images on say
Different techniques can be used for                    8 bits provide a limited 256 (== 28) possible
temperature measurement. Two of them                    values and require a particular conversion.
are considered here: single-color and                   In these cases, because the available span
bicolor.                                                of values does not cover the whole
                                                        dynamic range of the infrared camera,
   Before processing any thermal images,                manufacturers introduce two settings, a
it is necessary to convert the raw image                level and a range. These settings make it
                                                        possible to cover the whole dynamic span
FiGURE 9. Spectral emissivity curves of various materials:34 (a) crown glass; (b) red tile;
(c) foliage; (d) water; (e) concrete; (f) road asphalt; (g) black rubber; (h) metals. Unit
conversion: 1.0 f-Jffi == 4 x 1Q-5 in.
1.0(a)                                                  (e)
0.5.w£-~"
                                                             1 0 1 · · ·;.         :-  :::L:.t,            .   ..' .;;:''.·.~
 ·~ ~                                                                  ·· ;        :
                                                                                       ~.. :. -~           ~
00.5·~~                                                                            -
                                                                                                           .
t~                                                                                     ·•·.+.·I-...:{...,: . :, ., ::i--
                                                             05 •      :
                                                                       : ;. :::j:.t : ':;: :, .
                                                                       : .. - ""i""i' : .. ' ' .~
                                                             0
                                                                  0.5              2 3 4 5 6 8 10 12
                           wavelength ), (11m)                         wavelength }, (i.Jm)
(b)
                                                        (I)
1 . 0 1 . :. .'.:-;·;.-::                       :
            0  -     T ":"  :·                     '00
                  + '' i•
                                                l ''
0 5 . -~ :. ...}.~.:tt .;·--::.::;~.-...
                         ' •'I"~ :· ,., " "
 0.5-~:;:::
0
                           2 3 4 5 6 8 10 12
            wavelength A (!Jm)                                         wavelength ), (!Jm)
                     2 3 4 5 6 8 10 12
(c) 1.0                                                 (g)
0.5pwG-"
                                                             1 0 1.. .....o5'.  '  1   ·.-·:Ti~-::-..';:!  .:  ....
··-~ 0~                                                           .
                                                                       .I                                  ''  _:'::.!;; :...,
 .\:2·;:;
                                                                       ,                                   _.
00.5E."!
                                                                       ' .,                                    '''
t~
                                                              0.5 : : :l.:-~ - ~ ::: ::--
                                                             0
                                                                                         2 3 4 5 6 8 10 12
1.0(d)      wavelength ), (j.Jm)                        1.0(h)         wavelength A (j.Jm)
0.5w-"                                                  0.5w-"
                     2 3 4 5 6 8 10 12                                                           .: ..:.:.:.:.:;.:
 .£~        wavelength ), (tJm)                           .»~ ~~
                                                                          10 12..., ' ' ''
 -~ ~                                                    -~ ~
                                                                                2 3 45 6 8
    0·-                                                 0·~~           wavelength ), (pm)
00.5w·E!~-                                               t~
                                                        Noncontact Sensors for Infrared and Thermal Testing 197
but have to be taken into account to                  Now considering a sequence of
compute the thermal values:                        thermograms taken at different
                                                   temperatures, it is noticed that this
(6) G  r    --7205C61C2:7:-       Range  +  Level  difference is a linear function of the
                                                   temperature in gray level:
       '--
                                                   (8) di,j (c!rer,rref) a;,j G.~ref,pef
If no corrections are needed, as for
                                                                            + b;,j
instance in 12-bit or 14-bit systems,
then G = r.                                           In the visible spectrum, a possible
                                                   hard\vare solution to this vignetting
Correction of Vignetting Effect in                 problem is to add an additional lens in
                                                   front of the objective.39 If the original
Single-Color Focal Plane Array                     optics of the camera introduces a
                                                   distortion P then a lens with a distortion
The next step before quantitative analysis         function F-1 corrects the response of the
of thennograms is to convert the image             global system. Of course such an
sequence into temperature images. In the           approach would attenuate the signaL ·rhis
case of focal plane arrays, the image              approach is possible if the function P does
restoration is generally limited to the            not depend on the features of the scene
vignetting effect (if present) because the         such as temperature due to self-emission
noise level is generally low.                      of the optical elements.40 Because in
                                                   infrared thermography F depends on the
   Vignetting is explained as follows.:{? lf       temperature, a software approach is
                                                   preferred. The idea is to create a
a cone of rays is formed from a point in           (M x N x 2) matrix file (where A,/ x N is the
the object space and limited by the                image format) containing the coefficients
diaphragm of the lens, and if this cone is         ai,i and hi,; (for every location (i,j) in the
intercepted with the image plane                   image:
perpendicular to the lens axis, the
intercept is a circle if the object lies on the    (9)
optical axis and more generally an ellipse
if the object is laterally displaced.              wllere Gr~1rr is the gray level at the
Moreover, for many lenses, the front and           reference point location corresponding to
rear apertures are too small to fully              the actual ambient temperature (at the
transmit oblique rays and a part of the            time the correction is computed) and
light cone may be cut off, causing an              Gcc;;\;r is the temperature (in gray level) of
amplitude reduction at the edges of the            the room when the correction matrix was
image. J~inally, this effect is also caused by     created.
antireflection coatings of camera optics
optimized for normal incidence, thus               Temperature Calibration
explaining reduced distortiOns for central
pixels.                                            After assessment of vignetting, the next
                                                   step consists of converting gray level
   Vignetting is more severe if expansion          values into temperature. The common
rings are used to restrict the field of view       procedure is as follow. A blackbody is set
because of the limited effective aperture          at a given temperature, 283, 298, ... K (10,
obtained in this case.2s
                                                   25, ... oc; so, 77, ... 0 1") and positioned in
   As predicted by theory, 38 experiments
carried out with the focal plane array             front of the camera. For each blackbody
camera show this effect depends on both            temperature, an image is recorded and
pixel location and temperature difference          readings arc obtained in a restricted area
between the target and the ambient.                at the center of the image where
Below ambient temperature, 31 S K                  radiometric distortion effects are less
(42 "C = 107 °F), vignetting has behavior          important. Values in a central subwindow
opposite to that above ambient                     of say 10 x 10 pixels are averaged together
temperature: the curvature direction               and plotted as function of blackbody
changes and at ambient temperature                 temperatures. A polynomial fitted to these
vignetting is not visible.                         values provides the calibration curve
                                                   (Fig. 10). For instance, in the case of a
    Equation 7 expresses the difference            focal plane array camera, the following
between the signal at the central reference        relationship is obtained ·where G
point corresponding to the center of the           represents gray level values (linear best fits
brightness area and three points placed at         using a third order polynomial function):
different distances from it:
where Gf,; is the gray level of pixel (i,j) at
temperature t and G~rcf,)ref is the gray level
of the reference at temperature t.
198 Infrared and Thermal Testing
(10) T  -13.4 + o.os sG                                  that also uses emittance, emissivity is used
                                                                now.
               1.6 x w-' G2
                                                                   The main sourc~ of UQf~rtainty in
               + 2.2 x w-9 G 3                                  radiometric temperature measurement is
                                                                the unknown emissivity. The problem is
          Obviously, such a calibration procedure               worse because of emissivity variations
       is valid only for a specific experimental                with ·wavelength ).. and temperature T. It
       setup. If the experimental conditions                    is, however, possible to assume a simple
       change, it is necessary to repeat the                    relationship between emissivity and
       process.                                                 wavelength to calculate the temperature
                                                                from measurements at different
          If instead of the third order polynomial              wave1engths. 41 -45 Pyrometers based on
       of Eq. 10, a line fit is used, calibration is            that principle are called multiwavelength
       considered a two-step process. To speed                  pyrometers. The signal measured in
       up calibration, conversion values might                  channel i of such a pyrometer is given by:
       he precomputed and saved in a lookup
       table for quick access: input of a gray                  where K; is a constant for this channel
       value G directly provides the                            and C2 is the second radiation constant.
       corresponding temperature T. If a                        Equation 11 is known as Planck's law
       hardware lookup table is available, the                  under \1\,!ien's approximation.34
       processing time is very fast. Digital frame
       grabbers often include such a                               One simple assumption about the
                                                                variation of the emissivity and
       functionality.                                           wavelength is that a smooth curve exists
                                                                between these two variables over the
       Two-Color Pyrometry for                                  wavelength range of interest.41 •42 This
       Temperature Evaluation                                   assumption holds for graybodies (for which
                                                                emissivity is constant ·with wavelength)
       The spectral surface emittance radiated by               and to some extent to colored bodies (for
       tm incandescent graybody depends only                    ·which emissivity varies with wavelength).
       on its temperature 1~ its emissivity E and
       the spectral bandpass of the observation.                    For bicolor pyrometers, an easy way to
       The term is properly named the spectral                  compute the temperature is to form the
       emittance referring to the property of a                 ratio R of the signals, because for a given
       particular surface, rather than spectral                 set of wavelengths and temperature T the
       emissivity, the intrinsic property of an                 spectral emittance ratio Iri2- 1 is unique:
       uncontaminated, optically smooth
       surface. However, to avoid the possibility
       of confusion with the radiant energy flux
FIGURE 10. Infrared camera calibration curve and level and      (12) R
range settings for temperature computations.
Calibration curve without radiometric
         distortion for a given pixel (i,J)
                                                                which simplifies to:
                                             Pixel of interest  (13)
level                                                              K 1 regroups all the constant terms:
                  Blackbody temperature T (relative scale)      (14) "Jj ~ P(R)
legend                                                             A calibration curve P(U) that relates the
   G "" thermal value (arbitrary unit)                          measured ratio R to the calculated
                                                                temperature T 1 can be experimentally
  i,f = coordinates that define pixel                           obtained. Although Planck's law is the
                                                                underlying physical basis, it docs not
    r =- raw image value                                        appear explicitly in Eq. 14.
   T = temperature
                                                                Noncontact Sensors for Infrared and Thermal Testing 199
The error on the calculated
temperature 7'1 is given by the following
fonnula: 4S
;i)~(15) c2( -
   Zero error is obtained with the
condition corresponding to a ratio of one
in Eq. 12. Equation 15 assumes no
measurement errors in either channel. If
any of such errors are present (random
errors from detector and photon noise,
detector nonlinearity, drift in channel
calibration, error in nominal channel
wavelengths), the equation becomes:44
(16)  C2  t>.T
          Tz
   For instance, a 1 percent error in one
channel leads to an error in the
temperature of a!Jout ±15 K (±15 "C =
±27 "F) at 1273 K (1000 "C = 1832 "F) for
the \\'avelengths selected.
200 Infrared and Thermal Testing
PART 3. Schemes for line Scanning
In thermal nondestructive testing the          constants arc combined into a single
surface of an object is usually heated with    parameter called thermal diffusivity a:
a periodic or pulsed heat source
generating time dependent heat flow            (18) "  k
inside the object. The inner structure and             pc
possible anomalies of the object affect the
heat flow. Information about the effects          In the case of a scanned line source,
can be obtained by monitoring the              the excitation is directed on the surface of
surface temperature of the object in time.
                                               the solid and as such the case does not
   In line scanning techniques the time        represent volume heating. Therefore, it is
dependent heating is obtained by moving        more convenient to put q = 0 and to give
a line shaped source across the object         the excitation as a boundary condition to
surface or by translating the object itself
in relation to a stationary Jine source.       Eq. 17. For example, if a semiinfinite
Thus each surface point is subjected to a
varying amount of heat in time. Because        solid, whose surface is the z = 0 plane, is
of heat diffusion in the object, the
temperature of a particular surface point      heated with a moving laser beam, the
reaches its maximum after the source has       heat flow in the direction normal to the
passed the point. In this sense, the           surface is caused by a scanned line source:
moving Hne source is followed by a
thermal wake. The behavior of the wake         I(19) k iJT(r,t)
depends on the object material and the
possible anomalies in the object.                            ()z z=O
   As the surface area of the object is                               +
heated line by line, the monitoring of the
surface temperature is usually done the        where a is the 1·rl radius of the gaussian
same way. The detection line is located a      line source in the X direction and bin the
distance behind the heat source to allow       Y direction. The source moves to the
time for the heat diffusion. The correct       positive Y direction ·with a velocity\' and
distance has considerable importance in        has an amplitude of Qo. In Eq. 19. it is
subsurface discontinuity detection.            assumed that the surface absorbs the
                                               excitation completely.
   The monitoring is performed in a
noncontact way by using infrared photon           Equation 17 can now be solved with
detectors with suitable optics. \-\'ith        standard Green's function techniques:46,47
postprocessing the monitored lines are
composed into a two-dimensional surface                                        t
temperature map, the usual form of                                       Q~~/Z Jdt0
information used for evaluating the            (20) T(.t,)•,z,t)
characteristics of the object.
                                                                         pc1r  --e-o
Scanned Line Excitation                                           x exp[ z -2x2
Time dependent heat transfer phenomena                                     a + 8o:(t- to)
in solids are described by the heat                                      -Z(y- vt )2
diffusion equation:
                                                                  ' b2+Ba(t- to)
      iJT(r,t)
(17)  pc---                                                       + 4u(tz~ t )]
                                                                                        0
            ilt
                                                                  7 [ v~s-,-(t---~o-)
where cis specific heat U·kg-1-K-1), k is
thermal conductivity (VV-m-I.kl), q is                            x Jb2+8a(t-t0)
heat input per unit volume (\-\1·111-:{) at a
                                                                  x ~4a(t -t0 )]
given time (second) and point F in the
solid, f is position, Tis temperature
(kelvin) and pis mass density (kg·m-3).
Usually, the last three material dependent
                                               Noncontact Sensors for Infrared and Thermal Testing 201
Equation 3 cannot be solved                                     models. Already in a two-layer case the
analytically but can be integrated                                  analysis is quite complex, 48 although
numerically. By putting a== 15 mm,                                  analytical expressions can be obtained
b ~ 0.3 mm, p ~ 1400 kg·nr3, c ~ 935                                even for general multilayer structures.-t9,~0
}kg-1-K-1 and K ~ 0.87 W·m-1-K- 1 and by                            However, the introduction of true
                                                                    three-dimensional object geometry or
plotting the isotherms at the Z = 0 plane                           discontinuities ln the object renders
(Fig. 11) it is revealed that the surface                           analytical solutions in most cases
temperature profiles are distorted in the)'                         impossible. Therefore, these kinds of
direction as the result of the movement of                          models have to be solved numerically,
the line source. As a consequence of the                            which can be accomplished witll a variety
asymmetry of the isotherms in the                                   of techniques.zs,SI-53
y direction, a net heat flow can be
expected in this direction.                                            The finite difference technique, for
                                                                    example, has been successfully applied to
    r:igure ] 2 shows surface temperature                           several line scan problems by
profiles computed with tbe same                                     Hartikainen, 54 Lehtiniemi55 and Varis.56 In
parameters at various scanning velocities.                          this technique, the object is described
The nonsymmetrical behavior due to the                              with a discrete three-dimensional grid.
motion of the source is evident here also.                          The diffusion values in Eq. 17 with
As the line source moves across the object                          suitable boundcuy conditions are replaced
sltrface, every surface point in turn                               \Vith their discrete equivalents. The
experiences a heating pulse, whose                                  resulting large set of equations is usually
duration tis the source width b divided by                          solved both in the case of the object's
the scanning velocity 1'. Therefore, the                            having a discontinuity and the object's
higher the scanning velocity, the less time                         not having one. To determine the effect
there is to deposit heat into the object. As                        caused by the discontinuity, the surface
a result, the peak surface temperature                              temperature profiles are plotted and
drops as the scanning velocity is                                   compared as shown in Fig. 13. The
increased. Because of heat diffusion, lt                            materials parameters are the same as used
takes a certain amount of time for the                              for plotting Figs. 11 and 12. Because of
surface temperature to reach the peak                               the diffusion again, it takes a certain
value, during which time the source has                             amount of time for the heat pulse to
moved a distance vl. Because of this, the                           reach the discontinuity and reflect back to
maxima of the temperature profiles occur                            the object surface. For this reason, the
behind the line source.                                             surface temperature profiles are practically
                                                                    identical on the leading edge; the
    For practical purposes, the simple                              differences emerge on the trailing edge.
semiinfinite object is seldom adequate.
Many advanced materials have                                            The surface temperature difference
complicated layered structures that must                            between the object with the discontinuity
be taken into account by theoretical                                and the Object without one can be
                                                                    determined by simply subtracting the
FIGURE 11. Isotherms on surface of solid heated with moving         FIGURE 12. Surface temperature profiles at various scanning
gaussian line source.                                               velocities generated by moving gaussian line source.
       +1.0 (+0.04) ~~ -~1 ~-· ~·----.------~,~---------r'-~~~
     l0                                                             1.25
      -1.0 (-0.04)                                                        1.00
0vc
E                                                                   ·3c"
E -2.0 (-0.08)                                                      c~ 0.75
                                                                    g
.!::2~
 X                                                                  :e 0.50
 ~                                                                  ~
                                                                    h
>- -3.0 (-0.12)
                                                                          0.25
      -4.0(-0.16)
                                               1                    0 CL----~~-L~~j_~~~~~od
      -5.0 (--0.20)                            1
                     -20   -~•~~.~ . ~ ~ ~-~J                        -5.0 --4.0 -3.0 -2.0 -1.0                               0   1.0
                    -0.8)                                           (-0.20) (-0.16) (-0.12) (-0.08) (-0.04)                     (0.04)
                                                                                Distance from heat source center, mrn (in.)
                           -10 0 +10 +20                            Legend
                           (-0.4)                    (0.4)  (+0.8)      T =- temperature
                                                                      vl-= scanning velocity of 6 mrn-s-1 (14.2 in.·rnin-1)
                                   X axis, mm (in.)                   v2 0; scanning velocity of 8 mm·s-1 (18.9 in.·min-l)
                                                                      v3 = scanning velocity of 10 mm-~-1 (23.6 in.·min-1)
202 Infrared and Thermal Testing
curves from each other. Figure 13b shows              maximum gives an estimate of the
                 the surface temperature difference caused             detectability of the discontinuity. If the
                 by the discontinuity obtained from                    surface temperature difference caused by
                 Fig. 13a and similar curves computed ·with            the discontinuity is smaller than the
                 different line source velocities. As can be           temperature difference that can be
                 seen, the temperature difference maxima               resolved with the detecting system, there
                 and their locations depend on the                     is obviously little hope of success. The
                 scanning velocities. Naturally, they                  location of the maximum is the optimum
                 depend on the depth of the discontinuity              point for detection and therefore
                 as welJ. 57                                           determines how far away from the
                                                                       excitation the detection point should be
                    Both the magnitudes and locations of               placed. Unfortunately in practice, there is
                 the maxima have great practical                       seldom prior knowledge about the depth
                 importance. The magnitude of a                        of the discontinuity, which makes the
                                                                       determination of the optimum point
FIGURE 13. Comparison of objects with and without                      merely an approximate technique in real
discontinuity: (a) numerically computed surface temperature            experiments.
increases for object having defect (solid line) and for object
without defect (dashed line) generated by moving gaussian              Line Heating Methods
line source at 10 mm-s-1 (23.6 in.·min-1); (b) surface
temperature differences between object without                         A typical infrared line scanning setup is
discontinuity and object with discontinuity at various                 shown in Fig. 14, ·where a heating line
scanning velocities.                                                   and a line scanner is focused on the
                                                                       surface of a moving object. By combining
(a)                                                                    the horizontal translation of the object
                                                                       and the infrared detection alongside a
     18 ,---,~--,--·-,-                                                vertical line, a two-dimensional surface
                                                                       temperature map (an infrared image) can
     · - -16 - · - f - - ··- f---·+~--+~.                              be constructed.
     14-·                                             ·--                 The detection line has to he some
                                                                       distance away from the heating line to
     12-·                                             --               allow for heat diffusion in the object as
                                                                       discussed previously. Otherwise, the
g 10 . -         I··--\--- -+-~--+-11_-11-----1                        heating and the monitoring of the object
                                                                       surface happen simultaneously.
~ 8 --           Discontinuity---+·---+/-"Cf-~1\--·-
     : "-, -==~r---                                                       The line detection can be obtained
                          .-~--t"---+1                                 with a single-element infrared detector, an
                                                                       infrared lens and a suitable scanning
      2                        "-No discontinuity"- \-~-               optical element like a deflection mirror
                                                                       (Fig. 14a), a rotating polygon mirror or a
      0                   -~--L--~-- ~..                               rotating prism. Also, it is possible to
      -5.0                                                             forego the scanning optical elements
     (-0.20}      -4.0    -3.0 -2.0 -1.0 0 1.0                         completely by using modern
                 (-0.16}                                               one-dimensional focal plane array
                          (-0.12) (-0.08) (-0.04)              (0.04)  detectors (Fig. 14b).
                 Distance from heat source center, mm (in.)               There are various ways to generate line
                                                                       heating: (1) lasers, (2) hot air jets and
(b)                                                                    (3) induction currents. Basically, any
                                                                       source that can excite heat in the sample
     0.25                                                              and be formed into a remotely line
                                                                       shaped form is applicable.
     0.20
                                                                       Heating by lasers
     0.15
                                                                       Perhaps, the most often used heating
g                                                                      source is a laser beam. The laser beam can
                                                                       be formed to the line shape by first
h    0.10                                                              expanding it and then focusing it with a
<I                                                                     cylindrical lens (Fig. 1Sa).58 Another
                                                                       variation is to use a focussed laser spot
     0.05                                                              and to move it rapidly with a deflection
                                                                       mirror (Fig. 1Sb).59 \o\'ith two mirrors this
     0            --4.0 -3.0 -2.0          -1.0    0            LO     technique has also been used for
         -5.0    (-0.16) (-0.12} (-0.08)  (-0.04)                      generating a two-dimensional raster
                                                               (0.04)  SCaiL 61 l-r,z The size of the heated area is
        (-0.20)                                                        easily controlled with optics and a highly
                                                                       localized source can be generated.
                   Distance from heat source center, mm (in.)
legend
   T = temperature
  vl =velocity of 6 mm·s 1(14.2 ln.·min·l)
  v2 =velocity of 8 mm·s 1 (18.9 in.·min-1)
  v3 =velocity of 10 mrn·s-1 (23.6 in.·min-1)
                                                                       Noncontact Sensors for Infrared and Thermal Testing 203
The power of the source can be                         semiconductor lasers are available. The
                   controlled fairly accurately, too. Possible               laser beam can be transferred via an
                   heating lasers are, for example, argon ion                optical fiber, 63 if the wavelength of the
                   lasers,:;,!'\ neodymium-yttrium aluminum                  light is in the visible or near infrared
                   garnet Jasers63 and carbon dioxide lasers.64              region. This makes it possible to place the
                   Argon lasers yield output power in the                    often fragiJe laser device farther from the
                   order of few watts, whereas both the                      test area, which plays an important role in
                   neodymium-yttrium aluminum garnet                         the development of a transportable
                   and carbon dioxide lasers can provide                     testing systems.6s
                   output power in excess of 20 \~'if
                   necessary. Even high power                                   Disadvantages of laser heating are the
                                                                             price of high power lasers, the fragility of
                 '.··                                                        the lasers and the ·water cooling
                                                                             requirements of the lasers. Because of the
fiGURE 14. Operational principle of infrared line scanning                   optical fiber the fragility and the cooling
measurement system: (a) single-element detector with                         requirements do not pose a problem. The
scanning optics; (b) multiple-element line detector.                         length of the fiber can be several meters
                                                                             without any considerable loss of output
(a)                                                                          power. Therefore, the laser itself can be
                       Germanium tens
                                                    Infrared detector
Deflection                                                                   fiGURE 15. Arrangements: (a) line focused laser heating;
    mirror                                                                   (b) flying spot laser heating; (c) infrared lamp heating;
                                                                             (d) hot air jet heating with fish tail nozzle; (e) radio
   (                                                                         frequency induction heating.
                                           Detection tine                    (a)                                                  (c) Lamp
                     Object                                Heating                     Beam              r-,
                                                           line                     !'Xpander
(b)
                                                                Object              ~
 Focal plane                                                    translation                          {\
         array
                                                                             K-I                              laser               Reflector
      infrared                                                                                                beam
     detector                                                                -I
                                                                                                                ~                                          Object
                                                                                                         Cylindrical
                                                                                                             lens
                                                                                                                          Object
                                                                             (b) (d)
                                                                             Def lection                                          t==~H~o=.,je:t r~r
                                                                                mir~~ las~
                                                           Heating line      lens                        -----------                               ~
                                                                                                                                                        Nozzle
                                                                                                                          ObjeCt                                Object
                                                                                                               (e)
                                                                                                                                     Induction
                                                                                                                                             coil
Detection tine
        Object                                                                                                                                     Object
204 Infrared and Thermal Testing
placed near a water source and in a place        Otherwise, the coil is mechanically very
of safety. An alternative technique for          rugged, which makes it a good choice for
generating heat with light is to use a high      industrial applications. Furthermore, the
power infrared lamp with a reflector             necessary equipment is relatively
(Fig. 1Sc).66 For example, quartz lamps          inexpensive.
can have radiative power exceeding
1000 W. The lamps are typically 200 to           Imaging Methods
300 mm (8 to 12 in.) long and thus are
capable of heating much larger objects           In the line scan schemes the infrared
compared to laser heating situations.            images are formed by combining in the
Naturally, the generated heat source is not      computer the object translation and the
as localized as in the case of a laser beam.     image line scanning perpendicular to the
                                                 translation in the computer (Fig. 14).
Heating by Hot Air jets                          Usually, this is achieved by placing the
                                                 object in a translation stage (Fig. 16a).5t>
Another excitation technique that can be         Alternatively, the object can be kept still
used is hot air jet heating (Fig. 1Sd).s6,67.69  and the scanner moved (Fig. 16b),65
Bringing a narrow fisll tail nozzle near the     although this configuration is rare. In
surface of the sample directing the hot air      both these cases, the sample )las a planar
flow through it can generate an                  geometry. However, other possibilities
approximately line shaped heat source on         exist as well. The sample can have a ring
the sample surface. Unfortunately, the hot       shaped geometry (Fig. 16c), in which case
air jet generates a wide source, which does      the ring is rotated around its axis and the
not provide a good spatial resolution.           heating and the detection line is arranged
However, there is a lot of heating power         alongside the radius of the ring. 55 Also
available with the hot air jet heating,          possible are cylindrical shapes like tubes
which can be used for looking for                and shafts (l;ig. 16d), which can he
discontinuities that have large dimensions       rotated around their longitudinal axis. 56
and are located relatively deep.56 This
technique is also suited for materials with      FIGURE 16. Imaging techniques for (a) moving planar object;
low diffusivities. 69 In addition to the good    (b) stationary planar object; (c) ring shaped object;
pmver reserve (0.1 to 10 kW), hot air guns       (d) cylindrical object.
are much less expensive than lasers. An
interesting variation of the technique is to     (a) (c)
use cold air with already hot objects.
Plasma jets instead of air jets are also         Sample translation                          Ring rotation
possible.67
                                                   Df'tector  Lens   'l\ O~f!ection
Heating by Induction Currents
                                                 (b)                 )l mirror
Radio frequency induction is a heating
technique that can be used for heating                                                  (d)
electrically conducting materials
conveniently. Heat is excited by resistive       Scanner
losses of the eddy currents induced in the       translation
material (comprehensive treatments have
been published 70,71), although it is also
possible to make a conductive filament
radiate enough heat.72
    In thermal nondestructive testing,
induction heating can be used for
generating harmonic source73 as well as a
line source. 74 The source is generated with
an induction coil that is driven with an
amplified radio frequency signal
(Fig. !Se). The coil has to be matched to
the object material and to the cable
carrying the signal with an impedance
matching circuit. The resonance
frequency of the matching circuit depends
on the size of the coil and the material of
the object. Typically, the frequency is in
the MHz region. Amp1ifier powers range
from few hundreds of watt to few tens of
kilowatt.
    Downsides of induction heating are the
large source size and the incapability of
heating nonconductive materials.
                                                 Noncontact Sensors for Infrared and Thermal Testing 205
In this case, the heating and the detection    of a problem. For most cases, the
are placed alongside the longitudinal axis.    difficulties with surface reflection can be
The rotation can be achieved, for              removed by using hot air jet heating or
example, with direct current motors and        induction heating. The emissivity
can be controlled ·with the computer by        problem cannot be solved with a proper
using optical encoder disks. In principle,     choice of heat source. The effect of
other slightly curved objects could be         emissivity variations can be eliminated
imaged as well but the control of the          with a combination of controlled
translation system lJecomes much more          temperature measurements and image
involved.                                      post processing,80 but the technique is
                                               rather involved to be applied for line scan
    The infrared image is formed in the        schemes.
computer. Usually, the computer controls
the translation of the object in such a way       One of the advantages of the modern
that a preset number of line scans is          infrared testing method is that it produces
performed on the object. The number of         images, where the locations of
the line scans and the ri1agnification of      discontinuities are readily recognizable by
the optics define the surface area that can    comparing to the object geometry.
be imaged. Each line scan consists of a        Usually, the discontinuities are easy to
preset number of pixels, in which the          recognize without any special training of
signal of the infrared detector is sampled.    the operator. Hmvever, sometimes it is
The signal is amplified and filtered before    necessary to process the image further and
the sampling. If a deflection mirror or        the computer program controlling the
rotating polygon mirror is used, the           imaging system should be able to. Normal
computer controls the mirror rotation so       operations include correction for
that the image point at the sample surface     heterogeneous heating profile, noise
moves correctly.                               elimination by median filtering, contrast
                                               enhancement to correct for dynamic
    Most often, the thermal image is           range problems and edge tracing for shape
formed after one heating round. llowever       recognition. Beyond simple
in the case of low diffusivity materials, it   postprocessing are problems in
is possible that good enough contrast          determining the sizes and depths of
cannot be obtained with one frame. This        discontinuities or the severity of
is especially true for deep discontinuities,   discontinuities. In these cases, rather
In situations like these, it is possible to    complicated and specialized algorithms
use several heating rounds to enhance the      are needed.
contrast as long as proper care is taken to
avoid damaging the object.69 To improve        Applications
signal-to-noise ratio, the consecutive
frames are averaged and embedded into a        Detection of Adhesion
single image. Another possibility is to        Discontinuities in Ceramic Coated
average pixels during the sampling.            Steel Rings
   The pixel size on the surface of the        Thermal nondestructive testing methods
object is defined by the magnification of      have proven to be beneficial in several
the optics. In principle, the smallest detail  applications where traditional methods
possible to resolve is the size of the         like radiographic testing, electromagnetic
detector multiplied by the magnification.      testing and ultrasonic testing have been
However in practice, various experimental      problematic. The applications in question
factors limit this. The spatial resolution in  usually relate to new materials or
thermal imaging systems is complicated         advanced materials. These include
and no analytical theory in the 1900s has      ceramics, composite materials, plastics,
described it. Experimental studies show        semiconductors etc.
that in addition to the size of the detected
area, the spatial resolution is affected by        A typical example is plasma sprayed
the size of the heated area and the            coatings on steel substrates like the ones
diffusion in the sample.75 The                 used on hydrostatic seal rings in a
discontinuity size and geometry affect the     circulatory water pump in a nuclear
thermal image as well. 76 Several authors      power plant. ss,sH The ring material is an
have also discussed the problem of             austenitic stainless steel, American Iron
defining the point spread function of          and Steel Institute (AISI) 316 (18 percent
thermal imaging to reconstruct the size,       chromium, I0 percent nickel, :~ percent
the shape and the depth of the                 molylJdenum). The actual seal consists of
discontinuity accurately. 77-79                two such rings that rub against each
                                               other. To prevent excessive wear, the
   Besides spatial resolution, other factors   surfaces of the rings are coated with
that influence the detectability of            dichromium trioxide layers. The bonding
discontinuities are object surface             between the coating and the substrate has
reflectivity and emissivity problems.
Surface reflectivity is difficult especially
\Vith metal objects heated with lasers or
lamps. \\1ith nonmetals reflectivity is less
206 Infrared and Thermal Testing
to be strong enough to keep the coating       Crack, Inclusion and Impact
                     from breaking loose from the substrate. It    Damage Detection in Carbon
                     is not even necessary to have an air gap      Fiber Reinforced Composites
                     between the coating and the steel.
                     Weakened adhesion is enough.                  The infrared line scanning technique can
                                                                   be used for finding discontinuities like
                         Unfortunately, ultrasound is strongly     cracks,81 inclusions,56 and impact
                     attenuated in the coating material and        damage65,74 in carbon fiber reinforced
                     electromagnetic testing is not sensitive to   composites. One of the advantages of the
                     bonding strength variations. However,         infrared line scanning technique is the
                     thermal nondestructive testing has proven     generation of lateral heat flow in the
                     to be suitable for the task. Figure 17 shows  direction of the movement of the line
                     an infrared image of a 2 x 2 mm               source. In most of the pulsed thermal
                   (0.08 x 0.08 in.) adhesion discontinuity        nondestructive techniques the heat flow is
                    between a coating and a seal ring. ss The      in the direction normal to the surface of
                     discontinuity can be seen clearly as the      the composite, which makes it difficult to
                     hotter surface area (white) against the       detect vertical cracks or broken fibers.
                     otherwise cooler surroundings. In this
                     case, the weaker adhesion hinders heat           Hgure 18 shows that the detection of
                     flo'N from the coating to the substrate       fiber cracks is feasible with the infrared
                     causing the hot spot. The size of the         line scanning technique. In this case, the
                     imaged area is 100 x 14 mm                    sample in question is a unidirectional
                     (4.0 x 0.6 in.).                              carbon fiber composite that has protective
                                                                   skins on both sides. The composite is
                        The infrared image in Fig. 17 was          heated with the induction technique. In
                     obtained by using the line scanning           the infrared image an area of 50 x 30 rum
                     measurement setup depicted in Fig. 16c.       (2.0 x 1.2 in.) of the composite having a
                     The heat source was an argon ion laser        20 nun (0.8 in.) long and 160 ~m
                     beam focused on a 20 mm (0.8 in.) long        (0.006 in.) wide cut in it is shown. The
                     and 300 ~m (0.012 in.) wide line on the       direction of the fibers is from left to right
                     surface of the ring. The radial direction of  in the image.
                     the ring in Fig. 17 was from top to
                     bottom. The output power of the laser            In addition to the cut in the middle of
                     was 4 W. The diameter of the ring was         the image, a lot of finer details of the
                     270 mm (11 in.) and the \Vidth 37 mm          structure of the protective skin are
                     (1.5 in.). The thickness of the coating was   resolved with high contrast. These details
                     300 ~m (0.012 in.). For the detection, a      are typical for infrared images obtained
                     single-element mercury cadmium telluride      from carbon fiber composites heated with
                     detector measuring 25 x 25 pm                 the induction technique.
                     (0.001 x 0.001 in.} ·with a germanium lens
                     and a deflection mirror 'i\'as used (see         The technique is especially attractive
                     Fig. 14a). The detector operates in the 8 to  for carbon fiber reinforced composites
                     12 pm wavelength region and is cooled         because they contain both conductive
                     with liquid nitrogen to a temperature of      materials (carbon fibers) and
                     77 K (-196 'C = -321 'F). The line rate of    nonconductivc materials (epoxy and glass
                     the deflection mirror was about 100 Hz.       fibers). Discontinuities affecting the
                    The ring rotation and the data acquisition     carbon fibers alter the fibers' electrical
                     were controlled ·with a microcomputer.
                                                                   FIGURE 18. Infrared image of 20 mm (0.8 in.) long x 160 ~m
FiGURE 17. Thermal image showing 2 x 2 mm                          (6.3 x 10-3 in.) wide cut in unidirectional carbon fiber
(0.08 x 0.08 in.) delamination in ceramic coated steel ring.       composite plate.
                                                                   Noncontact Sensors for Infrared and Thermal Testing 207
properties, which in turn affect the eddy      stationary to
 currents and therefore the heat generation
 in the sample. On the other hand, the          transported t '1lposite panels and                             e
 nonconductive elements contribute to the       shaemcpolvee,rtehdebS0taat-dtCeCstasreitae.oIfntshteeasdaomfrtJle1 can
 heat generation hardly at all. As a result     (Fig. 16h). 'fl~~ moving the line scanne!
 the thermal image will show only details
 corresponding to the elements responsible      applied man s movement can                          even b         1.9~
 for the structural integrity of the sample.       In the il1} ltaiJy by hand115 as                 in Hg.
                                                with a vicke age, a carbon fiber compostt
    A good spatial resolution is vital in the                         r~1,hine
 detection of closed cracks. J:or such          representeq                     dentation        on it is   s  of     a
 purposes, the wide source generated by         glass fiber Q.                  composit         e consist
 the induction coil is not the best possible.   with carbo 11P~xy matrix strengthened .
 However, the induced eddy currents,            nets. The btl lber bundles forming loose
 which flow in the carbon fibers, are verr
 sensitive to the fiber breakage. In this       {0.3 in.) ap<tr~~les are about 7 mm
 sense, the induction heating again             induction teq IIl. each net. Again, th~ ·til ,
 provides a selective feature. \-\'hether this  conductive      ll1       1n1que hea     ts      the eiectnC•         11)e
 factor provides enough heat to be              carbon fibe               aterials. As   a       result, onlY      t
detected by infrared testing is                                 r
questionable. More likely, the detection is     {-eimage. The spets are resolved in th~
 possible because of the stopped heat flow      SO x 30 m 111                of the i.maged area IS
in the broken fibers. The heat input in the     indentation               2·0 x 1.2 m.). The                          f
composite is sensitive to the distance          1the image a.sC'an be seen in the middle ~)t
 between the induction coil and the             spot.                 a srnall diamond shaped
sample. Therefore, any curvature or
notches in the composite surface affect               Figure 19 h-                                                 t
the surface temperature. These effects can      quality typic <IS the same high cont:as
also be detected in Fig. 18.
                                                tgthe induco0         a} of images obtained               wtth
    Figure 18 was obtained by using the                                 l~eating. However
measurement setup described in Fig. 16a.        comparing
The radio frequency signal was obtained         dmeataniulsalblscuarr11e~~lnttgnpagroevwidieths  aFonifg.itmh1e8a,gsectl~1'ne"11.,111e~
from a standard signal generator and
                                                and variation ?Y the jitter
amplified \Vith a 200 '"' radio frequency       \Vith the det s 1 ~ the scanning veloCJ~}·
amplifier. The high power signal was then       Fig. 14a, the ~C'hon system described 111
fed through an impedance matching               cmoamnpuaacl tsc'Hal1c1i 0~IIalgn.neInr
circuit to a four turn rectangular coil used                                             is too heavy  for
for coupling the power to the composite                                                  future, more
(Fig. J5e). The size of the coil was about      become poss·~ensitive scanners \'\'ill
70 x 6 mm (3 x 0.25 in.) and the                                      1
resonance frequency 10 MHz. The                 plane    array  t     ,   le    with     the  use of  focal
direction of the coil movement was from                         0t~hchhtn~ohlforgeyqu(eFnigc,ie1s4ab)n-d
left to right in the image. Again for the          Because                                                      all
detection, a single-element cooled              skin depth,
mercury cadmium telluride detector                                                                          SD1'
(Fig. 14a) was used. The measurement
setup was controlled with a computer.           aradtdhiteior np,o_otrh~1eeptIhnd~uecnetitornathioena.tiInng haS a
    Another example of the power of the         induction co· couphng between the
induction he<Hing is impact damage
detection in carbon fiber composites.           become diffi Il and the sample will
Impact damages are an important
category of discontinuities. This kind of a     differs from cult if the sample geometrY
discontinuity can result, for example,          example, Wif~anar geometry- as, ~or. 56
from a bird striking an aircraft or from a      Figure   2f0ibseh, 0    tube    isnhfarpareeddciommapgoesoifte~s~.-
tool dropped during maintenance of an           carbon                \Vs an                                       Ill5
aircraft. Characteristically, there is only a   1. s                  2C  o.mposJ. te                     e r,(1(
minor mark on the impact side of the                  8  mm  (0.~--{      tn.) and       tube,   wh   os
composite, whereas severe delaminations                                                  thickn  ess  2   J11 111
and fiber breaking can occur inside and
on the other side of the composite.             FIGURE19,fiea ,                               .                Q12X0.12in,)
Unfortunately, the other side of the
composite is often inaccessible.                vickers hard    11estsStiegsntaitnudreenotfat3ioxn  3 mm       (·        glass           fiber
                                                composite.                                          in car     bon
    Lehtiniemi and llartikainen7·1 have
discussed the detection of impact damage
with the same kind of equipment as
represented above in the case of the crack
detection. However, it is also possible to
design a line scanning measurement
system that can be used for testing
208 Infrared and Thermal Testing
(0.08 in.). Instead of induction heating,               Other Applications
the composite is now heated with a hot.
air jet. The tube consists of six layers                Line scanning systems have been used for
embedded in epoxy matrix. In the top                    discontinuity detection in glass fiber tubes
layer the carbon fiber bundles, which can               and aluminum honeycomb compositesJ2
be seen as wide vertical stripes in Fig. 20,            It is also possible to detect moisture in
are parallel to the longitudinal axis of the            resin matrix composites and honeycomb
tube. Between the bundles are glass fibers.             structures. A variety of applications use a
The thickness of the first layer is 0.5 mm              line heat source for heating an objecti an
(0.02 in.). The deeper layers are wound                 infrared canlera is applied instead of a line
helically around the tube axis. Signs of                scanner for imaging. Such applications
the second layer can be seen as hot stripes             are, for example, the study of adhesive
at an angle of about 45 degrees. The                    bonds in aluminum laminates, where
almost horizontal stripes correspond to                 infrared lamps, cool and hot air jets are
fine grooves on the epoxy. These grooves                used as heat sources. 6b,s2 A related
steer the hot air jet along the tube surface.
As a result a distracting heat signature is             application studies corrosion in aircraft
constantly present during the testing.                  fuselages.83 Line scanning can be used
However, the discontinuities in carbon                  both as a reflection and a transmission
fiber composites can be quite large.                    measur~ment technique, although
Sometimes they can be detected despite                  detection from a single side of an object is
all the complications. In this case, the                usually preferable.
composite has an inclusion that can be
seen between the third and fourth carbon                   The applications discussed previously
fiber bundle from the left.                             apply active heating for detecting
                                                        discontinuities. Naturally, line scan
   l:igure 20 was obtained by using a                   techniques can be used for passive
measurement setup described in Fig. 16d.                monitoring as well. Line scanners are easy
The hot air jet was directed through a                  to place above conveyor belts, where they
narrow nozzle as shown in I:ig. lSd. The                can be used for monitoring various
nozzle was aligned parallel to the                      industrial products. Commercial line
longitudinal axis of the composite tube.                scanners are available for such
The narrow end of the nozzle has the                    applications, although infrared cameras
dimensions of SO x 3 mm (2.0 by                         are becoming more and more popular in
0.12 in.). The heating was generated with               industry. Other passive monitoring
a standard 1400 W hot air gun. The                      applications are airborne or satellite
angular velocity of the tube rotation was               infrared imaging applications. Line
adjusted to equal the scanning velocity,                scanners have been used for night aerial
that is, one full rotation of the tube                  surveys, mapping of land resources,
matches one frame exactly. The infrared                 meteorological observations and various
detection system was the same as                        military purposes.s4
described earlier.
FIGURE 20. Infrared image of inclusion in carbon fiber
composite tube.
                                                        Noncontact Sensors for Infrared and Thermal Testing 209
PART 4. Multicolor Radiometry near Ambient
Temperatures
Infrared radiometric imaging has been            A technique of determining the target
widely used to estimate the                   temperature in the environment is
two-dimensional temperature distribution      proposed by radiation intensities of the
on the surface concerned. As a means of       infrared radiometer with different wave
nondestructive remote sensing, infrared       hands. The respective infrared radiometers
thermography is applicable to various         and those sensors have a selected wave
engineering problems such as                  band in the infrared range. Described next
                                              is the methodology of determination of
discontinuity detection, condition            the temperature by multicolor radiometry
monitoring and characterization of heat       in consideration of the reflection intensity
and mass transfer. It is important to         in a simple model near ambient
analyze the fundamental characteristics of    temperature.
thermography to establish a practical
technique to distinguish the temperature         The applicability of the numerical
from the measured radiation intensity.        simulation to the temperature
The technology described below has been       determination is confirmed through a
documented in the published                   parametric study on how different values
literature.H7-93                              of emissivity correspond to output of the
                                              individual infrared radiometer. The
    A multicolor radiometer, often called a   experimental study is also performed to
radiation difference pyrometer, measures the  estimate the measurement error. The
radiation intensities at different            tricolor technique radiometer permits
wavelengths and deduces the temperature       quantitative temperature measurement
of the surface from the balance of these      without presuming temperature,
spectral radiation intensities. Generally,    emissivity and reflectivity of the surface
the multicolor radiometer is mainly used      wall. The temperature difference
to calculate the surface temperature \\'hen   calculated with the tricolor pyrometer is
the surface temperature of the objective      compared with that calculated with the
material is higher than that of the           hicolor pyrometer.
surroundings. The reflection intensity of
the surface injected from the                 Test Setup
surroundings is smaller than the emission
intensity of the surface. If the radiance     Jv1easurement of the temperature by
intensity is measured by infrared             means of bicolor and tricolor infrared
thermography near ambient temperature,        radiometers is carried out using a specially
the reflected ratio of the surface from       designed test apparatus to stabilize the
surrounding surfaces cannot be neglected.     background radiation. Two groups of the
Therefore, it is necessary to exclude the
reflection rate of total incident energy.
FIGURE 21. Schematic illustration of apparatus for testing of infrared bicolor radiometer.
Water tank                                    Cathode ray
                                              tube
      ~Hc--------=-H
                                              Central
                         Test plate           processing
                                              unit
                                              Personal
                                              computer
210 Infrared and Thermal Testing
infrared radiometer with filters are used      infrared radiometer near ambient
                     for the experiment.                            temperature. Three infrared radiometers
                                                                    are installed in an experimental cubic
                        The group A consists of a mercury           space. The sidewall of the space consists
                     cadmium telluride infrared radiometer          of the insulation layer inside covered with
                     with three calcium fluoride filters cooled     a black velvet texture. Temperature of the
                     by liquid nitrogen. The group B consists       cubic space is measured using several
                     of an indium antimonide and two                thermocouples. It is kept constant using a
                     mercury cadmium telluride radiometers          suction blower connected to the wall.
                     cooled by a stirling engine.
                                                                       A test piece with the heater is placed
                        Figure 21 shows a schematic                 700 mm (28 in.) from the three infrared
                     illustration of the experimental apparatus     radiometers. The test piece consists of
                     for testing the hicolor infrared radiometer    polished copper, stainless steel and black
                     near ambient temperature. The apparatus        painted copper plates. The size of test
                     consists of the test piece with the electric   plates measures 300 x 100 mm (12 x 4 in.)
                     heater, conical water hood regulated by        and is 10 mm (0.4 in.) thick. A silicon
                     the heat exchanger, infrared radiometers,      rubber heater is stuck on the backside of
                     cathode ray tube monitor and personal          the test piece. The surface temperature is
                    computer.                                       measured by the thermocouple of 0.1 mm
                                                                    (0.004 in.) diameter embedded in the
                        The water hood is installed between         plate of 1 mm (0.04 in.) deep. The
                     the test piece and infrared radiometer. The    experiment is performed at steady state
                     temperature of the inner blackbody wall        condition in the temperature range from
                     of the water hood regulated by the heat        322 to 435 K (49 to 162 "C; 120 to
                    exchanger can be constant. A velvet cloth       323 "F). A blackbody furnace is used to
                     the emissivity of which is nearly unity        calibrate each sensor. Thermography is
                     covers the surface of the inner wall of the    performed at a steady state condition.
                     water hood at a uniform temperature. The
                     covered black wall avoids the                  Multicolor Technique
                     multireflection effect from the
                     surroundings, people and light. The            Radiative Characteristics of
                     experiment is performed at steady state        Infrared Radiometer
                     condition in the ambient temperature
                     range- from 293 to 373 K (+20 to               Figure 23 shows a detection sensitivity of
                     100 "C; 68 to 212 "1').                        the infrared radiometer with three
                                                                    filters A1, A2 and A3. The central
                        The test piece is made of stainless steel,  wavelength of the filters are 8.37, 10.86
                     graphite, epoxy and polycarbonate resins       and 11.46 pm. The waveband width of
                     heated by the electric heater. The size of     each filter is about 1 pm.
                    test plates measures 150 x 150 mm
                     (6 x 6 in.) and is 15 mm (0.6 in.) thick.      FIGURE 23. Detection sensitivity of bicolor infrared
                    The temperature of the test piece is
                     measured by chromel-to-alumel                  radiometer with three filters.              . . -,,-""'l
                     thermocouples embedded in the test
                     plate.
                        Figure 22 shows a schematic
                     illustration of the experimental apparatus
                     for testing the bicolor and tricolor
FIGURE 22. Schematic illustration of apparatus for testing of
infrared bicolor and tricolor radiometers.
1 + - - - - - 1 . 9 m (75 in.)_-:----~1
          Test piece
t Heater                                 Thermographic
                                         cameras                                                                          I
                                                                                                                           I
                                                                           50       8 10 12
                                                                                                                            14
                                                                    .cg                  Wavelength i, (~rn)
                                                                    u
                                                                    *0
                                                                             0
                                                                                 6
                                                                    legend
                                                                       }.1 =filter 1 wavelength= 8.383 pm
                                                                       ),2 = filter 2 wavelength= 10.8821-Jm
                                                                       /,3 "'" filter 3 wavelength~ 11.482 IJm
                                                                    Noncontact Sensors for Infrared and Thermal Testing 211
Figure 24 shows a detectable energy of            3. Sensor A.{ has a wavelength
                    the radiometer with three sensors                        'A= 11.462 pm, temperature exponent
                    calculated using the Maxwell-Boltzmann                   11.-... == 3.6064 and detected blackbody
                    equation and the detection :..e11:-.ilivity, as          etH::'rgy Qh == 3.8526 X J0-2 G·'fthOM.
                    already shown in Fig. 23. The upper
                    straight line shows the detected blackbody              Figure 25 shows tile detection
                    energy denoted by the Stefan-Boltzmann               sensitivity of three infr<Hed radiometers
                     Ja-w:                                               B1, B2 and B:t. Three infrared radiometers
                                                                         are an indium antimonide sensor at 2 to
                    ·where Qh is energy (\'V·m-2) absorbed by            5 pm wavelength, a mercury cadmium
                    the blackbody, Tis temperature {kelvin)              telluride sensor at 6 to 9 pm and a
                   and Stefan-Boltzmann's constant o- =                  mercury cadmium tt'lluride sensor at 8 to
                     5.67 x 10--X \V·m-Z.K-4.                            13 pm.
                        The detected energy equations for the                Figure 26 shows a detectable energy of
                     three mercury cadmium telluride sensors             the three radiometers B 1, B2 and BJ
                    are simplified in the first ordered equation         calculated by a Maxwell-Boltzmann
                    in the temperature range from 293 to                 equation applied to the detection
                    373 K (20 to 100 oc; 68 to 212 °F):                  sensitivity. TJ1e upper straight line shovvs
                                                                         the detectable blackbody energy, as
                      1. Sensor A 1 has a ·wavelength /, = 8.363         defined by Eq. 21. Detection eneq,')'
                         pm, temperature exponent 111 = 4.8050           equations of indium antimonide and
                         and detected blackbody energy                   mercury cadmium telluride radiometers
                                                                         are simplified in the first ordered equation
                      Qb ~ 2.2451 x I()-' <>· T 4·8°5°                   in the temperature range from 322 to
                      2. Sensor A2 has a ·wavelength                     435 K (49 to 162 oc; 120 to 323 °F):
                         ), = 10.86 pm, temperature exponent               1. Sensor B1 has an indium antimonide
                         liz~ 3.7916) and detected blackbody                 element, a wavelength I~= 2 to 5 pm,
                                                                              a temperature exponent 114 = 9.2493
                      energy Qh = 1.1818 x 10-2 cr·Y:~.7YI6                  and detected blackbody energy
                                                                             Qh = 2.083 x 1o-16 o· y9.2-19].
fiGURE 24. Detectable energy of bicolor radiometer with
three filters.                                                            2. Sensor B2 has a mercury cadmium
                                                                              telluride element, a wavelength 1, = 6
                                                                             to 9 pm, a temperature exponent
                                                                              115 ~ 6.5377 and detected blackbody
                                                                             energy Qb = 6.5284 x 1o-9 o· 'f6.SJ77.
                                                                          3. Sensor B3 has a mercury cadmium
                                                                              telluride element, a wavelength ), == 8
                                                                              to 13 pm, a temperature exponent
                                                                              116 = 4.3067 and detected blackbody
                                                                             energy Qh = 4.3476 x H>-] 0;ruom.
                                                                             Bicolor and tricolor thermography tests
                                                                         using radiometers A and B are carried out
                                                                         with combination of two radiometers
                                                                         selected from three radiometers.
                                                                         FIGURE 25. Detection sensitivity of bicolor and tricolor
                                                                         infrared radiometers.
 200    f 300                                              400     500
(-73)                                                      (127)  (227)
f-100]     (+27)                                           [2601  [440)
           [+81]
        Temperature T, K(OC) [GF}
                                                                         23 4  5 6 7 8 9 10 11 12 13
                                                                                    Wavelength A (!Jm)
legend
                                                                         legend
  A Blackbody emission, Q/1 ,.-- GT,4.
   B. Qb=1.9818x1Q·lxo-f,4.Ct~l<'                                           ------ "'short wave, indium antimonide
                                                                           - =medium wave, mercury cadmium lellwide
      (mercury cadmium telluride, /,at 8 to 13 j.Jrn).                     -·-·- =long wave, mereury c.1dmium telluride
  C. Ql, = 3.8526 >·. J0-1 x oT,3LC6l ().1 at 11.462 pm).
  D. Qb = 1.1818 x 1Q-2 x oT?-79!6 (>, 2 a! 10.862 jJm).
  L Ov = 2.2451 x 10-s x or,uCtso (J,3 at 8.363 J.lm).
212 Infrared and Thermal Testing
Graybody and Pseudo Graybody                                            The hypothesis that T~ and Ta are
        Approximation                                                        much larger than Tv. is usually true when
                                                                             the sensor is cooled by liquid nitrogen.
        In case when lhe h'~l piece is enclosed                              Equation 21 is therefore rt>written in the
        with the blackbody surroundings, an                                  following form:
        enclosure model is shown in Fig. 27. \•Ve
        consider that tested surface S is                                    (23) ''"
        surrounded by blackbody surfaces A
        maintained at ambient temperature '(11 to                            where a is the radiosity coefficient and T5
        simplify the measurement field as a                                  is the radiation temperature.
        standard measurement system. The
        radiosity heat flux /i is a quantity leaving                             In general, the grayhody
        the surfaceS and is the sum of emitted                               approximation of nonmetal diffused
        and reflected energies. The reflected                                surfaces nm be applied:
        enert,•y is incident from the surroundings
        at '/~ and is transferred to the sensor R.                           (24) c + p ~
        The sensor is cooled at temperature of
        liquid nitrogen TR.                                                     The measurement fields for metal
                                                                             surfaces generally become complicated
            Because the test piece is surrounded by                          owing to the influence of specular
        the blackbody surfaces1 the effect of                                reflection of the surface. The sample
        multiple reflections between A and S is                              surface is estimated in a different way.
        negligible. Transferred heat flux /i from S                          Under a constant surface temperature,
        toR using emissivity and reflectivity is                             two radiosity coefficients a1 and a2
        expressed in the following form:                                     corresponding to two ambient
                                                                             temperatures ~~~ and T112, are shown in
        where c is emissivity and p is reflectivity.                         the following form using Eq. 23.
FIGURE 26. Detectable energy of bicolor and tricolor                         (T'I~:I]"
radiometers.
10' (26) (/2
1O'
                                                                             FIGURE 27. Enclosure model.
  L_                 I                                                           Enclosed surface
 200                      I                                                  /
(-73)
[-100]               I                                                                                             Sensor
                     I
                                                                                                                   /
                          I
        ____l_l_
         300    400           500                                                                                  Radiosity --+- R
        Ct27)  (127)         (227)
        {+80]  [260]         [440]
legend                                                                                                Refl('ction
  A Blackbody cmis5ion, Ot. =crT/.                                                         /
  B. Q =- 4.3476 ;<. 10-l x of,4 J01.9
                                                                                                  A
      (mercury cadmium telluride, ), at 8 to 13 11m).
  C. Q= 6.5284 x lQ-9 xof,6Hll                                               legend
                                                                                A=- blackbody surf<Jce
      (mercury cadmium telluride, }, at 6 to 91-fm).                            R =sensor
  D. Q = 0.2083 x 10· 15 x af,9.249l (indium antimonide, /,at 2 to 5 1-1m).     5 ""test surfilce
                                                                             Noncontact Sensors for Infrared and Thermal Testing 213
Using Eqs. 25 and 26, the summation        where ni is temperature index for three
of both emissivity E and reflectivity pis     filters, T5 is temperature of test piece, 'fa is
represented by the pseudo graybody            temperature of surrounding wall, £ is
appwximation b:                               emissivity, p is reflectivity, subscript s
                                              represents the test piece and subscript a
(27) b = £ + r                                the surrounding wall. The radiosity
                                              coefficient a includes the emission and
        a,crt- 7;~1) - az(Tsn -1~q            reflection of the incident irradiation.
                    r;1 -1~~                     The radiosity coefficient a and
                                              emissivity e for three filters are expressed
A glossy metal surface has a directional
property if its temperature is measured by    as follows:
a narrow band infrared radiometer. The
summation of both emissivity E and b          (32) (/
does not become unity. The summation b
is the pseudo graybody approximation in
a way similar to the graybody
approximation; b is the characteristic
value for various metal surfaces; a is also
given by the following form by
e)(~ rtransforming Eq. 23 using b.
(28) (/ = £ + (b-
                                              (33) E      1 - (7_,~)"'
                                                                     7~
         a-{~)"
i: r(29) £                                                T.,Iili _ b 1~ni
         1 - /J(                                          Tti - Tani
   The radiative properties for metal and     TABlE 1. Radiative properties on various material surfaces
nonmetal surfaces are shown in Table 1.       measured by three sensors. Ta == 293 to 373 K (20 to
The data are measured by the indium           100 °(; 68 to 212 °F),
antimonide (2 to 5 pm), mercury
cadmium telluride (6 to 9 pm) and              Material              Indium               Mercury
mercury cadmium telluride (8 to 13 pm)        Properties          Antimonide       Cadmium Telluride
sensors in the range of 293 to 373 K (20
to 100 oc; 68 to 212 °F) where the mean                           (2 to 5 ~m)  (6 to9~m) (8 to 13 ~m)
temperature is T, = 293 K (20 oc = 68 °F).    Stainless Steel     0.30         0.39 0.22
                                                  Emissivity £    0.60         0.59 0.71
Those data arc applied to calculation of          Reflectivity p  0.90         0.98 0.93
the multicolor technique for metal                b =E+p
surfaces.                                                         0.22         0.25 0.22
                                              Brass               0.61         0.65 0.71
Temperature Calculation                           Emissivity £    0.83         0.90 0.91
                                                  Reflectivity p
It is assumed that emissivity£, reflectivity      b =£+p          0.15         0.14 0.15
p and term b for each filter are constant                         0.75         0.76 0.83
and that graybody and pseudo graybody         Aluminum            0.90         0.90 0.98
                                                  Emissivity r
approximations can apply. The heat flux li        Reflectivity p  0.40         0.40 0.35
                                                  b =o£+p         0.50         0.47 0.63
from the surface of the test piece is                             0.90         0.90 0.98
expressed as:                                 Steel
                                                  Emissivity E    0.96         0.95 0.94
(31) I;  cr(cTti + PT.lni)                        Reflectivity p  0.04         0.05 0.06
                                                                  1.00         1.00 1.00
         a( cT~ni + (b - c)7~111 1                  b=~·+p
                                              Concrete
                                                  Emissivity £
                                                  Reflectivity p
                                                  b = £+r
214 Infrared and Thermal Testing
where i = 1,2,3 ... and T~ is the radiation                   (37) F, (7;,)      . [b'J~li~('J;iti]'J~lk
temperature for three filters used. The
ambient temperature Ta is already known                                        TJll + (7~'"'rk- bTtk
for bicolor calculation.
                                                                                Ti1k('l~l)m· - Tsni (T;k) nk
   These approximations are applied in
the range where two wavelengths of                                           + (T;k)nk ~ bTilk
bicolor filters are located close1y. The
radiation temperatures measured by the                                       =0
bicolor radiometer 7~1 and T~1 are
expressed in following equations:
(34) (T;i)ni               aT~ni                              i:;(where i = 1,2,3; j = 1,2,3; k = 1,2,3; i
                           €J~ni + pl~:Ii                     *for Eq. 36; and k j for Eq. 37.
                           cTti + (b- c)~~~i                     Because T~i• T;2 and Ta are measured by
                                                              thermography using the tricolor
(35) (T;jfi                a'/~11 i                           radiometer and thermocouple, the
                           €J:t1+ p7~lj                       temperature of the test surface T~ is
                                                              numerically and simultaneously solved by
                           tT~nj + (b- c)~111i
                                                              simultaneous Eqs. 36 and 37. Three
   Eliminating the emissivity, 7~ is given                    calculation temperatures using three
by solving the following equation Fi(T5).
                                                              filters 1'12, T2:{ and Tu are solved as
                                                              follows:
                                                               1. T 12, F1(T,), i = 1 and j = 2; and F.1(T,),
                                                                  i = 3 and k = 1;
                                                               i2. Tn, F2(1~), i = 2 and = 3; and F1(T,1),
                                                                  i = 1 and k = 2;
                                                               3. Tu, F1(T,), i = 3 and j = 1; and F2(T,),
                                                                  i = 2 and k = 3.
                               [ ( )";].bT;1m. - '}~i T;lJ.
                        Tsni + .L--~-~'----                   Experimental Results and
                                                              Numerical Analysis
                                       (TS.'J·)nj  -  bTnj
                                                         a
                                                          nj  Result and Analysis of Bicolor Test
                 ~1nj (T~i')ni - J:ti (T;i)
              +
                                                              Results of the birolor test were applied to
                        0                                     calculate test surface temperatures, using
                                                              the test apparatus shown in Pig. 21.
                                                              1-'igure 28 shows the relation between the
where i = 1,2,3 and j = 1,2,3 and i ":/: ;.                   calculated temperature 7 13 and function
                                                              FJCJ~) of the epoxy resin using sensor A1
   As the radiation temperatures T511 T\ 2                    (8.37 pm) and sensor A3 (11.46 pm) of the
and T53 are measured by thermography
and the ambient temperature by the                            mercury cadmium telluride radiometer.
thermocouple Ta (the temperature of the                       In this experiment, the temperature of
test surface 7~ is solved numerically. Three                  the ambient Ta is 293.2 K
calculation temperatures '1'121 '123 and T13
using three filters are solved in the                         (20.1 °C = 68.1 oF) and the temperature Ts
following conditions:                                         of the test piece is 363.8 K (90.7 "C =
1. T 12, F1('!;), i = 1 and j = 2;                            195.2 °F). The   calcul  ated temperature T  13
                                                                               358.8
                                                              at F3(T,) =0 is          K (85.7 oc = 186.2  °F)
2.  T 23 ,  Fz(T~),     i  =2  and  j  = 3;                   and isS K (Soc= 9 oF) less than the
3.                             and  j
    T 13 ,  F., ('I;),  i  =3          = 1.                   temperature measured using the
The cycle of numerical calculation is                         thermocouple 'J~.
iterated 20 to 30 times until the values
                                                              Figure 28b shows the relation between
converge.                                                     the calculated temperature T12 and
   The tricolor technique does not need                       function F 1(Ts) of the polycarhonate resin
to consider the ambient temperature Ta of                     using the mercury cadmium telluride
the enclosed wall in numerical calculation
                                                              sensor A1 (8.37 pm) and sensor A2
process. Eliminating emissivity €, the                        (10.86 pm). The ambient temperature'/~
values of T5 and Ta are deterrnined by                        is :l03.9 K (30.8 "C = 87.4 °F) and that of
solving Eqs. 36 and 37:
                                                              the test piece T, is 375.2 K (102.1 'C =
                                                              215.7 °F). The calculated temperature     T 12
                                                              at F1 u·,) =0 is 378.0 K (104.9 oc =
                                                              220.7 °F) and is 2.8 K (2.8 oc = 5.4 "F)
                                                              gre<~ter than the temperature measured
                                                              using the thermocouple Ts.
                                                              Noncontact Sensors for Infrared and Thermal Testing 215
Figure 29 shows the experiment<tl and        However, the temperature difference
                     theoretical result on the epoxy resin to
                     summarize the relation between the              !J.T23 = Tn-T~ (combining sensors A2 and
                     calculated temperature using the bicolor        A3) is 40 to 70 K (40 to 70 "C; 72 to
                     theory and the temperature measured             126 "F).
                     using the thermocouple. The result shows
                     that the temperature difference between         FIGURE 29. Experimental results on epoxy resin.
                     the experimental temperature and
                     calculated temperature is 5 to 20 K (5 to          t-.-:- -+--=t·500 (227) [440]~..
                                                                        ·t-(187)[368]~-t-···460                                  -J ..:
                     t•:r20 "C ~ 9 to 36 "1'): 12 ~ T12 - T,
                                                                                                                              .l_
                     (combining sensors A1 and A2) and 8T1.1 =
                     Tu- T~ (combining sensors A1 and A3).                                                                                        i
FIGURE 28. Relation between temperature Ts and function              E_"_ -{ t-1--~=-~G                                    -JI-ll
F3Ts of epoxy resin: (a) experiment using sensor 1 and                "-'
sensor 2; (b) experiment with slightly different parameters             420
                                                                               (147) [296]!
and using sensor 3 instead of sensor 2.                               "-tl ' .""1-;;, 380 (107) [224]1- - -
                                                                        :_!}-340 (67) [152], __
(a)                               H--                c~
          6                       t=                                    300 (27) [80)                1                            _l
                                                                                             300
       4              . r-                                                                  (27)   __l___       420         460    500
                                                                                             [80)               (147)      (187)  (227)
0                                                                                                  340 380      [296]      [368]  [440]
                                                                                                   (67) (107)
0                                                                                                  [152] [224]
 X2                                                                                                Temperature T5, K (0 C) [°F)
;:?
                                                  B
J: 0
                                                       l             legend
                      A
                                                             -~      + = filters 1 and 2
     I-2
           +                                         370 390          o = filters 2 and 3
                                                     (97) (117)
                                                     [206] [242]      A. =filters 3 and 1
                                                                     ~ = theoretical line
     -4        ...L   _.L.L ·: -
      250      270       290      310 330 350                        fiGURE 30. Measured emissivity 8£ and
     (-23)     (-3)      (17)     (37) (57) (77)                     temperature difference 8 T;i of epoxy and
     [-10]     [+23]     [62]     [98] [134] [170]                   polycarbonate resins.
                         Temperature Til K ec) [°F]
(b)
     2
0    0                                                           D.
0                        290 310 330 350 370 390
                         (17) (37) (57) (77) (97) (117)
"'X                      [62] [98] [134] [170] [206] [242]
                          Temperature T1, K (0 C) [°F]
;:?
~ -2
     -3
     -4
     -5         270
               (-3)
         250   [+23]
       (-23)
        [-10]
legend                                                                                       Drift of emissivity ~~£
  A. Temperature Ts = 293.2 K(20 oc = 68 <F).                        legend
  B. Temperature Ts = 358.2 K(85 °C = 185 "F).                        + = epoxy re~in results using filters 1 and 2
  C. Temperature fs = 303.9 K{31 oc = 87 oF).                          • =epoxy resin results using filters 2 and 3
                                                                        J,. = epoxy resin results using filters 3 and 1
  D. Temperature fs = 378.0 K(105 '>c = 221 °F}.                       (> "'" polycarbonate results using filters 1 and 2
                                                                       D = po!ycarbonate results using filters 2 and 3
                                                                       1:, = polycarbonate results using filters 3 ands 1
216 Infrared and Thermal Testing
Temperature measurement results on a                                     Experimental result of the bicolor test
                                                                                           is applied to solve the test surface, using
                 polycarbonate resin test piece using the                                  the test apparatus of Fig. 22. Three
                                                                                           radiometers of indium antimonide and
                 bicolor technique show that the                                           mercury cadmium teJiuride sensors B are
                                                                                           used to measure the radiation temperature
                 calculated temperature difference i'l.T12 of                              of the polished copper surface. The
                 sensors A1 and A2 combined and                                            graybody approximation is applied for
                                                                                           this calculation. The test result shows that
                 temperature difference                    i'l.Tu  o  f sensors     oAc1;  the temperature difference Tii is from 0.3
                 and A3 combined is S t                    o 20    K  (S to 20             to 8.0 K (0.3 to 8.0 'C; 0.5 to 14 ol') and is
                                                                                           4.0 K (4.0 'C = 7.2 'F) in mean.
                 9 to 36 °F). However, the calculated
                                                                                           Result and Analysis of Tricolor Test
                 temperature difference i'l.Tn in the second
                                                                                           Table 4 shows the numerical results of
                 combination of sensors A2 and A3 is over                                  calculated surface temperature Tst with the
                 100 K (1 00 'C = 180 'F). The result on                                   emissivity as a parameter in the case that
                 polycarbonate resin is quite similar. The                                 the true temperature is 340 K (67 °C =
                 temperature difference T23 that the central                               152 ol;). Calculated temperature Ts and its
                 detection wavelength approaches with                                      emissivity are shown in the table. The
                                                                                           graybody approximation is applied for
                 each other becomes inferior to that of 1'12                               this calculation.
                 and T13 •
                                                                                              Table S shows the calculated results of
                    Figure 30 shows the calculated                                         the surface temperature of blackbody and
                                                                                           copper surface. Proposed equations Fi(T5)
                 emissivity curve versus measured                                          in Eq. 36 and Fi(7~) expressed in Eq. 37
                                                                                           are used to obtain the calculated
                 temperatures Tii for epoxy and                                            temperature. ?vieasured and calculated
                                                                                           temperature is shown in the table. Result
                 polycarbonate resins. The temperature
                 differences 1'12 and 1'13 become smaller
                 than 10 K (10 'C = 18 'F) where
                 emissivity E = 0.02. However, 1'23 is 65 K
                 (-208 'C = -343 'F) where £ = 0.02. Filters
                 A2 and A3 cannot be combined for bicolor
                 measurement. An interval of the center to
                 center wavelength of two filters is needed
                 to be greater than the waveband ·width of
                 each filter.
                     The pseudo graybody approximation is
                 applied to calculate for the stajnless steel
                 surface. Table 2 shows the true
                 temperature 1~; calculated temperatures                                   TABLE 3. Temperatures T9 calculated temperature T13, T23,
                                                                                           T31; and temperature difference i'J. T13, t1 T23, tl T31 of
                 1'12, Tn, Tz3; temperature difference                                     graphite at T, ~ 293 K (20 'C = 70 °f).
                 i'l.Ttz = 1'12- 1~; temperature difference
                                                                                              r, t).Tt2 Tn nTu T23 ~T23 T,
                 tlT13 = 1'13 - Ts; and temperature
                 difference L'J.72.-.. = T23 - 1~. The mean value
                 of the temperature differences of i'l.T12 and                             299.9   -2.4  299.9             -2.4  300.3    -2.0      302.3
                 8T13 are 1.3 and 1.5 K (1.5 'C = 2. 7 'F)                                 321.9   -1.9  319.3             -4.5  320.8    -3.0      323.8
                 respectively.     However, AT23 are 2.6 K                                 330.8   -1.5  332.4                   332.4              332.3
                                   °F) greater than values of                       7'12   340.3   -1.8  344.0              0.1  343.5     0.1      342.1
                 (2.6 oc = 4.7                                                             350.1   -2.5  353.2              1.9  353.5     1.4      352.6
                                                                                           361.2   -1.4  364.5              0.6  365.8     0.9      362.6
                 and T13•                                                                  370.7   -1.8  375.2              1.9  377.5     3.2      372.5
                                                                                           !Ts12!        !Tsnl              2.7            5.0
                     Table 3 shows the calculated result of                                         1.9                     2.0  1Ts231    2.2
                 the graphite surface using radiometer A.
                 The temperature differences of i'J.7'12, tlT13
                 and i'J.T23 are 1.9 and 2.0 and 2.2 K (1.9
                 and 2.0 and 2.2 'C; 3.4 and 3.6 and
                 4.0 °r), respectively.
                                                                                           TABLE 4. Numerical results of surface temperature by
                                                                                                                                          = 340
TABLE 2. Temperatures Ty calculated temperature T13, T23,                                  tricolor technique:  f 12(T,),  F23 (T,),  T,         K
T31i and   tempera   tu  re  diff  eKre(n2c0e'Ci'l.T=136,  L\T23,  i'J.T31  of             (67 'C = 152 'F).
stainless  steel at  T,      293
                         =                                 8 'F).                                 Calculated Ts                             Emissivity
                                                                                           K ('C) ['F]
r, o.T12                 Tn flTn T23 nT23                                       T,                                                    c,'J E2
302.7       0.3      304.9          2.5  302.0             -0.4             302.4          333.43  (60.28)      [140.50]              0.90 0.91 0.92
315.7       0.4      315.4          0.1  313.3             -2.0             315.3          347.91  (74.76)      [166.57]              0.52 0.50 0.51
326.5       0.8      326.6          0.9  323.3             -2.4             325.7          331.96  (58.81)      [137.86]              0.22 0.21 0.20
332.8       0.8      330.0         -2.0  329.3             -2.7             332.0          333.45  (60.30)      [140.54]              0.12 0.11 0.10
343.6      -1.3      343.1         -1.8  340.0             -4.9             344.9          329.05  (55.90)      [132.62]              0.62 0.61 0.60
350.5      -1.3      349.4         -2.4  347.6             -4.2             351.8          348.84  (75.69)      [168.24]              0.60 0.20 0.40
364.5       1.7      362.1          0.7  359.8             -3.0             362.8
376.4       3.9      373.9          1.4  371.5             -1.0             372.5
ITs12!      1.3      lT5nl          1.5  lT523 l
                                                             2.6
                                                                                           Noncontact Sensors for Infrared and Thermal Testing 217
TABlE 5. Calculated results of surface temperature by tricolor method. F1(T5) by n1 and
n2, F3(T,) by n2 and n3, T, = 340 K.
True Tem~erature T5                         Calculated Tem~erature   Tem~erature Difference
K ('C) ['F]
                                            K ('C)  ['F]             K ('C)            roFJ
Blackbody                         [133.52]  343.97 (70.82) [159.48]  -14.42  (-14.42)  [-25.96]
      329.55 (56.40)              [161.33]  344.73 (71.58) [160.84]   -0.26   (-0.26)   [-0.47]
      345.00 (71.85)              [177.44]  348.86 (75.71) [168.28]   -5.09   (-5.09)   [-9.16]
      353.95 (80.80)
                                  [144.32]  346.49 (73.34) [164.01]  10.94   (10.94)    [19.69]
Polished Copper                   [160.70]  352.68 (79.53) [175.15]  -8.23   (-8.23)   [-14.81]
      335.55 (62.40)
      344.65 (71.50)
of the proposed calculation shows that
estimated error isS to 10 K (S to 10 oc; 9
to 18 oF) at nearly ambient temperature.
    The tricolor radiometer can measure
the surface temperature of reflective and
emissive materials without considering
the surrounding wall at nearly ambient
temperatures. ?vfeasured temperature error
of the tricolor radiometer isS to 10 K (S
to 10 oc; 9 to 18 °F) greater than that of
the bicolor one.
218 Infrared and Thermal Testing
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222 Infrared and Thermal Testing
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                                                                Noncontact Sensors for Infrared and Thermal Testing 225
CHAPTER
                   Contact Sensors for
                  Thermal Testing and
                               Monitoring
                                                              E. john Dickinson, University Laval, Quebec, Quebec,
                                                              Canada (Part 6)
                                                             Erik E. Muller, Agilent Technologies, Everett,
                                                              Washington (Parts 1 to 5)
                                                              Dennis P. Redline, Tempi!, Incorporated, South
                                                              Plainfield, New jersey (Part 7)
Parts 1 to 5 adapted with permission from Hewlett-Packard Application Note 290, Practical
        Temperature Measurements. © 1997 Agilent Technologies, Everett, Washington.
PART 1. Temperature Measurement1
This chapter discusses contact sensors for                        Development of
temperature measurement. The four most                            Thermometric Scales
common temperature transducers provide
electrical signals: the thermocouple, the                         Galileo is credited with inventing the
resistance temperature detector (RTD), the                        thermometer circa 1592,2<~ Jn an open
therrnistor and the integrated circuit                            container filled with colored akohol, he
sensor (Hgure 1 and Table 1). '1\vo types                         suspended a long narrow throated glass
of material applied to the surface of the                         tube at the upper end of which was a
test object are also discussed: liquid                            ho!Jow sphere. \'Vhen he<1ted, the <1ir in
crystals and temperature sensitive lacquer                        tht' sphere expanded <md bubbled
or crayon. Both have chemistries that                             through the liquid. Cooling the ~phere
change color when temperature changes.
FIGURE 1. Four kinds of temperature sensors: (a) thermocouple; (b) resistance temperature
detector; (c) thermistor; (d) integrated circuit.
(a) (c)
Temperature T                                                     Temperature T
(b) (d)
                                                   Temperature T  Temperature T
228 Infrared and Thermal Testing
caused the liquid to move up the tube.2                           48 and eventually 96 parts. The
Fluctuations in the temperature of the                            fahrenheit scale gained popularity
sphere could then be observed hy noting                           primarily hecause of the repeatability and
the position of the liquid inside the tube.                       quality of tht' thermometers that
This upside down_ thermometer was a poor                          Fahrenheit built.
indicator because the level changed with
barometric pressure and the tube !lad no                              Around 1742, Anders Celsius proposed
scale. Vast improvements were made in                             that the melting point of ice and the
temperature measurement accuracy with                             boiling point of water be used for the two
the development of the Horentine                                  benchmarks. Celsius selected zero degrees
thermometer, which incorporated sealed                            as the boiling point and 100 degrees as
construction and a graduated :scale.                              the melting point. l.ater, the end points
                                                                  were reversed and the centigrade scale \Vas
    In the ensuing decades, many                                  born. In 1948 the name was officially
thermometric scales were conceived, all                           changed to the celsius scale.
based on two or more fixed points. One                            In the early 1800s \-\'illiam Thomson
scale, however, was not universally                               (Lord Kelvin), developed a universal
recognized until the early 1700s when                             thermodynamic scale based on the
Gabriel Fahrenheit, a Dutch instrument                            coefficient of expansion of an ideal gas.
maker, produced accurate and repeatable                           Kelvin established the concept of absolute
meKury thermometers. For the fixed                                zero and his scale remains the standard
point on the low end of his temperature                           for modern thermometry.
scale, Fahrenheit used a mixture of ire
water and salt (or ammonium chloride).                               As an increment, one kelvin (K) equals
This was the lowest temperature he could                          one degree celsius ("C). One degree
reproduce and he labeled it zero degrees.                         fahrenheit ("1:) equals one degree rankine
For the high end of his scale, he chose                           ("H). One kelvin equals 1.8 degree
human blood temperature and called it                             fahrenheit. So I K = 1 oc ~ 1.8 op = 1.8 °1(,
96 degrees.                                                       The rankine scale ("R) is simply the
                                                                  fahrenheit equivalent of the kelvin scale
   \'\'hy 96 and not 100 degrees? Earlier                         and was named after an early pioneer in
scales had been divided into twelve parts.                        the field of thermodynamics, W.].1'f.
1n an apparent quest for more resolution,                         Rankine. Notice that the official kelvin
Fahrenheit divided his scale into 24, then                        scale does not carry a degree sign. The
                                                                  units arc expressed in kelvin, not degrees
TABLE 1. Advantages and disadvantages of temperature              kelvin.
sensors.                                                             On the absolute scale, the freezing
Advantages                           Disadvantages                point of water is 273.1 S K = 0 "C =32 "F.
Thermocouple                         nonlinear                    Reference Temperatures
    self-powered                     low voltage
    simple                           reference required           A temperature divider cannot he built as
    rugged                           least stable                 can a voltage divider, nor can
    inexpensive                      least sensitive              temperatures be added as lengths would
    wide temperature range                                        be added to measure distance. It is
    wide \'ariety of physical forms  expensive
                                     slow                         TABLE 2. Fixed temperature points in International
Resistance temperature detector      current source required
    most stable                      small resistance change      Temperature Scale.4
    most accurate                    four-wire measurement
    more linear than thermocouple                                 Element  Type                     Temperature       "F
                                     nonlinear                                             K oc
Thermistor                           limited temewture range
    high output                      fragile                      Hydrogen triple point       13.8033  ~259.347     -434.824
    fast                             current source required                                  24.5561               -415.469
    two·wire ohm measurement         self-heating                 Neon     triple point       54.3584  --248.594
                                                                                              83.8058               ~361.825
lntergrated Circuit Sensor           T < 523 K (250 "C ~ 482 'F)  Oxygen triple point       234.315    ~218.792     ~308.820
    most linear (temperature T)      power supply required                                  273.16     ~189.344
    highest output                   slow                         Argon    triple point     302,9146                  ~37.903
    inexpensive                      self-heating                                           429.7485     ~38.8350
                                     limited configurations       Mercury triple point      505.078                    32.018
                                                                                            692.677         0.0100     85.5763
                                                                  Water    triple point     933.473       29.7646    313.8773
                                                                                           1234.93       156.5985    449.470
                                                                  Gallium melting point    1 337.33     231.928      787.149
                                                                                                        419.527     1220.58
                                                                  Indium freezing point                 660.323     1763.20
                                                                                                        961.780     1947.52
                                                                  Tin freezing point                   1064.18
                                                                  Zinc freezing point
                                                                  Aluminum freezing point
                                                                  Silver   freezing point
                                                                  Gold freezing point
                                                                  Contact Sensors for Thermal Testing and Monitoring 229
necessary to rely on temperatures
                  established by physical phenomena that
                  are easily observed and consistent in
                  nature.
                      The International Temperature Scale
                  (ITS) is based on such phenomena.
                  Revised in 1990, it establishes seventeen
                  fixed points and corresponding
                  temperatures. A sampling is given in
                   Table 2. 4
                      Because only these fixed temperatures
                  are available instruments must interpolate
                  between them. But_ accurately
                  interpolating between these temperatures
                   can require fairly exotic transducers,
                  many of \\'hicll are too complicated or
                   expensive for practical situations.
                      The discussion immediately below
                  emphasizes the practical considerations of
                  transducer placement, signal conditloning
                   and instwmentation. Despite the
                  widespread popularity of the
                  thermocouple, it is frequently misused.
                   For this reason, the discussion
                  concentrates on thermocouple
                   measurement techniques. A more
                   thorough discussion of thermocouple
                   theory has been published elsewhere.5
230 Infrared and Thermal Testing
PART 2. Thermocouples1
                \'\'hen two wires composed of dissimilar       FIGURE 2. Thermoelectric effect:
                metals are joined at both ends and one of      (a) continuous current in thermoelectric
                the ends is heated, a continuous current       circuit; (b) net open circuit voltage, function
                flows in the thermoelectric circuit (Fig. 2).  of junction temperature and composition of
                Thomas Seebeck made this discovery in          two metals.
                1821.
                                                               (a)
                   If this circuit is broken at the center,
                the net open circuit voltage (the              @-<~---Me-ta-iA--1---;-Mre-tal-A--~1,
                thermoelectric voltage) is a function of
                the junction temperature and the                          MetaiB                       0
                composition of the two metals (Fig. 2h).
                                                               (b)
                   All dissimilar metals exhibit this effect.
                Table 3 lists common combinations of                                        Metal A
                two metals along with important
                characteristics. For small changes in
                temperature the thermoelectric voltage is
                linearly proportional to temperature:
                (1) aT
                wl1ere thermoelectric coefficient a is the     legend
                constant of proportionality. For real ·world
                thermocouples, a. is not constant but          eAll = thermoelectric voltage
                varies with temperature. Conversion from          i = electric current (A)
                voltage to temperature is discussed below.
TABLE 3. Thermocouple properties.
Type     Metal                     Color                  Thennoelectric             Wire Error                  NIST
      Proportion                   Codea                     Coefficient                                        Ranged
                                                                          Range Standard Special
                                           Resistance S (ttV·K-1)          (K)< (percent) (percent)               (K)<
                                           (see noteb) at T (K)'
B (+) 0.7 platinum ,0.3 rhodium gray       0.22   5.96 at 273             1143 to 1973 ±0.50           ±0.25    0 to 1820
                                           0.71  58.67 at 873              273 to 1173 ±0.50
B (-) 0.94 platinum, 0.06 rhodium red      0.36  50.38 at 273              273 to 1023 ±0.75
                                           0.59  39.45 at 273              273 to 1523 ±0.75
E (+) 0.9 nickel, 0.1 chromium     violet  0.78  25.93 at 273              273 to 1523 ±0.75           ±0.40 -270 to 1000
                                           0.19  11.36 at 873              273 to 1723 ±0.25
E (-)constantan                    red     0.19  10.21 at 873              273 to 1723 ±0.25
                                           0.30  38.75 at 273              273 to 623 ±0.75
I (+)iron                          white                                                               ±0.40 -210 to 1200
I (-) constantan                   red
K (+) 0.9 nickel, 0.1 chromium     yellow                                                              ±0.40 -270 to 1372
K (-)nickel                        red
N (+) nicrosit                     orange                                                              ±0.40 -270 to 1300
N (-) nisil                        red
R (+) 0.87 platinum, 0.13 rhodium black                                                                ±0.10 -50 to 1768
R (-)·platinum                     red                                                                 ±0.10 -50 to 1768
                                   black
s (+) 0,9 platinum, 0.1 rhodium
s (-)platinum                      red
T (+)copper                        blue                                                                ±0.40 -270 to 400
T (-·)constantan                   red
a. Standard United States color code.
b. Ohm per 305 mm (per double foot) at 293 K (at 20 ~c = 68 "F) for 20 American wire gage (AWG) wire.
c. 273 K= 0 "C = 32 <F.
d. Specified material range is for 8 AWG wire and decreases with decreasing wire size.
                                                               Contact Sensors for Thermal Testing and Monitoring 231
Measuring Thermocouple                                  only \'1 but connecting the volt meter in
Voltage                                                 an attempt to measure the output of
                                                        junction j 1 has created two more metallic
The thermoelectric voltage cannot be
measured directly because a volt meter                  junctions: 12 and J.t- Because h is a
must first be connected to the
thermocouple. The volt meter leads                      copper~to·copper junction, it creates no
themselves create a new thermoelectric
circuit.                                                thermal electromotive force (v~ = 0) but Jz
    A volt meter may be connected across a              is a copper~to-constantan junction, \Nhich
copper~to-constantan (copper nickel alloy)
thermocouple (type T) to produce a                      will add an electromotive force 0'2) in
voltage output (Fig. 3). It might he
expected that the volt meter would read                 opposition to \11• The resultant volt meter
                                                        reading \f will be proportional to the
fiGURE 3. Measuring junction voltage with
digital volt meter. Diagrams of equivalent              temperature difference between J1 and Jz,
thermoelectric circuits: (a) volt meter is
connected to copper constantan (type T)                 The temperature at j 1 cannot be
thermocouple; (b) thermoelectric circuit is
created by connecting volt meter to                     determined unless the temperature at h is
thermocouple (V3 = 0 V); (c) thermoelectric
circuit is equivalent to that in Fig. 3b,               measured first.
because copper-to-copper connection
junction creates no electromotive force.                Reference Junction
(a)                                                     One way to determine the temperature Jz
        ---1                                            is to physically put the junction into an
                                                        ice bath, forcing its temperature to be
               lh
                                                        273 K (0 oc ~ 32 °F) and establishing], as
 + ~rH.. igh1"1'...-------._-----"c''--'~+ h
   v~                                                   the reference junction. Because both volt
                                       Cn - ~           meter terminal junctions are now
                                                        copper-to-copper, they create no thermal
(b)                                                     electromotive force and the reading 1' on
                                                        the volt meter is proportional to the
                                                        temperature difference between j 1 and Jz.
                                                        Now the volt meter reading is (see Fig. 4):
                                                          If 1J 1 is specified in degrees celsius:
                                                        FtGURE 4. External reference junction for copper constantan
                                                        thermocouple: (a) thermocouple connected to volt meter;
                                                        (b) equivalent thermoelectric circuit.
                                                        (a)
                                                        -vrylow   Cu        +                                               h
                                                                 + V2-         1',
                                                                        Cn -
(c)                                                                    Vo~m~!~~TJ J4
  legend                                                +~(b)
    Cn = constantan resistance alloy (50 to 65 percent                        v - vl r 11
            copper, 35 to 50 percent nickel}                                  - +v, -
    Cu =copper
                                                                                                b
     I= electrical junction                              Legend
      \ 1 = voltage (V)                                    Cn =constantan resistance alloy (SO to 6S percent copper, 3S to
                                                                  SO percent nickel)
                                                           Cu =copper
                                                              I= electrical junction
                                                             T"" temperature (K)
                                                             V = voltage (V)
232 Infrared and Thermal Testing
(3) T11 ('C) + 273.15                                    This circuit still provides moderately
                                                      accurate measurements as long as the volt
then the volt meter reading F becomes:                meter high and low terminals (h and j 4)
                                                      act in opposition (Fig. 6).
(4) v1 - \;z
                                                         If both front panel terminals are not at
                 o:[(T11 + 273.15)                    the same temperature, there will be an
                                                      error. For a more precise measurement,
            (T12 + 2n 1s)]                            the copper volt meter leads should be
                                                      extended so the copper-to-iron junctions
                   o:(7j1 - T12 )                     are made on an isothermal (uniform
                  (T11 - 0)                           temperature) block (J'ig. 7).
                   aT11
                                                         The isothermal block is an electrkal
This protracted derivation is used to                 insulator but a good heat conductor and
emphasize that the ice bath junction
output V2 is not 0 V. It is a function of             it serves to hold 1:~ and J4 at the same
absolute temperature.
                                                      temperature. The absolute block
    By adding the voltage of the ice point            temperature is unimportant because the
reference junction, the reading F has now             two copper iron junctions act in
been referenced to 273 K (0 'C = 32'F).               opposition:
This technique is very accurate because
the ice point temperature can be precisely            (5) v
controlled. The ice point is used by the
National Institute of Standards and                   FIGURE 6. Junction voltage cancellation:
Technology (NIST) as the fundamental
reference point for their thermocouple                v, = vif v, = V4.
tables, so thermocouple tables can be
consulted to convert directly from                    legend
voltage \1 to temperature 7)1•                        Cu = copper
   The copper constantan thermocouple                   I = electrical junction
shown in Fig. 4 is a unique example
because the copper wire is the same metal               V = voltage (V)
as the volt meter terminals. If an iron
constantan (type J) thermocouple is used              FIGURE 7. Removing junctions from digital volt meter
instead of a copper constantan                        terminals.
thermocouple, the iron ·wire (Fig. 5)
increases the number of dissimilar metal                                           Cu h
junctions in the circuit as both volt meter                 +
terminals become copper-to-iron
thermocouple junctions.                                 legend
                                                           Cn = constantan resistance alloy (50 to 65 percent copper, 15 to
FIGURE 5. Iron constantan (copper nickel                           50 percent nickel)
alloy) couple.                                             Cu =copper
                                                            Fe = iron
    Cu           + ,,
               ~Cn -v,                                      I = efectrie<ll !unction
+
  v                                                          T = temperature (K)
 Vo!t~e~ J 14                                              \'=voltage M
Legend
  Cn ==constantan resistance alloy (50 to 65 percent
        copper, 35 to 50 percent nlckel)
  Cu =copper
  Fe= iron
    J =electrical junction
   V =voltage M
                                                      Contact Sensors for Thermal Testing and Monitoring 233
Reference Circuit                                       junction will have no effect on the output
                                                                         voltage as long as the two junctions
                 The circuit in Fig. 7 will gh•e accurate                formed by the additional metal are at the
                 readings but it would be expedient to                   same temperature (Fig. 9). This conclusion
                 eliminate the ice bath if possible.
                                                                         is useful because it completely obviates
                    The ice bath can be replaced with                    the iron wire in the low lead (Fig. 10).
                 another isothermal block (Fig. 8). The new
                 block is at reference temperature Trer and                  Again F = o:(T1 - 'J~l'f) l\'here o: is the
                 because hand 14 are still at the same                   thermoelectric coefficient for an
                 temperature it can again be shown that:
                                                                         iron-to-constantan thermocouple.
                     This is still a rather inconvenient                 Junctions J~ and J-1 take the place of the
                 circuit because two thermocouples must                  ice bath. These two junctions now
                 be connected. The extra iron wire in the                become the reference junction.
                 negative (low) lead can be eliminated by
                 combining the copper~to-iron junction J.J-                  The next logical step is directly to
                 and the iron-to-constantan junction .Iref·              measure the temperature of the
                    This connection can be accomplished                  isothermal block (the reference junction)
                                                                         and use that information to compute the
                 by first joining the two isothermal blocks
                 (Fig. 8b). The output voltage V remains                 unknown temperature 7J 1 (Fig. 11).
                 unchanged (Eq. 5):                                          A thermistor, whose resistance R-r is a
                     Now the law of intermediate metals                  function of temperature, provides a way
                 eliminates the extra junction. This                     FIGURE 9. law of intermediate metals:
                 empirical law states that a third metal (in             (a) intermediate metal with isothermal
                                                                         junctions; (b) lead equivalent to Fig. 9a;
                 this case, iron) inserted between the two               (c) lower lead in Fig. Sb; (d) lead equivalent
                 dissimilar metals of a thermocouple                     to Fig. 9c.
                                                                         (a)
                                                                              Metal A           Metal B           Meta! C
                                                                                       \) \)
fiGURE 8. Elimination of ice bath: (a) replacing of ice block
with isothermal block; (b) joining of isothermal blocks.
(a)                                         Isothermal block                                                       Isothermal connection
        ---,
                   ,----,/                                               (b)
+ ,,                                                                                   Metal A           Metal C
                                                                     Cn
     Volt meter    I.                                                    (c)
                                                                                 Cu             Fe                Cn
                 r..:f isothermal block                                         \)              \
(b)                                                                         [
     High Cu.---------~
     ,,+ --1>---,                        II''+~
              IV
                  vI h I _v'_j ''
                                                                         (d)
                 Cu: Fe +~
     low
                 L -''----- -'-"' J
                            \
                                           Isothermal block at T" 1
legend                                                                   legend
  Cn =constantan resistance atroy (50 to 65 percent copper, 35 to          Cn =constantan resistance a!toy (50 to 65 percent
          50 percent nickel)                                                      copper, 35 to 50 percent nickel)
  cu =copper                                                               Cu =copper
                                                                            Fe= iron
   Fe =iron                                                                T" 1= reference temperature (K)
    I = electrical junction
    V =voltage (V)
234 Infrared and Thermal Testing
to measure the absoh1te temperature of                 any device that has a characteristic
the reference junction. junctions hand ;.1             proportional to absolute temperature: a
and the thermistor are all assumed to be               resistance temperature detector, a
at the same temperature, because of the                thermistor or an integrated circuit sensor.
design of the isothermal block.
                                                       Advantages of Thermocouples
 1. Use a digital multimeter to measure Rr
    and find 'J~cf·                                    H seems logical to ask why, if a device
                                                       that will measure absolute temperature
 2. Convert Tree to its equivalent reference           (like a resistance temperature detector or
    junction voltage Free·                             thermistor) is available, a thermocouple
                                                       that requires reference junction
 3. 1\,feasure V.                                      compensation is needed. The single most
 4. Add Vrcf and F to find \'1•                        important answer to this question is that
 5. Convert \11 to temperature TJJ.                    the thermistor, the resistance temperature
                                                       detector and the integrated circuit
   This procedure is known as softwme                  transducer are only useful over a certain
compensation because it relies on                      temperature range. Thermocouples, on
software in the instrument or a computer               the other hand, can be used over a range
to compensate for the effect of the                    of temperatures and optimized for various
reference junction. The isothermal                     atmospheres.
terminal block temperature sensor can be
                                                          Thermocouples are much more rugged
FIGURE 10. Equivalent circuit.                         than thermistors, as evidenced by the fact
                                                       that thermocouples are often welded to a
            Cu                                         metal part or damped under a scre\\'. They
                                                       can be manufactured on the spot, either
+                                                      by soldering or welding. In short,
                                                       thermocouples are the most versatile
v                                                      temperature transducers available and
                                                       because the measurement system
       Cu                                              performs the entire task of reference
                                                       compensation and software
                II                                     voltage-to-temperature conversion, using
                : ,, 1"-                               a thermocouple becomes as easy as
                ____ j          T,d                    connecting a pair of wires.
Legend                                                    Thermocouple measurement becomes
                                                       especially convenient when it is necessary
Cn = constantan resistance alloy (50 to 65 percent     to monitor many data points. This is
        copper, 35 to 50 percent nickd)                accomplished by using the isothermal
                                                       reference junction for more than one
Cu = copper                                            thermocouple element (Fig. 12). A relay
 Fe = iron                                             scanner connects the volt meter to the
  J = electrical junction
T,.1 = reference temperature (K)
  V = voltage (V}
FIGURE 11. External reference junction                 FIGURE 12. Switching multiple thermocouple types.
without ice bath.
                                   Block               +~
                                   temperature           v I High
                                IT"'                   -~Low
                                                          __i ~--
                Cu
                                           Fe          Vo!t meter
                                                                       All copper wires
                                          v+, '·                                                    \ Pt/10Rh
           I    Cu                   Cn ~                                                                                           Isothermal
Volt~et~ J                                                                                                                          block
                                R,                                                                                                  (zonE' box)
Legend                                                 Legend
  Cn =- constantan resistance alloy (50 to 65 percent         Cn = constantan resistance alloy (50 to 65 percent copper, 35 to
         coppN, 35 to 50 percent nickel)                              50 percent nickel)
  Cu = coppN                                                   Fe = iron
   Fe=- iron                                                    Pt = platinum
                                                        Pt/lORh = 90 percent pl"tinum; 10 percent rhodium
    J = electrical junction                                    Rr = resistance measurement
   Rr = resistance measurement                                  V =voltage 0/)
    V = voltage (V)
                                                       Contact Sensors for Thermal Testing and Monitoring 235